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We have synthesized fourdioxotetraamine ligand appended with fluorenyl group and their transition metal complexes.The crystal structures of the complexes were determined by x-ray diffraction. Stability,electrochemistry and switch properties in aqueous solution was studied by pH-potentiometricand fluorimetric titration as well as cyclic voltammetry.

合成了带侧链荧光基团—芴的二氧四胺配体及其过渡金属配合物，测定了过渡金属配合物的晶体结构，研究了他们在水溶液中的稳定性、电化学性质和荧光开关性质。

A novel supramolecular complex, [Cu2]CH3OHH2O (fum=fumarate dianion, dpphen=4, 7-diphenyl-1, 10-phenanthroline), has been prepared from the reaction of bidentate ligand, fumarate with CuCl2, and were characterized by element analysis, IR, thermal analysis and X-ray diffraction technique.

利用螯合配体4，7-二苯基－1，10-邻菲罗啉与反丁烯二酸钠及铜盐反应合成了一种新型超分子配合物[Cu2]CH3OHH2O（fum=反丁烯二酸根，dpphen=4，7-二苯基－1，10-邻菲罗啉）。通过元素分析、红外光谱、热分析和X射线单晶衍射等技术对其进行了表征。

Associated minerals are primary glauberite, halite and terrigenous mud; while calcite is absent or rare. The X-ray diffraction analysis shows that the mud-sized crystalline dolostone has an average CaCO3 mole content of 57.30% and an average degree of order of 0.40, revealing the characteristics of higher calcium content and lower degree of order. It is closely intergrown with glauberite, indicating that the aqueous medium in the depositional environment of mud-sized crystallinedolostone was hypersaline water or dilute brine. The temperature of water in the depositional environment calculated according to the oxygen isotope data averaged 30.5℃ and the minimum homogenization temperature of inclusions in primary glauberite crystals associated with mud-sized crystalline dolomite was 44℃. The two groups of temperature data are close, indicating that the temperature of the water in the paleolake environment during the deposition of mud-sized crystalline dolostone ranged from 30.5℃ to 44℃.

泥晶白云石在阴极发光下呈红色、橙红色，与其伴生的矿物除原生钙芒硝、石盐、陆源泥质外，方解石没有或极少；X衍射分析结果表明，泥晶白云石的CaCO3摩尔含量平均为57.30%，有序度平均为0.40，具高富钙、低有序的特征；与钙芒硝岩的紧密共生，说明泥晶白云岩沉积环境的水介质为高盐度的咸水或淡卤水；根据氧同位素数据计算的沉积环境的水体温度平均为30.5℃，与泥晶白云石伴生的原生钙芒硝晶体中的包裹体均－温度最低值为44℃，这两组温度数据基本接近，表明泥晶白云石沉淀时环境水体的温度大致在30.5-44℃之间。

Mechanism of poly(dioxanone- co -glycolide) sutures in vitro degradation was studied by DSC and X-ray diffraction and the surface morphology was studied with photography for the purpose of improving properties of absorbable sutures.

用DSC和X-ray衍射法对聚对二氧环己酮-乙交酯缝合线的初期体外降解过程进行了研究，并使用纤维摄影仪对纤维在降解过程中的表面形态变化进行了观察。

The product was characterized by scanning electron microscopy, X-ray diffraction and laser granula analyzer, etc.

采用扫描电子显微镜、X射线粉末衍射仪和激光粒度分布测试仪等对实验产品进行表征。

PAAS was selected as dispersant to evaluate the dispersion stabilization of SiO2 nanoparticles by a diffraction-based laser granulometric analyzer and identify the state of adsorption of the dispersant on the surface of nanoparticles by an IR spectrometer.

选择了聚丙烯酸钠作为分散剂，并通过激光粒度分析仪对纳米颗粒的分散稳定性进行评价，通过红外光谱仪对分散剂在颗粒表面的吸附状态进行识别。

The products determined by X-ray diffraction are graphitic.

产品晶态结构完好，碳的石墨化程度较高。

X-ray diffraction experiments indicated that the films consisted of g-C3N4 and β-C3N4, and the graphitic form carbon nitride was the main component of the film.

IR光谱证实了薄膜中碳氮化合物的形成，而XRD的检测结果表明，类石墨相g-C3N4是碳氮薄膜中的主要成分，同时有极少量的β-C3N4晶相生成。

The XRD studies show obvious diffraction peaks associated with graphitic carbon and Co metal. Co particles in the composite are stable even at 2500℃ in inert atmosphere .

复合微球的 X 衍射图显示出明显的石墨碳和金属钴的衍射峰，2500℃石墨化后，复合微球中的钴仍能稳定存在。

The products were characterized by X-ray diffraction, scanning electron microscopy, transmission electron microscopy and thermal gravimetric analysis.

采用X射线衍射仪、傅里叶变换红外光谱仪、扫描电子显微镜、透射电子显微镜和热失重分析仪等对产物的组成、形貌以及热失重情况进行了表征。

Nowadays, most of research are to build a transmutative Petri Nets through adding controlling place sets, controlling arc sets and controlling policy to the basic Petri Nets, while the Controlled Petri Nets could be used to argue many controlling theory problems conveniently and to induce many logically and physically supervisory and solve the Event Feedback Controlling Problems and State Feedback Controlling Problem in DEDS supervisory theory.

目前大多数的研究表现为在变形后的受控Petri网基础上，利用各种方法求得各种逻辑型、结构型控制器，解决DEDS监控理论中的事件反馈控制问题与状态反馈控制问题。

On one hand, there are discussions with the works council and union about extension of short time working up to the end of September.

一方面，有讨论，工程理事会和联盟关于延长工作时间短至9月底。