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The inperfect crystal structure and its analysis for materials, is an elective course for the master graduate student, which include the crystallology principle, development of crystal diffraction, crystal determination and computer simulation of new phase, analysis of solid solution and superstructure, correction of crystal structure and bondvalent theory, analysis of inperfect crystal structure, analysis of amorphous structure and so on.

材料不完整晶体结构及其分析方法，为材料科学及工程等专业硕士研究生的选修课，内容包括晶体学基础、晶体衍射技术最新进展、新相晶体结构测定与数值模拟、固溶体与超结构分析、晶体结构修正与价键理论、不完整晶体结构分析、非晶结构分析等。

According to the electrical diffraction of the conglomeration, the particles are A-zeolite crystals. In the surface of micro-crystal of A-zeolite, the cuboidal nano-crystal A-zeolite grows, so A-zeolite crystal steps can be observed with TEM.

同时，在A型沸石的晶化初期，样品的TEM照片中可见许多团聚体，部分团聚体表现为A型沸石所具有的立方体形态，根据电子衍射测定，构成团聚体的颗粒为大量的纳米晶体。

In the condition of keeping F、 K、Na content fixed, To improve slag structure and raise slag melting point and viscosity, MgO content is raised and TiO〓 is added. the main content is as follows:(1) Keeping CaO/SiO〓 fixed, MgO content rises from 10% to 16%, the free running temperature goes up 106℃, the viscosity goe down at bigger than 1425℃, but difference is little; keeping /SiO〓 fixed, MgO content rises from 10% to 16%, the free running temperature rises 87℃, the viscosity rises too; adding TiO〓 to 5%, the free running temperature goes up 98℃, the viscosity rise a little.(2) Powder crystal x ray diffraction and microscopic analysis shows: increasing MgO content, the cuspidine will decreace or even disappear, the monticellite goes up with MgO content rising, keeping /SiO〓 fixed, Akermanite content goes up, for high melting point minerals appear or go up, the free running temperature of the slag bearing F is raised; Adding TiO〓, high melting point mineral—Perovskite forms, it can making other minerals'crystalling fast, it is the reason that TiO〓 raises the free running temperature of the slag bearing F.

2对测定粘度的冷凝渣所进行的X粉晶衍射及显微分析和鉴定表明，增加MgO含量，渣中枪晶石将减少甚至消失，而钙镁橄榄石则随MgO含量增加而增加，在／SiO〓不变时，黄长石含量也有所增加，高熔点矿物的出现和增加，提高了含氟熔渣的熔化性温度；加入TiO〓熔渣中将形成高熔点矿物-钙钛矿，钙钛矿的形成还促使黄长石的结晶，这是TiO〓提高含氟熔渣熔化性温度的根本原因。

Based on the problem of various types of catalyst and according to the features of carbonylation catalysts reactions, our team has been designed a series of new metal complexes of benimidazoles, which can be used for carbonylation catalyst of industry. Seven new benzimidazole derivatives were prepared by the o-phenylenediamine、oxalic acid、glycolic acid、monomethyl monopotassium malonate、ethyl cyanoacetate、succinic anhydride. The structures of them were confirmed by IR、Elemental analsis. The crystal structures of d and e were determined by X-ray single crystal diffraction of Germanic Bruker Smart APEX II CCD. The catalysis of them was tested by carbonylation reactions.

本文设计以邻苯二胺和草酸、羟基乙酸、丙二酸单甲酯、氰基乙酸乙酯、丁二酸单甲酯为原料采用PPA催化和无机酸催化法，合成了4种苯并咪唑-2-羧酸衍生物并进行了表征；培养了2个化合物d、e的晶体并测定和讨论了晶体结构；制备了3种未见报道的苯并咪唑金属配合物，对配合物在羰基化法制醋酐-醋酸反应的催化作用进行了初步试验。

Take DMSO swollen treatment and DEA-SO2-DMSO decrystallization treatment for example, the X-ray diffraction and the Tobolsky's intermittent stress relaxation of treated woods were determined during soaking in water, analyzed the effects of water on crystal degree and inter-cohesion of treated woods. According to these continuous relaxation curves measured in water with different temperatures, various thermodynamic quantities were obtained by using Eyring absolute rate theory, and reviewed the chemical reactions in wood which occur in different relaxation process. For the first time quantify these crosslinkings formed in the process of tensional relaxation by using the SMCIR intermittent stress relaxation way, and defined the cross-linking reaction types. In order to find out the contribute of drying to the fixation of deformation of chemically treated wood, stress relaxation of oven-dry untreated and treated wood was measured during the process of temperature elevation and descend, then analyzed the effect of temperature change on relaxation mechanism of treated oven-dry wood. According to continuous relaxation curves of oven-dry treated wood under various constant temperature, calculated the thermodynamics of relaxation process and discussed the mechanism of molecule change in wood, at the same time, also quantified these cross-linkings produced in wood by intermittent method and on the basis of which the model of molecular change during relaxation process of chemically treated was constructed.

以DMSO膨胀处理及DEA- SO2-DMSO非晶化塑化处理为例，测定了两种处理木材在水浸渍过程中的X射线衍射及Tobolsky间歇应力松弛，分析了水对处理木材结晶度及内部凝聚力的影响；通过未处理和两种处理木材在不同温度水中的连续应力松弛测定，应用Eyring的绝对速度反应理论计算并获得了松弛过程中的各热力学量，分析了在水中松弛过程中不同阶段木材内部发生的化学反应；并首次采用SMCIR连续·不连续双曲线应力松弛法定量了轴向拉伸应力松弛过程中木材内部产生的架桥量，明确了交联反应的类型；为了了解干燥对处理木材塑性变形固定的影响，测定了未处理和两种处理绝干木材在温度下降过程和上升过程中的应力松弛，分析了温度变化对处理绝干木材应力松弛的影响；根据多个温度水平下的连续应力松弛测定曲线，计算松弛过程的热力学量，考察了绝干木材在松弛过程中内部发生的分子变化机理，同时也用间歇法定量了木材内部新形成的架桥量，并在此基础上构筑处理木材在松弛过程中内部分子构造的变化模型。

On the basis of developing a new technology to synthesize sodium diacetate successfully without any pollution,the culture of bigger crystal in perfect shape and single crystal of small dimension suitable for X-ray diffraction was attained.

在研究成功双乙酸钠零污染合成工艺的基础上，培养成功了晶型完美的大尺寸晶体和适宜进行X光结构分析的小尺寸单晶，并进一步应用四圆衍射仪测得其晶体结构。

This is the first example of two-dimensional lanthanide MOFs with one dimensional water chains.2、Coordination polymer[Nd_2_3(H_2O)_2]·bpy·4H_2O(2)(bpdc=2, 2′-bipyridine-3,3′-dicarboxylate,bpy=4,4′-bipyridine)had been synthesized under hydrothermal conditions and its structures were determined by X-ray diffraction,and confirmed by IR and TG analysis.

该结构是在二维骨架的镧系配位聚合物中首次观察到的一维的水链结构。2、以Nd_2O_3，2，2′-联吡啶-3，3′-二羧酸和4，4′-联吡啶为原料，采用水热法合成了一个具有二维骨架结构的配位聚合物[Nd_2_3(H_2O)_2]bpy·4H_2O，通过IR、x射线单晶衍射分析和热重等手段对其结构进行了表征。

Design and Analysis of Diffractive Optical Element on Laser Transmission Welding Based on Diffraction.

衍射型激光透射塑料焊接的衍射光学元件设计与分析。

Hexaaquamanganese dipicrate dihydrate is prepared and characterized by single-crystal X-ray diffraction.

并分析研究了作为杯芳烃配合物的客体之一的苦味酸锰的晶体结构。

Twelve regular copolyesters were synthesized by solution polycondensations of the four monomers with hydroquinone, chlorohydroquinone, 4,4'-dihydroxy biphenyl. The copolyesters were characterized by polarized microscope with hot stage, DSC and X-ray diffraction.

将上述单体与对苯二酚、氯代对苯二酚以及联苯二酚用溶液缩聚的方法合成了十二种规则共聚酯，并用热台偏光显微镜、DSC、X-衍射等方法对共聚酯进行了表征。

Nowadays, most of research are to build a transmutative Petri Nets through adding controlling place sets, controlling arc sets and controlling policy to the basic Petri Nets, while the Controlled Petri Nets could be used to argue many controlling theory problems conveniently and to induce many logically and physically supervisory and solve the Event Feedback Controlling Problems and State Feedback Controlling Problem in DEDS supervisory theory.

目前大多数的研究表现为在变形后的受控Petri网基础上，利用各种方法求得各种逻辑型、结构型控制器，解决DEDS监控理论中的事件反馈控制问题与状态反馈控制问题。

On one hand, there are discussions with the works council and union about extension of short time working up to the end of September.

一方面，有讨论，工程理事会和联盟关于延长工作时间短至9月底。