查询词典 dibasic carboxylic acid

The ammonia was evaporated under decreasing pressure, and the precipitate was filtered off and the liquid was poured into hot saturated picric acid solution to get picrate with a yield of 85.0%. The optimum process starting from imidazole-4,5-dicarboxylic acid was: imidazole-4,5-dicarboxylic acid in acetic anhydride was refluxed to get imidazole-4-carboxylic acid, and the product was esterification in ethanol with a catalyzer of concentrated sulfuric acid to get ethyl imidazole-4-carboxylate, at last the compound above was reduced by LiAlH4 in ether at room temperature to get the target compound, the total yield of this route was 49.6%.

以4，5-二羧酸咪唑为原料的较佳工艺：1 脱羧反应：4，5-二羧酸咪唑40g，醋酐1200ml，回流10h，过滤并将滤液浓缩至干，所得固体加至50%的乙醇溶液回流，过滤并将滤液自然冷却过夜，过滤得固体；2 酯化反应：4(5)-羧酸咪唑50g，乙醇1000ml和浓硫酸60ml，加热回流2h，5%浓度NaOH溶液调节至pH＝8，减压浓缩至干，加入少量水回流，自然冷却过夜并过滤得固体；3 还原反应：LiAlH410g，乙醚300ml和4(5)-羧酸咪唑乙酯28g，常温反应1.5h，小心滴加25ml水后过滤，滤渣溶于300ml甲醇中并过滤，收集所得乙醚和甲醇滤液浓缩至干，将所得固体溶于300ml乙醇中加热回流，后将溶液浓缩至约30ml，冷却并过滤得固体，该路线总收率为49.6%。

The diluent solution of glyoxylic acid and oxalic acid was used as the separation object.TOA (in n-octanol) was used as the solvent. The extraction characteristics of single acid and two-acid solution were studied,and the influence of pH and the concentration of complexing agent on the distribution coefficients were measured. The suitable mathematic models were proposed to describe the relationship between TOA and carboxylic acid based on assumed extraction reaction in organic phase.

摘 要：以草酸和乙醛酸的稀溶液为分离对象，采用三辛胺为萃取反应剂、正辛醇为稀释剂，研究了单溶质、双溶质有机酸的萃取分离特性，测定了溶液pH值、萃取反应剂的浓度等因素对双溶质有机酸萃取的影响，提出了萃取的化学反应发生在有机相中的假定，建立了TOA萃取草酸的数学模型。

The diluent solution of glyoxylic acid and oxalic acid was used as the separation object. TOA (in n-octanol) was used as the solvent. The extraction characteristics of single acid and two-acid solution were studied, and the influence of pH arid the concentration of complexing agent on the distribution coefficients were measured. The suitable mathematic models were proposed to describe the relationship between TOA and carboxylic acid based on assumed extraction reaction in organic phase.

以草酸和乙醛酸的稀溶液为分离对象，采用三辛胺为萃取反应剂、正辛醇为稀释剂，研究了单溶质、双溶质有机酸的萃取分离特性，测定了溶液pH值、萃取反应剂的浓度等因素对双溶质有机酸萃取的影响，提出了萃取的化学反应发生在有机相中的假定，建立了TOA萃取草酸的数学模型。

Baseline separation of eight kinds of LCFAs (dodecanoic acid, tetradecanoic acid, palmitic acid, oleic acid, stearic acid, eicosanic acid, erudcic acid, behenic acid) was achieved within 2 min with high resolution performance.

建立了利用短的微径色谱柱直接测定食用油中未衍生化长链脂肪酸的快速气相色谱方法。C12~C22脂肪酸在2 min之内实现基线分离，定量标准曲线的相关系数大于0.988，最低检测限（S/N=3）为2.80~9.60 mg/L，回收率为

Octadecanoic acid、tetradecanoic acid、hexadecanoic acid、eicosanoic acid、9-octadecenoic acid、9,12,15-Octadecatrienoic acid、5,8,11,14-Eicosatetraenoic acid and 9,12-Octadecadienoic acid were increased dramatically in NASH group (P.05). Moreover,ω-6/ω-3 polyunsaturated fatty acids ratio is raised.

1脂肪酸分析结果提示NASH肝组织中正十二烷酸含量显著降低(P.05)，硬脂酸、十四烷酸、十六烷酸、二十烷酸、油酸、α-亚麻酸、花生四烯酸和亚油酸含量显著升高(P.05)，ω-6：ω-3多不饱和脂肪酸的比值升高。

The nutritional composition of six kinds of seed which belong to Labiatae plants have been studied,the results showed:the contents of fatty oil in the seeds was abundant and the contents of unsaturated fatty acid were rich,its unsaturated fatty acid in these kinds of seed oil reached 90% all.the main constituents of fatty acids were:α-Linoleni acid,linolic acid,oleic acid,arachidonic acid palmitic acid and stearic acid.

对六种唇形科植物种子营养成分研究的结果表明：种子含有丰富的脂肪油，其不饱和脂肪酸总量均在 90 %以上。种子油的主要成分为：α亚麻酸、亚油酸、油酸、花生烯酸、棕榈酸和硬脂酸等成分。

Tea seed oil fatty acids for oleic acid, linoleic acid, palmitic acid, stearic acid, linoleic acid, myristic acid and so on, and linoleic acid, linolenic acid is the maintenance of human skin, hair growth indispensable, able to prevent arteriosclerosis.

茶籽油的脂肪酸成分为油酸、亚油酸、棕榈酸、硬脂酸、亚麻油酸、豆蔻酸等，而亚油酸、亚麻油酸是维持人体皮肤、毛发的生长所不可缺少的，能够预防动脉硬化。

M treatment materials, and also tartaric acid and no maleic acid detected in G. v treatment materials. Inoculation also increased the content of organic acid secretion (increased by 19.80～56.87 mg/kg) of trifoliate root, and the application of AlPO4 greatly increased organic acid content (increased by 20.06～21.84 mg/kg); uninoculated plant root secreted a bit of organic acid; Mycorrhizal poncirus trifoliata seedlings excreted malic acid (42.87%), citric acid (39.22%) and oxalic acid (12.06%).

接种AM真菌的根系分泌的有机酸种类与对照有所不同，未接种处理枳分泌的有机酸有草酸、苹果酸、乳酸、乙酸、顺丁烯二酸和柠檬酸等6种，而接种G.m的则检测到草酸、酒石酸、苹果酸、乳酸、乙酸、柠檬酸、丁二酸等7种，G.v处理的检测到酒石酸，接种处理均未检测到顺丁烯二酸；接种丛枝菌根真菌增加了枳根系分泌有机酸的量比未接种处理增加19.80～56.87 mg/kg，且施用AlPO4后有机酸含量显著增加(增加20.06～21.84 mg/kg；未接种植株根系仅分泌少量有机酸；接种植株根系分泌的有机酸以苹果酸(42.87%)、柠檬酸(39.22%)和草酸(12.06%)为主。

As to the high polarity, high boiling point resultant—trimesic acid, the analysis methods of infrared spetrum, gas chromatography-mass spectroscopy, vapour-phase chromatography, acid number titration and so on are seperately used to characterize its property. Infrared spetrum and gas chromatography-mass spectroscopy are used to have a qualitative analysis on the resultant and are compared with the stand diagram. Sulfuric acid-methanol esterification and rapid esterification are used to prepare the trimesic acid trimethyl-ester and have a FID quantitative analysis. So that we make sure the purity of trimesic acid in the resultant and also we have an acid alkali titration on the resultant to get its acid number, in order to verify the purity of trimesic acid in the resultant.

对于高极性、高沸点的固体产物均苯三甲酸，分别采用红外光谱、气质联用、气相色谱、酸值滴定等分析手段进行了表征：利用红外光谱、气质联用的方法进行产物的定性分析，并与在同一仪器、同一条件下做出的标准谱图进行比对；采用硫酸-甲醇酯化法和快速酯化法制备出均苯三甲酸三甲酯，对其进行气相色谱FID定量分析，进而确定固体产物中均苯三甲酸的纯度；用酸碱滴定法确定固体产物的酸值，以对固体产物中均苯三甲酸的纯度进行验证。

The mycelial growth of Rhizoctonia solani was promoted by vanillic acid and syringic acid at levels of 0.1~1 mM/L, and it was inhibited remarkably by p-counaric acid of over 1mM/L and modestly by ferulic acid. The radial extent of mycelia of Fusarium solani was increased significantly by ferulic acid of 0.1~1 mM/L and limitedly by p-coumaric acid. vanillic acid had paradoxcial effects on the growth, positively at low levels and negtively at high levels, on which Syringic acid had a slight effect.

试验结果显示：浓度为0.1~1mM/L的丁香酸对西洋参立枯丝核菌菌丝生长具有促进作用，香草酸也有一定的促进作用，但不呈浓度效应，浓度在1mM/L以上的香豆酸对其有显著的抑制作用，阿魏酸也有一定抑制作用；对于西洋参根腐菌，阿魏酸对其生长有明显促进作用，香豆酸也有一定促进作用，香草酸表现为低浓度促进，高浓度抑制作用，0.1~1mM/L丁香酸对其生长基本无影响。

Alternatively, the con- trollers can use the synchronous rectifier itself or loss- less inductor current-sensing methods to provide overload protection with lower power dissipation.

另外，康威特罗勒斯可以使用同步整流器本身或亏损减少电感电流检测方法，以提供低功耗过载保护。

Mr. Dauber's other Schatz hangs in his home movie studio.

多伯把沙兹的另一件作品挂在家里的电影室。