查询词典 diazotization

METHODS:This compound was synthesize by steps of ammonolysis,hydrogenize,diazotization and coupling from 4-nitrobenzoyl chloride.

以对-硝基苯甲酰氯为原料，经氨解、氢化、重氮化及偶合四步反应得到了巴柳氮。

The 3-chloro-4-trifluoromethoxy benzonitrile was synthesized from 3-chloro-4-trifluorome- thoxy aniline by diazotization, formaldoximation ,hydrolysis and cyanation.

以3-氯-4-三氟甲氧基苯胺为原料，经重氮化、甲醛肟化、水解和腈化反应得到纯度≥99。

In the dyestuff production process, such as AZO pigments of diazotization, it controls temperature technical by adding ice, which can be effective to control the diazonium salt decomposition in coupling reaction.

在颜料生产过程中，例如偶氮颜料的重氮化反应，偶合反应中，采用加冰控温工艺，可有效控制重氮盐的分解。

The paper discloses a process for diazotization fluorination of aromatic primary amines utilizing sodium nitrite and anhydrous hydrofluoride to produce the corresponding diazonium fluoride which is decomposed, usually by heat, to make the desired fluoroaromatics .

本文通过重氮化工艺路线的改进，在液态氟化氢中进行重氮化和重氮盐的热分解，提高了芳香族氟化物的收率，并且使重氮化反应工艺能应用于工业化生产。

Diazonium salt which was formed by reaction of diazotization of eldest aromatic amine then coupling with N-(1-naphthyl)-ethylenediamine dihydrochloride,in NH_3·H_2O-NH_4Cl solution showed a sensitive polarographic wave at peak potential of 0.58vs,SCE.

本文报道了芳香族伯胺的重氮－偶氮化反应所生成的偶氮化合物在NH＿3·N＿2O－NH＿4Cl底液中，在单扫描极谱上，峰电位－0.58V

Objective To study resonance light scattering spectra of diazotization- coupling reaction and establish a new method for the determination of trace nitrite.

目的 研究重氮化－偶联反应的共振散射光谱并应用于亚硝酸根的测定。

After the diazotization, a mixture of 2,3,5-trichloropyridine and 3, 5- dichloropyridine-2-ketone was got as a result of Sandmeyer reaction.

收率达84.7%。接着，我们以制得的2，3，5-三氯吡啶为合成2，3-二氟-5-氯吡啶的原料，用NMP为溶剂，加入KF和CsF的混合氟化剂，高温下反应合成了2，3-二氟-5-氯吡啶。

High performance liquid chromatography and Griess diazotization reaction were employed to determine the levels of Hcy and NO in the plasma and the correlation between Hcy and NO was analyzed.

分别采用高效液相色谱法和Griess重氮化反应法检测62例急性脑梗死患者(起病24 h内)血浆Hcy及NO水平，分析两者的相关性及其与急性脑梗死的关系。

Methods 62 patients with acute cerebral infarction (within 24 hours) were enrolled. High performance liquid chromatography and Griess diazotization reaction were employed to determine the levels of Hcy and NO in the plasma and the correlation between Hcy and NO was analyzed.

分别采用高效液相色谱法和Griess重氮化反应法检测62例急性脑梗死患者(起病24 h内)血浆Hcy及NO水平，分析两者的相关性及其与急性脑梗死的关系。

Ultraviolet absorbent UV-326 was synthesized by means of diazotization, coupling and reduction, with rongalite as reduction agent.

以保险粉作还原剂，通过重氮化、偶合、还原反应合成了紫外线吸收剂UV-326。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。