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Influence of the concentration of Cr in the leachate and quantity of Pb(CH3COO)2 of Pb(NO3)2 on the reaction of synthesizing yellow chrome was also studied. Finally, according to the criterion and standard method in GB3184-82, some yellow chrome synthesized in the experiments was sampled and the concentration of PbCrO4 in these samples was determined. The following conclusion can be drawn from these experiments.

根据中华人民共和国国家标准GB3184-82中的规定铅铬黄颜料的技术质量指标和检测方法,测定了铬黄样品中铬酸铅含量的厂迄回【、矾士牢位论父泅仰yW盯皿'S川mS达标情况,结论如下:门)反应中重铬酸盐的浓度并不需要达到前人所提出的150~2509·L'的范围,在一定条件下低于此浓度时对铬黄生成反应并无不利影响。

Compounded functional drinks with unique flavour, rich nutrients and healthcare effects were made from carrot, chufa and arrowroot by the extraction of juices and the modern beverage processing technology, based upon the theories of nutrition and traditional Chinese medicine The optimal formula and technological conditions were determined through orthogonal test

以现代营养知识和传统的中医药理论为依据,研究以胡萝卜、荸荠、粉葛为原料,经现代饮料加工技术,提取其汁,采用正交试验,研制出最佳生产配方和最佳工艺条件,生产出口味独特营养丰富具有保健作用的功能性复合饮

The number of Chaetognatha was higher in Bering Sea than in Chukchi Sea. The density of dominant species determined the total Chaetognatha abundance and it was higher in south than in north.

研究表明:( 1 )两区共记录毛颚类 7种,可分为 3个类群,在数量上,白令海的个体数明显高于楚科奇海;其平面分布的状况主要由优势种所左右,并且都呈现出南高北低的分布格局。

The content of sulphate reducing bacteriaof the 35 sediment samples was determined by using MPN technique in the survey areas of Bering Sea and Chukchi Sea.

用 MPN法测定了取自白令海和楚科奇海 35个沉积物样品中的硫酸盐还原菌含量。

METHODS: The acute pancreatitis model was induced by retrograde injection of 50 g/L sodium taurocholate into the bili-pancreatic duct in SD rats. Forty-eight mas-culinity SD rats were randomly divided into 2 groups: the sodium taurocholate group and the operational control group. The serum amylase level and the histol-ogical pathologic changes of pancreas were measured at different time point in each group. The expression of pancreatic CINC protein and mRNA were determined by immunohistochemistry and semi-quantitative reve-rse transcriptase polymerase chain reaction, respectively.

采用向胆胰管逆行注射50 g/L牛磺胆酸钠建立大鼠SAP模型, 48只♂SD大鼠随机分为手术对照组和SAP组,分别检测各组不同时间点血清淀粉酶和胰腺组织病理学改变,用免疫组织化学法和半定量逆转录聚合酶链反应法检测胰腺组织中CINC蛋白和CINC mRNA表达的变化情况。

The thermodynamic parameters in the separation of enantiomers of amino acid derivatives and diastereomers of cinchona alkaloids were calculated and the dissociation constants of cinchonine and cinchonidine on the cinchonine imprinted monolithic disk were determined by frontal analysis.

计算了氨基酸衍生物对映体以及辛可纳非对映异构体分离过程的热力学参数并利用前沿色谱法测定了辛可宁和辛可尼丁在盘状分子印迹整体柱上的离解平衡常数。

It is demonstrated that the chiral quaternary ammonium salts catalysts exhibit promising catalytic properties for the substrate. Part III: The synthesis and the characterizing of the macroporous aminomethyl resin-supported cinchona alkaloid complexes and the study on its catalytic properties The part consists of two subsections. the macroporous aminomethyl resin -supported cinchona alkaloid complexes were synthesized by the stuff (cinchonine, quinine and macroporous aminomethyl resin). Their structures were characterized by means of elemental analysis, XPS, TG/DTA; the chiral polymer-supported complexes were first used as catalysts for the reduction of ketones. Their catalytic properties for the reduction processes were investigated. The comparison of the products e.e., the conversion of the substrate among different reduction processes was employed with determined by HPLC. The effects of the time, the temperature, the ratio of catalyst to substrate, reaction solvent as well as the recycle times were also discussed.

第三章聚-4-氨甲基苯乙烯负载金鸡纳碱金属络合物的合成与表征及其不对称催化性能研究本章分为两节,以辛可宁和奎宁及聚-4-氨甲基苯乙烯为原料,合成了4种聚-4-氨甲基苯乙烯负载金鸡纳碱络合物催化剂,并对它们的结构用元素分析、X-射线光电子能谱、TG/DTA等几种测试手段进行了表征;首次将所合成的手性高分子负载的金属络合物用于催化芳香酮不对称还原反应,详细研究了所得的手性高分子负载的金属络合物对不同底物的催化性能,用HPLC等分析手段定量检测了还原过程的底物转化率及其产物对映异构体选择性,并考察了反应时间、反应温度、催化剂和底物投料比、反应溶剂和循环次数对催化性能的影响。

The excess molar volumes of {1,8- cineole +CCl 4,+CHCl 3} were determined as a function of mole fraction x using a vibrating-tube densimeter at the temperatures 298 15 and 308 15K All mixtures exhibit negative values over the entire composition range at both temperatures.

在 2 98 15K和 30 8 15K下用振动管密度计在全浓度范围内测量了桉叶油素分别与四氯化碳和三氯甲烷构成的二元系的过量摩尔体积。这 2个二元系的过量摩尔体积均为负值,且桉叶油素与氯仿的过量体积显著大于桉叶油素与四氯化碳的过量体积

Chinese traditional herbal drugs for relieving away heat and toxic were treated with cineration,and the residues were dissolved by HNO_3.Eleven trace elements including,calcium,magnesium,manganese,copper,iron,zinc,cadmium,lead,cobalt,nickel and chromium in twenty sample solutions were determined by flame atomic absorption spectrometry.

采用灰化法处理样品,HNO3溶解灰化残渣,用火焰原子吸收光谱法测定了射干、白头翁、山豆根、鱼腥草、连翘、大青叶、车前草、野菊花、金银花、莲子芯、蒲公英、板兰根等20种中草药中的Ca,Mg,Mn,Cu,Fe,Zn,Cd,Pb,Co,Ni和Cr共11种微量元素。

The device parameter as well as resonance frequency,mechanical quality factor and work band width were determined by the equiv- alent circuit input impedance admittance circle diagram .

分析压电式超声波换能器的等效电路,并由等效电路输入阻抗的导纳圆图确定了换能器的元器件参数以及谐振频率、机械品质因数和工作带宽等特征参量。

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