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We also study characteristic index and its determination of complex flocculant, put forward the new concept of total basification degree and present the determined method of B〓.In this paper, the author studied and improved on the Ferron Timed Complex Colorimetry, put forward the determination principle and determined method of the improved Ferron Timed Complex Colorimetry, and determined successfully the iron and aluminum hydrolysis-polymerized species of FMA complex flocculation at the same time.

研究了复合絮凝剂的特性指标及其分析测定方法、复合絮凝剂的絮凝特性评价方法,提出了总碱化度作为复合絮凝剂特性指标的新概念,并给出了分析测定方法;研究改进了Ferron逐时配合比色法,提出了复合体系中铁铝水解聚合形态同时测定的测定原理及方法,成功地将其用于FMA中铁铝水解聚合形态的同时测定。

Abstracts The average molar weight of Sulfated polysaccharide 911 was determined by the content of its sulfate group, which was determined by the oxygen flask method at first in this paper, then the content of Sulfated polysaccharide 911 was determined by the decarboxylation method.

摘 要 该文采用氧瓶燃烧法测定了硫酸多糖911的硫含量,根据所测硫含量确定了硫酸多糖911的平均单体式量,然后在此基础上应用脱羧法对硫酸多糖911样品的含量进行了测定。

Urinary microalbumin was determined with immunoturbidimetry, urinary NacetylD-glucosaminidase,βDgalactosidase(GAL and glycyl proline dipeptidyl aminopeptidase were determined with rate, urinary creatinine was determined with Jaffe rate.

对127例糖尿病患者,采用免疫透射比浊法检测尿mA,速率法检测N乙酰βD氨基葡萄糖苷酶、βD半乳糖苷酶、甘氨酰脯氨酸二肽氨基肽酶,Jaffe速率法测尿肌酐。

Chromic trioxide and chromium hemitrioxide are determined with iodometry, the coefficient of variation of chromic trioxide is 0.056%, and the recovery of marked compound is 99.82-99.83%; the coefficient of variation of chromium hemitrioxide is 1.45%,and the recovery of marked compound is 98.55-99.26%; iron is determined by complexometric titration, the coefficient of variation of iron is 1.73%, and the recovery of marked compound is 99.12-99.23%;sulfate is determined by complexometric titration, the coefficient of variation of sulphate is 0.16%, and the recovery of marked compound is

Analysis Of The Chromium Electroplating Wastewater By Oxidation-reduction And Complexometric Titration-化学工程与工艺-本文采用氧化还原滴定法与络合滴定法对镀六价铬的废水中铬酸酐,三氧化二铬,铁和硫酸根的含量进行了测定:铬酸酐和三氧化二铬用碘量法测定,铬酸酐的变异系数为0.056%,加标回收率为99.82-99.83%,三氧化二铬的变异系数为1.45%,加标回收率为98.55-99.26%;铁用络合滴定法测定,其变异系数为1.73%,加标回收率为99.12-99.23%;硫酸根用络合返滴定法测定,其变异系数为0.16%,加标回收率为

Results showed:(1) The airway responsiveness of smoke control group was higher than that of normal control group, the airway responsiveness of smoke + exercise group was lower than that of smoke control group;(2) Plasma level of cortisol determined immediately after exercise was higher than that determined before exercise, no significant difference occurs between that determined next day morning after all exercise finished in contrast to that determined before exercise;(3) HE staining showed, there was severe chronic pulmonary inflammatory response in smoke control group, which was reduced in the smoke + exercise group;(4) chronic cigarette smoke downregulated the protein and mRNA expression of BKca in smooth muscles of bronchi and bronchioli, exercise increased the mRNA expression of BKca;(5) chronic cigarette smoke downregulated the protein and mRNA expression of Kv1. 5 in smooth muscles of bronchi and bronchioli, exercise increased both the protein and mRNA expression of Kv1. 5 in contrast to smoke control group in bronchioli and did not effect the expression of Kv1. 5 in bronchi;(6) chronic cigarette smoke induced upregulation of FIZZ1/RELMα in bronchial smooth muscle cells, exercise decreased these effect.

结果:(1)吸烟对照组的气道反应性明显增高,吸烟加运动应激可明显降低大鼠的气道反应性;(2)吸烟运动组运动后血浆皮质醇浓度明显高于运动前,但全部运动结束后次日晨测定的血浆皮质醇浓度与运动前无明显差异;(3)HE染色显示,吸烟对照组肺组织出现明显的慢性炎症反应,吸烟加运动应激组比吸烟对照组炎症反应轻;(4)慢性吸烟可降低大鼠大气道和小气道BKca mRNA和蛋白表达,而吸烟加运动应激可使BKca mRNA表达上调,但对小气道的蛋白表达无影响;(5)慢性吸烟可降低大鼠大气道和小气道Kv1.5蛋白和mRNA表达,在小气道吸烟加运动应激可减轻这种作用,大气道则无作用;(6)吸烟使支气管平滑肌的FIZZ1/RELMα蛋白表达明显增强,而吸烟加运动组的RELMα蛋白及mRNA均明显减弱。

With the observation of the outward appearances, it can be known roughly that if the sample was added with adulterations. Since the beeswax dissolves in the benzene but the adulterations, such as gypsum, starch and so on do not, these can be determined. By the verification of acid value and alcohol dissolve ability, the acid or non acid added can be determined. By the change of saponification value, the ester or non ester added can be determined. By the carbonification degree in the concentrated sulphuric acid, the mineral wax, such as paraffin wax added can be determined.

通过样品外观的观察初步定性是否掺有杂质;利用纯蜂蜡在苯中溶解,而掺入的石膏、面粉和淀粉等杂质在苯中不溶而定量鉴定这类杂质;由酸值变化和乙醇溶解物的量,测定掺入的硬脂酸等酸性物质或其它的非酸性物质;由皂化值变化,定量测定掺入的动物脂等酯类物质或其它的非酯类物质;根据蜂蜡中的烃类在浓硫酸中可被炭化,加入的石蜡等矿物蜡不被炭化来测定此类掺杂物。

After 24 hours, all rats were anesthetized again and their left common carotid arteries were cannulated to facilitate blood withdrawal for serum sample. The contents of tumor necrosis factor-a and interleukin-6 (IL-6) in serum were determined before and after experiment by ELISA; the activity of superoxide dismutase and content of malondialdehyde were determined by xanthinoxidanse method and modified TBA microdetermination. The content of NO2(superscript -)/NO3(superscript -), and activity of nitric oxide synthase and inducible NOS were determined by nitrate reductase method, and chemical chromogenic reaction, respectively; the immunoglobulin G, IgA, IgM and complement 3 (C3) and C4 were determined by immunoprecipitation method before and after experiment.

实验评估:手术创伤后24h进行采用酶联免疫吸附法测定实验前后血清肿瘤坏死因子α、白细胞介素6含量;应用黄嘌呤氧化酶法测定超氧化物歧化酶活性、改良TBA微量法测定丙二醛水平;以硝酸还原酶法、化学显色法分别检测NO2/NO3浓度及一氧化氮合酶、诱导型一氧化氮合酶活胜;以免疫比浊法经全自动生化分析仪检测血清免疫球蛋白IgG、IgM、IgA及补体C3、C4含量。

The compositions of complexes were determined as, by chemical and elemental analyses, Mn2CI2, Mn2Cl2, Cu2Cl2-2H2O, Cu(NO3)2-H2O, Cu(CH3COO)2, Zn2Cl2, Zn2(NO3)2-4H2O,ZnSO4 and Zn4(NO3)2, respectively. These complexes were characterized by IR,'H NMR and XPS. The crystal structures of these complexes were determined by single crystal X-ray diffraction techniques. The thermstability of the complexes was investigated by TG-DTG and the processes of their thermal decomposition were speculated. The constant-volume combustion energies of complexes, cU, were determined by a precision rotating bomb calorimeter at 298.15 K. Their standard enthalpies of formation, Hm, were calculated respectively. Finally, their biological activity was researched after the bactericidal activity was determined by selection of 1-2 bacteria.

通过化学分析、元素分析确定化合物分子组成分别为Mn_2Cl_2,Mn_2Cl_2,Cu_2Cl_2·2H_2O,Cu(NO_3)_2·H_2O,Cu(CH_3COO)_2,Zn_2Cl_2,Zn_2(NO_3)_2·4H_2O,ZnSO_4和Zn_4(NO_3)_2;借助IR、~1H NMR和XPS对化合物的键型特征进行了表征,运用X-射线单晶衍射分析法测定了个别化合物的晶体结构;以TG-DTG技术研究了化合物的热稳定性,阐明了它们的热分解机理;用精密转动弹热量计测定了化合物在298.15 K的恒容燃烧能,并计算了它们的标准燃烧焓和标准生成焓;选取1~2种病菌,初步测定了化合物的杀菌活性,进而研究了它们的生物活性。

The expression of one-dimensional mathematical model of vertical migration of ammonia in the CRI system is:The parameters in the CRI model are determined as following: the retardarce coefficient is determined by static isothermal absorption experiment, the velocity of sewage travel through the soil column is determined by permeability test, the vertical dispersion coefficient is determined by test the electric conductivity of tracer in the dispersion experiment, the rate of nitrification and denitrification is determined by test of Baps technology.

依据单一氨氮、硝氮配水条件下的试验结果,引入多孔介质的溶质运移理论及对流-弥散方程,考虑NH4+-N在CRI系统中的运移受到对流和水动力弥散作用的影响,并吸附-解吸、硝化与反硝化3个过程,首次将配水流经CRI土柱的孔隙水流速方程与CRI土柱内发生的、以氧为约束条件的硝化、反硝化过程联系起来,建立了CRI系统一维垂向氨氮运移转化数学模型,表达式为:研究分别通过静态等温吸附实验率定了模型方程中的阻滞系数、通过渗滤试验测定了土柱中的孔隙水流速、通过测定弥散试验中示踪剂的电导率确定了纵向弥散系数、通过气压过程分离技术测定了土柱中的总硝化与反硝化反应速率常数,最后通过测定土柱沿程氧化-还原电位的方法分析氨氮在CRI系统中的运移转化机理。

Esults LVSV and RVSV determined by RT-3DE were (15.90±10.62) ml and (12.42±4.69) ml respectively, which were shown good correlation with those determined by MRI [(16.56±10.64)ml and (13.96±7.96) ml]. The r value was 0.98, and 0.75, respectively. LVSV and RVEV determined by RT-3DE were (12.67±10.10) ml and (11.83±12.02) ml respectively, which were well correlated with MASE (8.17±1.92)mm and TASE (11.04±1.06) mm determined with ME. The r value was 0.86 and 0.88 respectively.

T-3DE测定左室每搏量(12.67±10.10)ml和ME测定二尖瓣瓣环收缩期平均位移(8.17±1.92)mm之间的相关性显著,相关系数r=0.86(P.001);RT-3DE测右室每搏量(11.83±12.02)ml和ME测定三尖瓣瓣环收缩期位移(11.04±3.06)mm两者亦存在显著正相关,相关系数r=0.88(P.001)。

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