查询词典 cyclohexanone

The vapor phase Beckmann rearrangement of cyclohexanone oximeover RBS-1 catalyst was carried out in a continuous flow fixed bed reactor under atmosphere pressure.

在常压连续流动固定床反应装置上，考察了反应温度、环己酮肟质量空速、溶剂种类、环己酮肟浓度、载气流量、水的质量分数等反应条件或反应氛围对环己酮肟气相Beckmann 重排反应的影响。

It was found that the Beckmann rearrangement of cyclohexanone oxime could be performed smoothly in the catalytic media consisting of room temperature ionic liquid and acidic phosphorated compounds, and excellent conversion and selectivity were achieved under mild conditions without any additional organic solvents.

发现酸性含磷化合物，如五氯化磷等在离子液体中可以高效地实现环己酮肟重排制己内酰胺，具有不需另加有机溶剂，选择性高等优点。

The Beckmann rearrangement of cyclohexanone oxime, phosphorus pentoxide (P_2O_5) and dimethyl formamide raction system into caprolactam was studied.

研究了以环己酮肟、五氧化二磷(P_2O_5)、二甲基甲酰胺组成的反应体系进行Beckmann重排制备己内酰胺工艺，考察了不同溶剂、催化剂用量、温度、浓度及水分含量对重排反应的影响。

The Beckmann rearrangement of cyclohexanone oxime was effectively realized to prepare e-caprolactam by using phosphorous trichloride (PCl3) as catalyst in a two-phase system composed of 1-n-butyl-3- methylimidazolium tetrafluoroborate ([BF4]) ionic liquids and toluene.

在1丁基3甲基咪唑四氟硼酸盐([BF4])与甲苯组成的两相体系中，以三氯化磷(PCl3)为催化剂，实现了由环己酮肟制备己内酰胺的液相贝克曼重排反应，两相体系有利于反应控制和体系取热。

By one-pot method,with p-toluenesulfonic acid as catalyst,trimethyl orthoformate and cyclohexanone reacted in isopropanol to form 1,1-dimethoxycyclohexane,which,without separation,reacted furthur with isopropanol to form the title compound by distilling off the low-boiling product.

用一锅法，以对甲苯磺酸为催化剂，在异丙醇中原甲酸三甲酯与环己酮反应，其产物不经分离直接与异丙醇交换，得到1，1-二异丙氧基环己烷。

Acetone, cyclohexanone, formaldehyde and ethylene diamine were adopted to synthetise HLZ corrosion inhibitor by means of Mannich reaction.Then LZ-620 salts corrosion inhibitor was synthetised on HLZ condensating chloroacetic acid.

针对盐类腐蚀采用丙酮、环酮A、甲醛、乙二胺通过曼尼希反应生成缓蚀剂后再与氯乙酸缩合生成盐类缓蚀剂(LZ-620)。

Sythesis and application of chlorostyrene-DVB strongly acidic cation exchange resin ;2. For this study,a series of poly( p -amino styrenes) with various amounts of supported hydrogen chloride,and a series of strongly acidic cation exchange resin s with various exchange capacity were synthesized,and their catalytic property for ketalization of cyclohexanone and glycol were investigated.

通过测定固载了不同量的氯化氢的聚和不同交换量的强酸性阳离子交换树脂催化的环己酮与乙二醇的缩酮化反应缩酮的收率，研究了聚合物固体酸催化剂的疏水性对其催化缩酮化反应性能的影响；发现在一定范围内增加催化剂的疏水性，可提高缩酮化反应的收率。

The original silk screen printing solvents: Pad open oil, silk screening for open water, 783 slow do water, do water 719 Medium .718 Net water washing, anti-white, wipe the word water, to sewage, PP treatment of water, white oil, a strong day and that water, cyclohexanone, thin water transfer printing.

各原装移印丝印溶剂：移印开油水，丝印开油水，783慢干水，719中干水。718洗网水，防白水，抹字水，去污水，PP处理水，白电油，强力天那水，环已酮，移印调薄水。

Production of epsilon-glycolylnium is carried out by Beckman rearrangement reacting for cyclohexanone-oxime under the existence of solvent to obtain epsilon-glycolylnium contained mixture, crystalline separating for the mixture to obtain crude epsilon-glycolylnium crystal, dissolving by arene, extracting by water, adsorbing by resin hydrogenation catalyzing to obtain the final product. The value of potassium permanganate is less than 5, extinction value is less 0.05, volatile alkali is less than 0.5meq/kg and alkalinity is less than 0.05meq/kg.

本发明涉及一种ε―己内酰胺制备方法，其特征为：在溶剂存在下，环己酮肟经贝克曼重排反应，得到含有ε―己内酰胺的混合物，该混合物结晶分离后，得到粗ε―己内酰胺晶体用芳烃溶解，然后用水萃取，再经树脂吸附、催化加氢后，得到99.995％以上的高纯度的ε―己内酰胺，其质量指标为高锰酸钾值小于5，消光值小于0.05，挥发性碱小于0.5meq/kg，碱度小于0.05meq/kg。

Moreover, the determination of the content of dissociate cyclohexanone-omine in the mixture of rearrangement process in caprolactam production was also studied. The rearrangement mixture is a complicated and difficult system to directly analyze, containing great volume of sulfuric acid and some amount of sulphur trioxide, with higher viscosity and strong corrosivity.

此外本论文还对己内酰胺生产过程中的重排混合物中游离环己酮肟含量测定进行了研究，重排混合物是一个很特殊、难以直接分析的体系，含大量硫酸和少量三氧化硫，粘度大，腐蚀性强，且杂质种类较多。

On the other hand, the more important thing is because the urban housing is a kind of heterogeneity products.

另一方面，更重要的是由于城市住房是一种异质性产品。

Climate histogram is the fall that collects place measure calm value, cent serves as cross axle for a few equal interval, the area that the frequency that the value appears according to place is accumulated and becomes will be determined inside each interval, discharge the graph that rise with post, also be called histogram.

气候直方图是将所收集的降水量测定值，分为几个相等的区间作为横轴，并将各区间内所测定值依所出现的次数累积而成的面积，用柱子排起来的图形，也叫做柱状图。