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The complexes were characterized with variable temperature magnetic susceptibility (4-300 K). The exchange integral J =-4.39 cm-1 for [CuCo(NO2-Phen)2] and -3.59cm-1 for [CuCo(NO2-Phen)2]. A weak antiferromagnetic superexchange interaction operates between the metal ions.

测定了配合物(4-300K)的变温磁化率，并用最小二乘法和自旋Hamiltonian算符，H=2JS1.S2-DSzl导出的磁方程拟合，求得交换参数为J=-4.39和-3.59cm^-^1，表明两个Cu-Co双核配合物中有弱的反铁磁性超交换相互作用。

In 0~60 cm soil profile,the concentrations of Hg and Cu exceeded the reference value of s...

此外，该文提出的土壤元素含量变化速率的概念，可以直观反映土壤中某一元素浓度的增加或减少的快慢，对预测土壤中元素浓度的变化趋势有参考价值。

In a climatically controlled chamber (28±1℃, L16:D8), E. splendens was planted in pots containing mixed vermiculite and perlite without Cu. At about 220 d after seeding, plants (around 65 cm in height) were used to collect their volatile using SPME. Eleven chemicals were identified using GC-MS, p-pinene, D-limonene, elsholtzia ketone, dehydro elsholtzia ketone,γ-elemene, humulene, caryophyllene, a-caryophyllene, and three sesquiterpenes. The most abundant volatiles were caryophyllene and y-elemene, followed by humulene and a-caryophyllene.

室内在不含Cu的蛭石和珍珠岩混合基质中种植海州香薷，用固相微萃取法收集健康植株(株龄220余天，株高65cm左右)的挥发物，采用GC-MS法识别出11种主要组分，从中鉴定出β-蒎烯，D-柠檬烯，香薷酮，脱氢香薷酮，γ-榄香烯，蛇麻烯，石竹烯，α-石竹烯(α-caryophyllene)，以及三种倍半萜类化合物，其中石竹烯和γ-榄香烯含量高，其次为蛇麻烯和α-石竹烯。

Results demonstrate that the Cu(superscript 2+) can be concentrated effectively under the following condition: exchange column internal diameter 0.8 cm and 15 cm high, the dosage of spiral algae 2 g and pH value 6, the flow rate of the dry food leach solution 10 mL/min, elute with 0.6 mol/L HCl at a flow-rate of 6 mL/min.

结果表明，在交换柱内径为0.8 cm、柱高为15 cm、螺旋藻用量为2 g、pH值6的条件下，干制品浸出液流速为10 mL/min时，用0.6 mol/L HCl以6 mL/min的速度洗脱，可对Cu(上标 2+)进行高效富集。

Methods: The following five sites in the city were selected as monitoring spots, namely, the First Smelter of Tongling Nonferrous Metal Group, the second Smelter of Tongling Nonferrous Metal Group, the Changjiang High-speed Passageway, Fenghuangshan Copper Mine district, residential area, respectively. The moss species Hypnum plumaeform e collected from Huangshan mountain was placed in nylon bag of 15.5 cm×5.5 cm in size and 2.0 mm×2.0 mm in meshes, with each bag having 3 g moss and then sealed by a nylon wire. Moss bags were suspended in five urban exposure sites and then gathered after two months. The content of heavy metal in the tested moss were analysed by atomic absorption spectroscopy.

选取铜陵市的铜陵一冶、铜陵二冶、长江快速通道、凤凰山铜矿区和居民区5处监测点，以采自黄山的大灰藓为材料，用尼龙筛网（网眼2.0 mm×2.0 mm）做成15.5 cm×5.5 cm的矩形袋子，每袋放3 g，2007年3月22日悬挂于各监测点，完全暴露在空气中，2个月后取回，采用原子吸收光谱法对样品中Cu、Cd、Cr、Pb、Zn 等重金属元素含量进行测定。

In combination of oxygen nonstoichiometry data determined using the iodometric titration, the oxygen chemical diffusion coefficient D〓 for YBa〓Cu〓O〓 is calculated. D〓 takes a value of 7. 8×10〓 at 650℃ and 2. 0×l0〓cm〓s〓 at 800℃, and the associated apparent activation energy is 51±0.9 kJ·mol〓.

根据Fick第一定律，结合氧渗透率数据及氧非化学计量数据，可计算出YBa〓Cu〓O〓的氧化学扩散系数D〓在650～800℃，D〓为7.8×10〓～2.0×10〓cm〓，D〓的表观活化能为51±〓0.9 kJ·mol〓。

The apparent density increased with the increase of Ag~+ complexing reagent A concentration, loadage, silver content and granularity, it firstly increased and then decreased with the increase of Cu/Ag ration, and it had no relation to other factors, and it was 1.3-1.4g/cm~3 usually.

3粉体的松装密度随Ag~+络合剂A浓度、装载量、含银量、粉体粒度的增加逐渐变大，随Cu/Ag比的增加先变大后变小，其它因素对松装密度都无明显的影响，均保持在1.3-1.4g/cm~3。

The study of crystal structure indicates that the complexes belongs to tetragonal,14(1)/a, a=b=27.047(5) A, c=14.103(3) A, a=b=y =90,V=10317(4)A3, Z=16, Dc=1.071g/cm3, F(000)=3408, R,=0.1395, R2=0.1766 and every unit of the tetranuclear complexes is four-coordinated to tridentate ligand and nitrogen atom in pyrazolone from other ligand. The complexes is slightly deformed square-planar geometry.

晶体结构研究表明，该配合物为四方晶系，空间群I4(1)/a，a=b=27.047(5)，c=14.103(3)，α=β=γ=90°，V=10317(4)，Z=16，Dc=1.071g/cm~3，F(000)=3408，R_1=0.1395，ωR_2=0.1766，其结构单元是由一个三齿配体中的ONO和另一个配体吡唑啉酮环二位上的N配位后形成略微畸变的平面四边形构型，其中Cu的配位数为4。

The energy spectra of hot electrons have been measured using the magnetic spectrometers, fitted with the LiF thermoluminescent dosimeter which were calibrated using Cs~(137)γ-ray sources, in the interaction of a 130 mJ, 60 fs, 800 nm, 1∶10~(-6), 7.0×10~(17) W·cm~(-2) P-polarized laser incidence on Cu foil target at an angle of 45° with respect to the target normal without any prepulse.

在激光能量130mJ，脉宽60fs，波长800nm，对比度1∶10-6，激光与靶法线成45°夹角， P偏振，靶面激光峰值功率密度约为7.0×1017W·cm-2，无预脉冲的条件下，采用电子谱仪与经γ标准源标定的LiF热释光探测器相配合，测量了飞秒激光薄膜靶相互作用中产生的超热电子能谱。

Transport behavior of various speciation and each chemical form of heavy metals in soil from the different field around Cu-Ni mining area in Jinchang were assessed. The results show that the mean transfer coefficient of acid-soluble/exchangeable, reducible, oxidisable and residual fraction is 0.13, 0.51, 0.30 and 0.54, respectively.

对金昌矿区不同区域土壤5~20 cm层中重金属各化学形态及活性态的迁移行为进行了研究，结果表明：土壤中重金属不同化学形态迁移率不同，弱酸提取态、可还原态、可氧化态和残渣态平均迁移率分别为0.13、0.51、0.30和0.54。

Neither the killing of Mr Zarqawi nor any breakthrough on the political front will stop the insurgency and the fratricidal murders in their tracks.

在对危险的南部地区访问时，他斥责什叶派民兵领导人对中央集权的挑衅行为。

In fact,I've got him on the satellite mobile right now.

实际上 我们已接通卫星可视电话了