查询词典 crystallinity

Treatment under mild condition with solvent of lower polarity was in favor of keeping the molecular structure and properties such as water-solubility, gelatination, etc. Acetyl groups were partially eliminated when purified by Pb2 method, leading to increased crystallinity and glass temperature, which resulted in losts of water-solubility and gelatinability. Owing to the slight oxidative degradation with H2O2 method, the changes of chain size and some functional groups of KGM molecule led to decrease of viscosity and excessive swelling rate.

采用温和条件及低极性溶剂有利於保持KGM本身的分子结构以及水溶性、凝胶性等性能；而Pb2法由於部分脱去了KGM的乙酰基，导致结晶度变大，玻璃化温度升高，最终失去水溶性和凝胶性；H2O2法则由於对KGM造成了氧化降解，也改变了分子链的大小以及部分基团，从而导致粘度降低以及溶涨速度较快。

Degradation test in vitro was carried out in phosphate buffer solution (0.1M, pH7. 4) at 37 ℃. The buffer solution was changed daily. Degradation test in vivo was implanted the sample to subdermal in adult ICH rat in the scapular area lateral to the dorsal midline. At suitable time the samples were recovered. Molecular weight changes in surface layer and bulk of polymer sample were measured by GPC and weight loss was determined gravimetrically. It was found that the degradation behavior can be regulated by changing the composition of copolymers. The critical compositions from surface to bulk degradation behavior for PGCA, PLCA, PLMCA, PLDCA systems were 15-20, 20-30, 30- 40, 40 of mol percent GA or LA unit in copolymers, respectively. The degradation behavior of PGCA, PLCA, PLMCA, PLDCA systems were compared and analysed. Some factors influencing the degradation character, such as copolymer composition, hydrophobicity, crystallinity and enzyme affect etc. played important role.

体外实验中材料降解环境为37℃，0.1M，pH7.4磷酸缓冲溶液，每天换液，定期取样；体内实验中将聚合物试样埋置于ICH小白鼠背部肩胛骨皮下部位，定期处死小鼠，取样，将体内体外样品进行重量损失及试样内外层分子量变化测定，分析各聚合物试样降解行为特性，实验结果证明，改变共聚物组成，可以调节各聚合体系降解行为特性，对PGCA，PLCA，PLMCA，PLDCA共聚体系，交酯摩尔百分含量15-20％，20-30％，30-40％，40％分别为各体系内降解行为特性由表面降解型向本体降解型过渡的临界转折点，交酯含量较低的聚合物不同程度地表现表面降解行为特性，论文对各共聚体系体内外降解行为作了分析对照，例如共聚物组成对材料降解速度与降解行为的影响；生物体内酶对降解行为的影响；材料亲疏水性，聚合物链段结晶行为及碳酸酯结构对材料降解行为的影响等，得出交酯/环碳酸酯共聚体系降解行为一些共性和规律。

Then they formed C hexahydric rings during the carbonization process.T-700 carbon fiber had high tensile strength due to its smaller d 002, thicker L c and higher crystallinity.

利用DSC/TG、FT-IR、XRD、元素分析、SEM、TEM和HRTEM系统研究了聚丙烯腈预氧化纤维碳化中的结构演变与碳纤维微观结构。

The performace of material was tested by DSC,XRD,SEM,EIS and charge-discharge cycles . The influences of various synthesized condition , sintering time and the amount of F were studied and correlative technics parameter to improve performance of material were optimized. DSC shows that three endotherimc peaks and one large exothermic peak are observed in the temperature range 150-400℃, which is because of the removal of water,the decomposition of the organic constituents and the formation of spinel. Only the citrate precursor is sintered at least 450℃, the crystallinity of spinel phase could be formed intactly.

通过DSC、XRD、SEM、EIS和充放电循环等手段对材料进行性能测试，比较了不同合成温度、烧结时间和不同掺杂元素量等条件对材料性能的影响，优选出提高材料性能的相关工艺参数， DSC表明，采用溶胶-凝胶-络合法制备的前驱体在150-400℃中有三个小的吸热峰和一个大的放热峰，这是前驱体中的水分、柠酸酸及其盐和醋酸及其盐在蒸发及分解，柠檬酸前驱体至少需在450℃以上才可能形成完整的尖晶石材料。

The degree of crystallinity of PTMO and the lamellar thickness of the crystallites were found to increase with increasing λ.

拉伸对体系中非结晶的高频分子运动并没有明显的影响，拉伸使得结晶区更加趋于完善。

The results showed that the structure of St-g-PAM was meshy,and porous,and integrant linetype,the soluble starch had elliptic form,and PAM was linear color;the crystallinity of St-g-Pam had been improved,and was better than PAM;the thermal stability of St-g-PAM was also better than PAM,which was the significant reason that the graft polymer had the ability of excellent flocculation.

线型St-g-PAM作为一种新型的高分子絮凝剂，它结合了淀粉与聚丙烯酰胺的特性，广泛应用于废水处理、石油化工、造纸工业等领域[3~5]。由于其原料淀粉来源丰富、价格低廉，且线型St-g-PAM的成本比PAM低，故越来越受到人们的重视。

New Zealand white rabbits (3-4 months old, 3-4 kg weight) were the test animals, and they were divided into three groups proceeding in this study. In group A:One PLLA screw and one commercial screw were implanted in the right tibia. Two PLLA screws were implanted in the left. Furthermore, one PLLA bar was implanted in both right and left tibia respectively with onlay model in group B. Also,one PLLA plate was implanted in the left tibia and one commercial plate in the right respectively with onlay model in group C . Many tests were done on each sample in 1, 4, 8 and 12 weeks which included the observation of tissue response in group A, and the change of three-points bending, weight loss, molecular weight, crystallinity and morphology of fracture surface by scanning electronic microscopyin group B, and the change of three-points bending, weight loss and molecular weight in group C.

所使用实验动物为24只3-4个月大，体重3-4公斤的纽西兰兔，并将所使用材料及动物分为A、B、C三组进行。A组中於实验兔之右胫骨植入两支骨钉，一支为自制骨钉，一支为MacroPore市售骨钉，并钻一孔但不植入骨钉做为控制组；另於实验兔之左胫骨植入两支自制骨钉，另标示一区不钻孔不植入骨钉做为控制组。B组采用onlay1 模式於实验兔之左右胫骨各植入一自制长型片。C组也采用onlay模式於实验兔之左胫骨植入一自制骨板，於右胫骨植入一市售骨板，各於不同时间点( 1， 4及12周)将A及C组，而於( 1，4，8及12周)将B组内的植入物取出进行各种测试，包括A组的组织切片观察及B组的三点弯曲变化、质量损失、分子量变化、结晶度变化及扫描式电子显微镜观察断面型态改变及C组的三点弯曲变化、质量损失、分子量变化。

X-ray diffraction showed that the hydroxy-chromium oligocations can be used as a stable pillaring agent after aging at 70 ℃ for four days, and a pillared composite with high crystallinity can be obtain...

与原料2H-MoS2相比，柱撑材料的层间距增大，晶粒变小，比表面积增加并且热稳定性提高。对催化苯饱和加氢反应表明，柱撑材料Cr-MoS2的催化活性明显优于未柱撑的2H-MoS2和RaneyNi催化剂，且结晶度较好的柱撑材料更具有较高的催化活性和较好的可重复性。

Suitable for material identification、analysis、pleomorphic crystallization and determination of crystallinity.

适合于物质鉴定、解析、多形结晶和结晶度的测定与管理。

Compared with non-nanopolyaniline synthesized by conventional emulsion polymerization, nanopolyaniline has the narrow and uniform distribution of particle dimension and the diameter of particle is about 4-5nm,and the conductivity reaches 3.2S·cm-1, which is more than 100 times higher than that of nanopolyaniline;Moreover, it has higher solubility in conventional solvent and the solubility reaches 95% in N-methyl pyrrolidone;what's more ,it has higher crystallinity and more uniform crystal proved by XRD, apparent blue shift indicated by UV, which makes it possible to prepare transparent conductive composite films.

结果表明，微乳液法合成的纳米聚苯胺与常规乳液法合成的非纳米聚苯胺相比，具有明显的优越性：粒径分布窄，95%的在10nm 以下，最大的不超过30nm；电导率较高，达到了3.2S/cm，提高了2 个数量级以上；在有机溶剂中的溶解度较高，其中在N-甲基吡咯烷酮中的溶解率达到了95%；X 射线衍射仪分析表明，纳米聚苯胺结晶度高，晶型更为规整；紫外可见光谱研究发现，纳米聚苯胺在可见光区有明显的蓝移，为制备透明的导电复合膜提供了可能。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。