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Differential scanning calorimetry and polarizing microscope were used to study their liquid properties. Among them, nine are found to exhibit liquid crystal properties, and most of them displayed as heating monotropic liquid crystals. There are one or two mesophases and certain phase transition temperature,Δ H and temperature range of liquid crystal.

用差示扫描量热仪和偏光显微镜研究了其液晶性，发现其中九个配合物具有液晶性，多为升温单变液晶，有一至两个中介相，有确定的相转变温度、热焓和相变区间。

In the paper, the multidentate carboxylic acid ligands were used to combine with Cd, resulting in the three dimensional MOCPs single crystals—C12H16CdN2O8, with a low temperature hydrothermal synthesis method. The sample was characterized with IR spectra to affirm the organic groups in the frameworks, single-crystal X-ray diffraction to determine the crystal structure and composition of the frameworks, N2 adsorption isotherms at low temperature to measure the specific surface area and pore size distribution, and with TGA/DGA analysis to scale the thermal stability. Furthermore, the dissolution property and the photocatalytic activity of MOCPs under the ultraviolet ray condition were explored.

本文用低温水热合成法，用多齿羧酸配体异烟酸和Cd配位合成出[Cd(C6H4O2N)2(H2O)4]∞三维晶体并进行了表征：采用红外光谱法确认骨架中的有机官能团；用单晶X射线衍射分析法测定MOCPs的晶体结构，并确定其骨架的组成；通过低温氮气吸附等温线测定了其比表面积和孔径分布；以热重分析和差热分析测定材料骨架的热稳定性；测定了晶体的溶解性能；最后以亚甲基蓝为目标降解物，对[Cd(C6H4O2N)2(H2O)4]∞的光催化活性及亚甲基蓝的氧化动力学进行了探索(来源：A2444BC论文网www.abclunwen.com)。

With the development of photoelectron technology, the role of lithium niobate crystal is more and more important. The need of ultra-precision device, made with lithium niobate crystal, increased steadily.

随着光电子技术的发展，铌酸锂晶体在行业中的作用越来越重要，利用铌酸锂晶体制作超精密元器件的需求与日俱增。

This article is divided into seven parts, the first part is the structure of LiNbO ; The second part is the basic physical property (especially for optical property); The third project is for the mix substance which takes some operation for LiNbO crystal; The 4th and 5th part for cyclical polarization niobic acid lithium crystal synopsis and application; The sixth part for Laman spectrum synopsis and the seventh part is the something about experiment.

本文共7部分，第1部分为铌酸锂晶体的结构；第2部分为基本物理性质；第3部分为铌酸锂晶体的掺工程；第45部分为周期极化铌酸锂晶体的简介及应用；第6部分为拉曼光谱简介；第7部分为实验部分。

This article is divided into seven parts, the first part is the structure of LiNbO ; The second part is the basic physical property (especially for optical property); The third project is for the mix substance which takes some operation for LiNbO crystal; The 4th and 5th part for cyclical polarization niobic acid lithium crystal synopsis and application; The sixth part for Laman spectrum synopsis and the seventh part is the something about experiment.

本文共七部分，第一部分为铌酸锂晶体的结构；第二部分为基本物理性质；第三部分为铌酸锂晶体的掺工程；第四五部分为周期极化铌酸锂晶体的简介及应用；第六部分为拉曼光谱简介；第七部分为实验部分。

Physical and chemic properties of Cr:LiSAF aresummed up. The characteristic of KN crystal is analyzed. At normal temperature, KN crystal can obtain noncritical phase match of 90 at wavelength of 857nm.

对Cr：LiSAF晶体的物理和光学性质进行了总结，同时对KN晶体各个面内的相位匹配角度和有效非线性系数进行了计算并对其相位匹配特性做了分析。

The 20 mm long KTA crystal cut for typeⅡ noncritical phase matching was adopted as the nonlinear crystal parametric converter in this experiment.

激光基质材料采用Nd：YVO4晶体，采用按Ⅱ类非临界相位匹配切割、长20 mm的KTA晶体作为非线性光学晶体。

Grounding on the purpose of industrialization of laser, based on the thought of astigmatism compensation and thermal stability of the cavity, we employed high power LD to pump Nd:YVO4 crystal and used the introcavity frequency doubling with type 1 noncritical phase-match LBO crystal, which has high damage threshold. The cavity parameters are optimized by the use of ABCD theory and the resonatorstructure CAD software.

立足于激光器的产品化，基于谐振腔的像散补偿和热稳定性的设计思想，采用大功率LD单端泵浦Nd：YVO_4晶体，具有高光损伤阈值的Ⅰ类非临界相位匹配LBO晶体腔内倍频方案，应用ABCD定律和腔结构模拟软件CDA设计并优化了一组腔参数。

The results show that the heterostructure photonic crystal can extend remarkably the photonic bandgap compared with the periodic structure;a defect is inserted into the heterostructure photonic crystal,the nontransmission band is wider than that of the symmetric structure without heterostructures,(1H1L)_m(1H)_n(1L1H)_m.

结果表明，与周期结构相比异质结构光子晶体可以显著地拓宽光子晶体的光子带隙；在该文提出的结构中引入缺陷，与(1H1L)m(1H)n(1L1H)m光子晶体相比，产生缺陷模式光子带隙范围明显拓宽，适当调整缺陷层的数目、位置和厚度可得到多通道滤波；并研究了实际操作中随机误差带来的影响，随无序度的增大，其带宽基本不变。

Finally, the cytotoxic and antibacterial activities of the oxamido-bridged binuclear complexes were studied in vitro.. This dissertation consists of three sections as follows:1. The crystal structure of a oxamide dinitrate,(1) [H_4dmaeoxd](NO_3)_2 H_2dmaeoxd = N,N\'-bis[2-ethyloxamide, has been obtained. The diversity of complexes with different structures is carried out by successful synthetic strategy of controlling species of metal ions, counter anions, pH values and solvents in the course of synthesis. Four dinuclear complexes bridged by trans-dmaeoxd2-: [Cu_2_2](ClO_4)_2 (2), [Cu_2_2](ClO_4)_2 (3),、[Cu_2(Me_2phen)_2](ClO_4)_2 (4), [Cu_2_2(H_2O)_2] (5); Four dinuclear complexes bridged by cis-dmaeoxd2-: [NiNi_2](ClO_4)_2 (6), [CuNi_2](ClO_4)_2·2CH_3OH (7), [CuZn_2]-(ClO_4)_2·2H_2O (8), [Cu(H_2O)Ni_2](ClO_4)_2.0.5CH_3OH (9); three 1-D polynuclear complexes: [Cu_2]_n·nH_2O (10), [Cu_2(H_2O)_2-]_n·4nH_2O (11), [Cu_2(H_2O)]_n(NO_3)_n·2nH_2O (12); one 2-D polynuclear complex,[Cu_6_3(μ_3-OH)_2(H_2O)_2]_n(ClO_4)_(4n).2nH_2O (13); the others: [VO(H_2O)]·2H_2O (14), [Zn_2_4](ClO_4)_2·H_2O (15), [Cu_2]·2DCM (16) have been synthesized and characterized by X-ray single crystal diffraction, elemental analysis, IR spectra.

本论文主要包括以下三部分：一、合成得到了一个草酰胺配体硝酸盐的单晶结构，[H_4dmaeoxd](NO_3)_2 (1)；通过调控金属离子的种类、端基配体、抗衡阴离子、溶剂、pH值等条件定向合成了四个反式草酰胺桥联双核铜配合物：[Cu_2_2](ClO_4)_2 (2)、[Cu_2_2](ClO_4)_2 (3)、、[Cu_2(Me_2phen)_2](ClO_4)_2 (4)、[Cu_2_2(H_2O)_2] (5)；四个顺式草酰胺桥联同/异双核配合物：[NiNi_2](ClO_4)_2 (6)、[CuNi_2](ClO_4)_2·2CH_3OH (7)、[CuZn_2]-(ClO_4)_2·2H_2O (8)、[Cu(H_2O)Ni_2](ClO_4)_2.0.5CH_3OH (9)；三个一维聚合物： [Cu_2]_n·nH_2O (10)、[Cu_2(H_2O)_2-]_n·4nH_2O (11)、[Cu_2(H_2O)]_n(NO_3)_n·2nH_2O (12)；一个二维聚合物： [Cu_6_3(μ_3-OH)_2(H_2O)_2]_n(ClO_4)_(4n)。2nH_2O (13)；单核钒配合物[VO(H_2O)]·2H_2O (14)、草酸根桥联双核锌配合物[Zn_2_4](ClO_4)_2·H_2O (15)、美洛西康铜配合物[Cu_2]·2DCM (16)，利用元素分析、摩尔电导、红外光谱、电子光谱和单晶X-射线衍射对上述所得化合物进行了结构表征，探讨了结构影响因素，并研究了其超分子结构。

Neither the killing of Mr Zarqawi nor any breakthrough on the political front will stop the insurgency and the fratricidal murders in their tracks.

在对危险的南部地区访问时，他斥责什叶派民兵领导人对中央集权的挑衅行为。

In fact,I've got him on the satellite mobile right now.

实际上 我们已接通卫星可视电话了