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A novel monomer the 1-methyl-4,5-bis(4-chlorobenzoy) cyclometer containing cyclohexene were prepared,so a group of novel polys containing the cyclohexene and phthalazinone moieties was prepared by the nucleophilic displacement reaction of 1-methyl-4,5-bis(4-chlorobenzoyl) cyclohexene and 4,4′-dichlorodiphenyl sulfone and 4-(3,5-dimethyl-4-hydroxyphenyl)-2,3-phthalazin-1-one.

用新型聚合单体1-甲基-4，5-二(4-氯代苯甲酰基)环己烯与4-(4-羟基苯基)-2，3-二氮杂萘-1-酮、4，4′-二氯二苯砜单体经亲核共缩聚反应，成功地合成了含环己烯结构的杂环联苯型聚醚系列聚合物。

A novel monomer the 1-methyl-4,5-bis (4-chlorobenzoy) cyclometer containing cyclohexene were prepared,so a group of novel polys containing the cyclohexene and phthalazinone moieties was prepared by the nucleophilic displacement reaction of 1-methy l-4,5-bis(4-chlorobenzoyl) cyclohexene and 4,4'-dichlorodiphenyl sulfone and 4-(3,5-dimethyl-4-hydroxyphenyl)-2,3-phthalazin-1-one.

用新型聚合单体 1-甲基-4，5-二(4-氯代苯甲酰基)环己烯与 4-(4-羟基苯基)-2 ，3-二氮杂萘-1-酮、4，4′-二氯二苯砜单体经亲核共缩聚反应，成功地合成了含环己烯结构的杂环联苯型聚醚系列聚合物。

The results showed that 1 there were no significant differences in the rates of cytoplast protrusion and enucleation between oocytes that were incubated in colchicine (0.4 μg/mL) for 0.5 h and oocytes that were incubated in colchicine (0.4 μg/mL) for 1 h, and the rate of cytoplast protusion can be 85.4% while the rate of cytoplast enucleation is 100%. 2 There was no significant difference in oocyte enucleation between oocytes treated with medium containing 0.2 μg/mL colchicine for 0.5 h and oocytes treated with medium containing 0.4 μg/mL colchicine for 0.5 h. 3 A maturation time of 18–23 h did not affect the rates of cytoplast protusion and enucleation by chemically assisted enucleation, whereas the rate of enucleation of oocytes by blind enucleation was found to decrease with a prolonged incubation time. 4 The development rates of reconstructed embryos could not be influenced by these two enucleation methods, increased from oocytes matured for 21–23 h.

结果表明： 1 卵母细胞在0.4 mg/mL的秋水仙素溶液中分别孵育0.5 h和1 h，胞质突起率和去核率没有显著的差异，突起率可高达85.4%，去核率达到100%； 2 0.2 mg/mL或0.4 mg/mL秋水仙素溶液将卵母细胞处理0.5 h，对去核效果没有显著影响； 3 对于体外成熟18~23 h的卵母细胞，随着成熟时间的延长，盲吸法的去核率降低，但没有影响秋水仙素诱导胞质突起的比率和去核率； 4 两种去核方法对重构胚的发育没有产生显著影响，但成熟21~23 h卵母细胞重构胚囊胚的发育率显著高于成熟18~20 h卵母细胞重构胚囊胚的发育率。

The fabrication of fibers was attempted. The copolymers, the copolymers containing MOCT and the copolymer films containing MOCT were characterized by using Fourier Transform Infrared Spectroscopy, Scanning Electron Microscopy, Differential Scanning Calorimetry, Thermogravimetric Analyzer and X-ray Diffraction etc. The conclusions were summarized as following,1. The AN/MMA copolymers were testified that copolymerization of most AN and MMA occurred and the ratio of AN and MMA in copolymer was less than the ratio of monomers. With the increase of the contents of MMA, the viscosity of copolymer solution, molecular weight and decomposition temperature of copolymers increase.

通过傅立叶变换红外光谱、扫描电子显微镜、差示扫描量热分析、热重分析、X-射线衍射分析等测试方法对得到的AN／MMA共聚物、含有正十八烷微胶囊的共聚物以及共聚物膜等进行了测试和分析，得到如下的研究结论： 1、丙烯腈—甲基丙烯酸甲酯之间发生了聚合反应，共聚物的组成比略小于投料比；共聚物的粘度和分子量随着第二单体MMA加入量的增加有增大的趋势；第二单体加入量的增大使得共聚物的分解温度升高，通过热重分析证实当AN／MMA摩尔比为85／15时，共聚物的耐热稳定性较高。

It can be seen from the evaluation result that the high and low diffluence measures of phosphorus-containing wastewater concentration implemented in the process and the improvement of air knife material and airflow mode at the etching machine can be controlled effectively and reduce the amounts of phosphorus-containing wastewater.

从制程端实施含磷废水浓度高、低分流处理措施及进行蚀刻机台风刀材质与流动模式改善，均能有效控制并降低含磷废水排放量。2。

When the molar fraction of SnO2 is 83%, the main component of the coating isO2 solid solution with rutile structure. When the molar fraction of SnO2 is 44%, the main components of coating are theO2 solid solution with rutile structure andO2 solid solution with fluorite structure. When the molar fraction of SnO2 is 17%, the main component of the coating isO2 solid solution with fluorite structure. Annealed at higher temperature than 450 ℃, CeO2 is found in the coating containing 83%Sn, and there is not SnO2 in the coating containing 83%Ce, which suggests that fluoriteO2 has higher thermal stability than rutileO2. When the molar fraction of SnO2 increases, the dispensability of the coatings is improved greatly.

结果表明：通过控制制备条件可获得具有纳米结构的钛阳极涂层；当Sn的摩尔分数为83%时，涂层主要为金红石相的O2固溶体；当Sn的摩尔分数为44%时，涂层中金红石相O2固溶体和萤石结构的O2固溶体共存；当Sn的摩尔分数为17%时，涂层由萤石结构的O2固溶体组成；高于450 ℃退火时，含83%Sn的涂层中出现CeO2相，而在含83%Ce的涂层中没有出现SnO2相，表明在相同的溶质浓度下，萤石结构的O2固溶体比锡基金红石相O2固溶体具有更好的热稳定性；而涂层中的SnO2具有明显改善涂层分散性的作用。

Since most of the large molecules containing phosphorus element have double bonds, it is necessary to consider the special structures of double bonds in order to deal with these large systems more accurately. So, based on density functional theory and electronegativity equalization principle, applying a general atom-bond electronegativity equalization method , using separated program, through regression and least-squares optimization , the parameters of atoms and bonds in molecules are determined . By these parameters , the charge distributions and the energy of some molecules containing phosphorus element, especial the fragment of DNA, RNA, are calculated . The results are quite good.

由于这些含磷生物大分子体系都含有双键，为了明确的处理双键，进而更准确的解释带有双键和共轭双键的含磷生物大分子结构与性质的关系，我们以密度泛函理论~([1-4])和电负性均衡原理~([5-9])为基础，应用和开发原子-键电负性均衡方法中的σπ模型，利用最小二乘法，拟合确定了一些分子（含碳、氮、氧、氢以及磷等原子）的各种类型原子及化学键区域的参数，并利用上述参数计算了一些多聚核苷酸的电荷分布以及分子的总能量，进行了讨论，得到的结果可以和从头算相媲美。

In comparison to the vector containing 4-exa gene without spacer peptide, the expression level of vectors containing glycosylation site sequence and enterokinase recognition site sequence as spacer was increased by 4 and 9 times, respectively.

在EXA的N端增加间隔肽可促进蛋白分泌，与不含间隔肽序列的4拷贝EXA串联表达载体相比，含有糖基化位点和肠激酶识别位点间隔肽的插入，使蛋白表达水平分别提高了4倍和9倍。

Methods:A YWG-C18 column was used.The mobile phase consist ed of acetonitrile containing 0.2% methanol-water solution containing 0.1% tri ethylamine and 0.1% phosphoric acid(3∶97)and the detection wavelength was 220 nm.

采用高效液相色谱法，色谱柱为YWG-C18柱，流动相为0.2%甲醇的乙腈溶液-含0.1%三乙胺、0.1%磷酸的水溶液(3∶97)，检测波长为220 nm。

Comerford, the versicle: May this Yuletide bring to thee, Joy and peace and welcome glee : a butt of red partly liquefied sealing wax, obtained from the stores department of Messrs Hely's, Ltd., 89, 90, and 91 Dame street: a box containing the remainder of a gross of gilt "J" pennibs, obtained from same department of same firm: an old sandglass which rolled containing sand which rolled: a sealed prophecy written by Leopold Bloom in 1886 concerning the consequences of the passing into law of William Ewart Gladstone's Home Rule bill of 1886: a bazaar ticket, no 2004, of S.

两张色情照片卡。

Neither the killing of Mr Zarqawi nor any breakthrough on the political front will stop the insurgency and the fratricidal murders in their tracks.

在对危险的南部地区访问时，他斥责什叶派民兵领导人对中央集权的挑衅行为。

In fact,I've got him on the satellite mobile right now.

实际上 我们已接通卫星可视电话了