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Utilizing 6 and several kinds of diazides prepared in our lab, polys containing 1,2,3-triazolyl and perfluorocyclobutane units were synthesized by "Click chemistry". Utilizing the polycondensation reaction between 6 and several commercially available aromatic diphenol or copolymerization reaction after adding another active aromatic dichloride, fluorinated polys containing phenylphosphine oxide units were synthesized. Utilizing the polycondensation reaction between 6 and several commercially available aromatic dianhydride, fluorinated polys containing PPO units were synthesized.Secondly, structure characterization of fluorinated polys.

利用化合物6同各种自制的二叠氮化合物，通过&Click chemistry&，合成了具有1，2，3-三唑环结构单元的全氟环丁基类聚芳醚；利用化合物22同各种商业化的芳香二元酚类化合物进行缩聚反应或者再加入另外一种活性芳香二氯代物进行三元共聚反应，制备了具有苯基氧膦结构单元的含氟聚芳醚；通过化合物25同各种商业化的芳香二元酸酐类化合物进行缩聚反应，得到了具有PPO结构单元的含氟聚醚酰亚胺。

An alkaline solution containing mercaptides is regenerated in an improved process wherein the alkaline solution to be regenerated containing a suitable oxidation catalyst is contacted with an oxygen-containing solvent which is immiscible with said alkaline solution in a reaction zone comprising a plurality of fibers positioned longitudinally within a conduit, whereby the two liquids are in contact while concurrently flowing through said reaction zone during which the mercaptides contained in the alkaline solution are oxidized to disulfides and are simultaneously extracted from the alkaline solution into the solvent solution.

包含 mercaptides 的碱解决在一个改良的程序被再产生在何处碱的解决被再产生包含一个适当的氧化催化剂与被说反应的碱的解决组成一个纤维的多数地域纵观地放置在一个导管里面的对一个包含氧的溶剂感到不能相混合的一起连络，那里当协同地流动过说的反应地域的时候，这二种液体保持接触在哪一个期间包含在碱的解决 mercaptides 被使氧化到 disulfides 而且同时地从碱的解决到有偿付能力的解决被吸取。

Serum containing SSTG was obtained at different time after perorally administrated with different dose of SSTG.The cardiomyocytes were deprived of oxygen and glucose to mimic hypoxia reoxygenation injury and were treated by serum containing SSTG when reoxygenation.LDH content in supernatant was detected after reoxygenation.LDH release suppression rate was used to study the time-effect and dose-effect of serum containing SSTG.

以中药有效组分配伍方剂双参通冠方不同灌胃剂量、药后不同取血时间所得的药物血清为受试药物；培养心肌细胞，进行缺氧复氧实验，复氧同时给予不同双参通冠方药物血清处理，实验结束后取培养上清检测LDH值，以LDH释放抑制率为指标，观察含药血清药理作用强度与体内给药的量效、时效关系。

To discover new strobilurin analogues with high pesticidal activity, a series of new strobilurin derivatives containing substituted pyrazole and pyrimide ring, which included 124 novel compounds (73 compounds containing substituted pyrazole ring and 51 compounds containing substituted pyrimide ring) were designed and synthesized. In addition, 36 new intermediates were synthesized. Their structures were characterized by ~1H NMR and elemental analysis, partial compounds were characterized by MS and IR once again.

为了发现具有更好生物活性的新型Strobilurin类化合物，本论文在详尽总结文献的基础上，设计并合成了含吡唑和嘧啶环的新型Strobilurin类化合物124个，其中含吡唑环的新型Strobilurin类化合物73个，含嘧啶环的新型Strobilurin类化合物51个；未见文献报道的中间体36个，所合成的化合物经过~1H NMR、IR、LC-MS或元素分析等确定了结构。

To discover new strobilurin analogues with high pesticidal activity, a series of new strobilurin derivatives containing substituted pyrazole and pyrimide ring, which included 124 novel compounds (73 compounds containing substituted pyrazole ring and 51 compounds containing substituted pyrimide ring) were designed and synthesized. In addition, 36 new intermediates were synthesized. Their structures were characterized by 1H NMR and elemental analysis, partial compounds were characterized by MS and IR once again.

为了发现具有更好生物活性的新型Strobilurin类化合物，本论文在详尽总结文献的基础上，设计并合成了含吡唑和嘧啶环的新型Strobilurin类化合物124个，其中含吡唑环的新加热管型Strobilurin类化合物73个，含嘧啶环的新型Strob 加热管 ilurin类化合物51个；未见文献报道的中间体36个，所合成的化合物经过1H NMR、IR、LC-MS或元素分析等确定了结构。

And a relative preparation is characterized in that according to mol ratio (0.8-0.975):(1.8-1.95):(0.010-0.15):(0.010-0.15) to prepare and mix Mg powder, B powder, C nanometer powder, and SiC nanometer powder uniformly to be filled into an iron tube or iron-copper composite tube to be sealed, rotationally forges, draws and rolls to obtain MgB2 superconductive material containing C and SiC nanometer powder, or tablets the raw powder mixed uniformly via a tablet press, to obtain MgB2 superconductive block containing C and SiC nanometer powder, arranges obtained band or block in a vacuum furnace, vacuums and fills argon gas, keeps temperature for 0.2-3h at 600-1200DEG C, and obtains MgB2 superconductive material containing C nanometer powder and SiC nanometer powder.

制备这种MgB 2 超导材料的方法，其特征在于，将Mg粉，B粉，C纳米粉，SiC纳米粉按照摩尔比(0.8-0.975)∶(1.8-1.95)∶(0.010-0.15)∶(0.010-0.15)配制并混合均匀，装入铁管或铁铜复合管中密封后，按顺序先后进行旋锻、拉拔、轧制，得到含C和SiC纳米粉的MgB 2 超导线材；或者将混合均匀的原料粉用压片机进行压片，得到含C和SiC纳米粉的MgB 2 超导块材；将得到的线带材或块材放置真空炉中，抽真空后充入氩气，在600℃-1200℃保温0.2-3小时，最终得到含有C纳米粉和SiC纳米粉的MgB 2 超导材料。

Group E = atmospheres containing metal dust including aluminum, magnesium, their commercial alloys, and other metals of similar hazardous characteristics; Group F = atmospheres containing carbon black, coal or coke dust; Group G = atmospheres containing flour, starch, or grain dust.

组E =大气中含有金属粉尘，包括铝，镁，它们的合金，具有类似危险特性的其他金属；组F =大气中含有炭黑，煤或焦炭粉尘；组G =大气中含有面粉，淀粉，或谷物粉尘。

Business card printing and membership card making business major movements of hazardous wastes: there are 7 mediumso waste, waste containing chromium, copper-bearing waste, waste containing mercury, lead-containing waste, scrap and waste halogenated organic solvents.

制卡和会员卡制作行业危险废物主要有7种：感光材料废物、含铬废物、含铜废物、含汞废物、含铅废物、废卤化有机溶剂、废有机溶剂。

According to the domain organization, the GGDEF-EAL containing proteins (pfam database, version 17.0) were classified into A and B types. Six hundreds and five of the 621 proteins were in A type, which was also found in the ancient bacteria Aquifex aeolicus VF5 suggesting that this is the ancestor of the GGDEF-EAL proteins. Phylogenetic analysis of GGDEF- and EAL- containing proteins in the genome of V. vulnificus YJ016 revealed that GGDEF-EAL proteins were clustered. Comparative analysis of domain organization of the clads in the EAL tree allowed identification of several duplication events. The results indicated that most of the GGDEF- and EAL- containing proteins arised by gene duplication.

根据pfam资料库(Version 17.0)，我们整理同时拥有GGDEF和EAL功能性区域的蛋白质，这些蛋白质可以被区分成两种型态，在总数621个GGDEF-EAL中有高达606个是A型态，而且它在古老的细菌Aquifex aeolicus VF5的基因体中也能找到，因此我们推测它可能是GGDEF-EAL的袓先，藉由分析创伤弧菌中所包含之GGDEF和EAL的演化关系，大部份的GGDEF-EAL会群聚在树型相近的位置，进一步比较在EAL树型上有邻近关系的蛋白质序列，根据他们的长度、与所包含的功能区域，我们找到了一些重制的演化痕迹，这样的结果指出，目前看到大多数的GGDEF 和EAL可能都是经过重制产生。

Methods(1) Construction of plant expression vector containing RS geneThe cloning vector pT-RS was constructed containing RS gene extracted from the leaf tip of Vitis vinifera by PCR amplification and RS sequence was identified by PCR amplification,enzymes digestion and sequence analysis.The plant expression vector containing RS gene was obtained and RS sequence was identified by PCR amplification and double enzymes digestion too.

研究方法(1)含白藜芦醇合酶基因的植物表达载体的构建提取葡萄基因组总DNA，通过PCR扩增得到RS基因，将此基因连接到克隆载体pGEM-T Vector，得到重组载体pT-RS；经PCR、酶切及序列分析鉴定后，将RS基因克隆到植物表达载体pBI121，得到重组载体pBI-RS，用PCR及双酶切方法进行鉴定。

Neither the killing of Mr Zarqawi nor any breakthrough on the political front will stop the insurgency and the fratricidal murders in their tracks.

在对危险的南部地区访问时，他斥责什叶派民兵领导人对中央集权的挑衅行为。

In fact,I've got him on the satellite mobile right now.

实际上 我们已接通卫星可视电话了