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Chemical research indicated that the main chemical constituents of Aquilegia is C- glycosylflavones and oxoaporphine alkaloids, which are the characteristic chemical constituents, especially, the content of C-glycosylflavones is very high in this genus.

通过对耧斗菜属植物的化学研究表明,黄酮碳甙和氧化阿朴菲类生物碱是该属的特征性成分;其中尤以黄酮碳甙含量较高,为主要成分。

It was shown that the stable carbon isotope composition of beef tissue was primarily dependent on the diet the animals were fed,meanwhile theδ~(13)C values of cattle tail hair, defatted muscle and crude fat all enhanced with the increment of the proportions of C4 constituents in diet, but those values were on the contrary with the enhancement of the proportions of C3 constituents. Moreover, allδ~(13)C values of different tissues were significantly correlated with the content of C4 and C3 plant material. So, the main component of cattle feed could be investigated with the help ofδ~(13)C values. Theδ~(15)N values of beef tissues were affected by feed composition to some extent, but it had no regularity. The cattle tail hair and defatted muscle enriched in 13C to their feeds gave different results between the two groups, but cattle tail hair enriched in 15N much more than defatted muscle and in the proportion of 3‰- 5‰, plus, cattle variety and individual had effect on the proportion of enrichment.

结果表明,牛组织中碳同位素组成主要受饲料的影响,牛尾毛、脱脂肌肉、粗脂肪中的δ~(13)C值随着C4植物含量在牛饲料中的比例增加而升高,随着C3植物含量在牛饲料中的比例增大而降低,并且均与C4、C3植物含量呈极显著的相关性(P.01),用牛组织中的δ~(13)C值可以调查牛饲料中的主要成分;牛组织中的氮同位素一定程度上受饲料因素的影响,但未随饲料组成成分的改变而呈现规律性变化;牛尾毛、脱脂肌肉相对饲料对13C的富集比例两组试验结果不一致,牛尾毛对15N的富集比例大于脱脂肌肉,富集比例约在3‰- 5‰,饲料种类、牛个体等因素对富集比例均有一定影响;牛尾毛、脱脂肌肉、粗脂肪中的δ~(13)C值三者之间相关性达到极显著水平(P.01)。

Were extracted by sterilize distillation and analyzed by GC-MS, 69 constituents were identified according to NIST MS database, the main constituents were thymol, carvacrol, p-cymene, caryophyllene, terpineol. 27 constituents from this plant were discovered for the first time. The phytochemical study of this plant was also conducted.

通过水蒸气蒸馏法提取牛至挥发油,利用GC-MS现代技术分析,通过NIST质谱库检索,鉴定了挥发油中的69种成分,其主要成分为麝香草酚、香荆芥酚、对聚伞花素、石竹烯、松油醇等;其中27种化合物为首次从该植物中鉴定。

A new technology, Supercritical Fluid CO_2 Extraction, was also supplied to study the plant. The technological parameter was optimal. Total extract of SFE-CO_2 were 4.86 times of the essential oil extracted by SDE, main active extracted constituents were 1.36% high than SDE. The chemical constituents of SFE-CO_2 were also analyzed by GC-MS. 57 constituents were identified, 29 constituents of them were first discovered. 24 constituents were discovered in two extract. Fingerprint is a good technology to elevate the quality of herb medicine. The main active fraction can be extracted by SDE and SFE, Fingerprint was studied respective, chromatographic parameter was acquired. 22 peaks were assigned common peaks in the spectrum of essential oil, 17 peaks were assigned to common peaks in the spectrum of SFE extract.

采用现代共性关键技术超临界CO_2萃取技术,通过正交试验,优选了超临界CO_2提取牛至挥发油的工艺,并与传统的水蒸气蒸馏法进行了比较研究,结果显示:前者提取有效部位的收率为后者的4.87倍,主要有效成分的转移率是后者的1.36倍;采用GC-MS分析方法和NIST质谱库检索,对SFE和SDE所提化学成分进行比较,SFE分离鉴定了57种化合物,占提取物总含量的86.96%,其中29种化合物为首次从该植物中鉴定;后者分离鉴定了69个化合物,占提取物总量的98.28%,其中27种化合物为首次从该植物中鉴定;两种方法的提取物中共有成分25种,包括主要有效成分麝香草酚、香荆芥酚、对聚伞花素等。

Results: the yield rate of the collected volatile oil of artemisia indica and artemisia feddei was 0.32%, 0.29%, respectively. the main constituents of them were as follows: eucalyptol, camphor, borneol, terpineol, cubebene, caryophyllene, caryophyllene oxide, germacrene d, etc, which was similar to the constituents of volatile oil from artemisia argyi. but the contents of volatile oil were different in different medicinal materials. longiverbenone with high content in artemisia feddei was can not be detected in artemisia indica and artemisia argyi.

结果:广西产五月艾与细叶艾挥发油的得率分别为0.32%、0.29%;五月艾、细叶艾和艾叶挥发油中均含有桉油精、樟脑、龙脑、松油醇、荜澄茄油烯、石竹烯及其氧化物、大根香叶烯d等药效成分,但各成分在不同药材中的含量存在一定差别;此外,细叶艾挥发油中含量较高的长叶马鞭烯酮在五月艾和艾叶挥发油中均未检出。

The immiscibility of heterophases of solid organic and inorganic constituents was resolved by the in situ sol-gel transition polymerization of ZnO nanofillers within PMMA in the presence of dual functional agent, monoethanolamine, which provided strong secondary interfacial interactions for both complexing and crosslinking of constituents.

混溶的有机和无机成分,通过原位溶胶凝胶聚合过渡锌有机玻璃内的双重功能驻留剂乙醇胺,提供强大的互动界面上,既络合交成分。

The constituents were extracted by some solvents. 18 constituents were isolated from Chloroform fraction by different chromatography. 15 constituents were identified by IR ,MS and NMR as follows: 3-sitosterol, P-sitosterylpalm itate,succinate acids, 1, 4-benzenediol, 1, 2-benzenediol, p-hydroxybenzaldehyde, syringaresinol, oleanolic acid, usolic acid, ethyl caffeate , Rosmarinic acid ethylster and etc. In such constituents ,nine compounds were isolated for first time from Origanum vulgare L..

牛至药材经水煮醇沉法所得浸膏,利用溶剂法和色谱法从中分离得到18个单体成分,通过IR、MS、NMR等波谱技术鉴定了其中的15个化合物,分别为β-谷甾醇(1)、β-胡萝卜苷(2)、琥珀酸(3)、对-二苯酚(4)、邻-二苯酚(5)、对羟基苯甲醛(6)、1.2-二羟基-4-异丙基-5-甲基苯(7)、新木脂素(8)、丁香脂素(9)、齐墩果酸(10)、乌苏酸(11)、4-二十六烯(12)、正二十六醇(13)、咖啡酸乙酯(14)、迷迭香酸乙酯(15)等,其中化合物3、4、5、6、7、8、9、14、15等9种化合物均为首次从该属植物中分离得到。

Aromatic constituents of Huangdan Oolong tea were analysed with GC and MS and were compared in different green-making humid conditions.The major aromatic constituents of Huangdan Oolong tea were nerolidol,α-farnesene, linalool and its oxide, geraniol, pheny lacetal dehyde, indole, cis-jasmine lactone β-ionone cis-jasmone, benzyl acetate and so on.At the same temperature,the content of aromatic constituents were different, the aromatic quality in the 75% humid condition was better,which was more fragrant and kept longer.

用GC/MS法分析了黄旦品种乌龙茶的香气组分,并对不同湿度做青环境条件下生产的乌龙茶香气组分进行比较分析表明:黄旦乌龙茶主要香气成分为橙花叔醇、α-法呢烯、芳樟醇及其氧化物、香叶醇、苯乙醛、吲哚、顺-茉莉内酯、β-紫罗酮+顺-茉莉酮、乙酸苄酯等;在相同温度(23℃),不同湿度做青环境生产的黄旦乌龙茶香气主要特征成分含量和精油总量各不相同,且香气品质以做青环境相对湿度75%为好,香气高且持久。

Immediate constituent analysis: The analysis of a sentence in terms of its immediate constituents-word groups, which are in turn analyzed into the immediate constituents of their own, and the process goes on until the ultimate constituents are reached.

直接成分分析法:先把句子分析为直接成分-词组,再把这些直接成分依次切分,得到各自的直接成分,层层切分,直到最终成分为止。

Immediate constituent analysis-----:IC analysis for short , the analysis of a sentence in terms of its immediate constituents---word groups,which are in turn analyzed into the immediate constituents of their own,and the process goes on until the ultimate constituents are reached.

先把句子分析为直接成分-----词组或短语,再把这些直接成分依次切分,得到各自的直接成分,层层切分,直到最终成分为止。

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