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The aliquot was determined and confirmed by gas chromatography-negative chemical ionization mass spectrometry using external standard method.

样品中三唑醇残留物由正己烷饱和的乙腈(含1%冰醋酸)提取，加入无水硫酸镁与无水醋酸钠振荡促使提取液分层后进行固相分散萃取净化，用气相色谱-负化学离子源质谱法进行测定与确证，外标法定量。

The best extraction parameters are confirmed. The extraction temperature is 30℃, the extraction time is 20min, the extraction ratio is 4:1, and the extraction solution is alkalescency.

通过实验，确定了理论上最佳的萃取工艺条件：萃取温度30℃、萃取时间20min、萃取比4∶1、保持废水在碱性条件下萃取。

Study on the Crystallization Process of Labeled GL-7-ACA Acylase CA130 Complex 7β-bromoacetyl amino cephalosporanic acid (BA-7-ACA), an analog of glutaryl-7-amino cephalosporanic acid (GL-7-ACA), can inhibit and specifically alkylate GL-7-ACA acylase (CA130) from Pseudomonas sp. 130, forming a carbon-carbon bond between BA-7-ACA and the C-2 on indole ring of Trp-β4 residue of CA130.Here we reported that BA-7-ACA labeled CA130 (BA-C130) could self-catalyze the hydrolysis of BA-7-ACA during crystallization process. The hydrolysis was confirmed to be a reaction analogous to the one of GL-7-ACA by comparative MALDI-TOF (matrix-assisted laser desorption/ionization-time of flight) spectrometry analysis.

二、GL-7-AcA酰化酶CA130标记复合物的结晶过程研究溴乙酰氨基头孢烷酸（7β-bromoacetyl amino cephalosporanic acid，BA-7-ACA）作为戊二酰-7-氨基头孢烷酸（GL-7-ACA）的类似物，不仅能够抑制GL-7-ACA酰化酶CA130的活力，而且能通过在BA-7-ACA和CA130的β亚基第四位色氨酸吲哚环二位碳原子之间形成碳-碳共价键而将CA130特异的烷基化。

Mapping of microsatellite markers in two wheat crosses segregating for Pm23 and Pm4b, respectively, in combination with the reported mapping of Pm4a, indicated that the three genes were all linked to the marker Xgwm356 with a distance of 3-5 cM. Allelism between Pm4b and Pm23 was then confirmed, when the progenies of a cross between VPM1 (Pm4b) and Line 81-7241, were shown to be all resistant to a B.

利用获得的8个标记对Pm4b进行遗传作图，结果表明，4个标记与Pm4b连锁(Xgwm356、Xgdm93、Xbar76和Xbarc122)。3个抗白粉病基因(Pm4a、Pm4b和Pm23)均与标记Xgwm356连锁，遗传距离为3-5cM，等位性测验证明Pm23与Pm4b为等位基因。

Allyl alcohol was used for preparation methacrylate photosensitive polymer with allyl in side chain.The structure of product was confirmed by FTIR and 1HNMR spectroscopy,and the molecular weight of the terpolym...

用FT-IR和1HNMR图谱确认了结构，用凝胶色谱测定其相对分子质量，并从引发剂浓度、聚合温度、单体配比等方面进行讨论，同时对其光刻性能进行了研究。

Linguistics and ethnographic studies have confirmed that Korean belong to Central Asia Ural - Altaic.

语言学和人种学的研究已确定韩语属于中亚的乌拉尔-阿尔泰语系。

In the part of producing TONALIDE, through single-factor-experiments , the highest yield of reaction condition was confirmed as: reaction time about 4 hours; reaction temperature about 20 ; the quantity of chlori-acytyl about 10g; the quantity of aluminum chloride 13-15g and the yield of reaction was as high as 90%.

在TONALIDE的合成部分，通过单因素试验，找到了反应收率最高的反应条件为：反应时间4小时左右；反应温度20℃左右；乙酰氯的用量10g左右；反应中的三氯化铝的用量13～15g，此时反应收率可达90％。

RESULTS:① No obvious sight defect was detected with the quantitative detection of automatic sight apparatus.② ECT cerebrospinal fluid imaging thought that proximal frontal sinus of right cerebral frontal lobe was the leakage, and the liquid glucose in nasal cavity was quantitatively confirmed to be cerebrospinal fluid.③ Cranial CT showed that cleft could be observed in bilateral frontal lobe and lateral ventricle, low-density gas shadow could be observed in cisterna ambiens, cortex of frontal bone was discontinuous, and bone matrix was trapped.④ ECG showed that right forehead and temple had irregular slow wave, and attack of θ wave. Brain topographic mapping showed that the δ power value of right forehead was increased.⑤ EPQ: The scores of extraversion-introversion, neuroticism, psychoticism and lie were 55, 55, 80 and 50 respectively;⑥ MMPI: The code showed a mode of 69/96, indicating that the brain organ tended to paranoid schizophrenia.

结果：①自动视野仪定量检测未发现明确视野缺损；②ECT脑脊液显像考虑右侧大脑额叶近额窦部为漏口；鼻腔液体糖定量证实是脑脊液；③头颅CT额叶及侧脑室双侧裂，环池见低密度气体影，额骨骨皮质不连续，骨质下陷；④脑电图右额、颞不规则慢波，有θ波发作；脑电地形图：右额δ功率值增高；⑤艾森克人格问卷：内外向分55、神经质分55，精神质分80，掩饰分50；⑥明尼苏达多相人格调查表：编码显示69/96模式，提示脑器质性偏执型精神分裂症；⑦症状自评量表：总分147、阳性项目分37，躯体化、强迫状态、人际关系敏感、焦虑、敌对和其他6项目平均分超过常模。

There are 2 confirmed deaths from the shooting in Ambler Johnston dormitory in addition to the 31 at Norris Hall.

在Ambler Johnston公寓内，已有2人死亡。

In accordance with the principle of chemical dynamics, a new evaluation method for rate of ammonification of urea was established, and the type of reaction of ammonification of urea was confirmed.

根据化学反应动力学原理，建立了尿素氨化速度的评价方法，确定了尿素氨化反应的级数，测定了普通尿素、缓释尿素在特定条件下的氨化反应常数和半衰期，并依此评价了涂层缓释尿素的缓释性能。

On the other hand, the more important thing is because the urban housing is a kind of heterogeneity products.

另一方面，更重要的是由于城市住房是一种异质性产品。

Climate histogram is the fall that collects place measure calm value, cent serves as cross axle for a few equal interval, the area that the frequency that the value appears according to place is accumulated and becomes will be determined inside each interval, discharge the graph that rise with post, also be called histogram.

气候直方图是将所收集的降水量测定值，分为几个相等的区间作为横轴，并将各区间内所测定值依所出现的次数累积而成的面积，用柱子排起来的图形，也叫做柱状图。