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Synthesis of the antiepileptic tiagabine hydrochloride;2. Starting from tetrafuran, 2_(4_Aminosulfonylphenyl)_4H_1,2_thiazine_1_dioxide, an antiepileptic drug with special structure, was obtained via esterification, sulphonation, chloridization, condensation and cyclization.

以四氢呋喃为原料，经酯化、磺化、酰氯化、缩合、环化等步骤，合成了化学名为 4_(四氢_2H_1，2_噻嗪基_2 )苯磺酰胺_S_S_二氧化物的抗癫痫药舒噻嗪，通过IR、1HNMR和元素分析对其结构进行了表

The invention relates to condensation products comprised of cyclic carboxylic acid anhydrides of dicarboxylic acids, tricarboxylic acid anhydrides or tetracarboxylic acid anhydrides and difunctional polyamines, especially polyoxyalkylene amines.

本发明涉及由二元羧酸的环状羧酸酐、三羧酸酐或四羧酸酐和二官能化多胺，特别是聚氧化烯胺制备的缩合产物。

Bis (P—bromobenzylamino) ethane and 1,2—bis (m—Iodobenzylamino) ethane may be prepared by condensation of the corresponding halo benzaldehyde with ethylenediamine and followed by catalytic hydrogenation of the Schiff's bases over Pto_2 in glacial acetic acid solutions: Both Ⅱa and Ⅱb may react in neutral mediam with aldehydes to form well—defined crystalline tetrahydro—imidazole, which may be served as derivatives of identification for aldehydes: Under the same condition, however,Ⅱb may ...

用1，2-二乙烷与二十余种醛类作用，得到有固定熔点的晶体衍生物，它们的熔点分布在85—210℃之间，产率为40—96％，这试剂与甲基酮类在相同条件下无反应，因此，它可作为鉴定醛类的专属试剂。 2。上述衍生物用稀盐酸在室溫处理，能发生水解，可以定量地收回原来的醛，因此这试剂又可作为分离醛类的试剂。 3。上述衍生物可以用非水滴定法半微量地测定其分子量可作为鉴定醛类的另一项参考数据。 4.1，2-二乙烷与醛类能生成晶体衍生物，但这试剂也与甲基酮在同样条件下发生反应，所以不适合作为鉴定醛类的专属试剂。

A series of 3,3,6,6 tetramethyl 1,8 dioxo 9 aryl 1,2,3,4,5,6,7,8,9,10 decahydro acridines have been synthesized by the condensation of aromatic aldehydes, 5,5 dimethyl 1,3 cyclohexanedione and ammonium acetate in the presence of triethylbenzylammonium chloride as catalyst in water.

芳醛、5 ，5 二甲基 1，3 环己二酮与醋酸铵在三乙基苄基氯化铵催化下以水作为溶剂反应，生成一系列 3 ，3 ，6，6 四甲基 1，8 二氧代 9 芳基 1，2 ，3 ，4，5 ，6，7，8，9，10 十氢吖啶，与其它溶剂相比，水作为该反应的溶剂具有价格便宜，不易燃和无毒等优点，而且产率较高，产物的结构通过单晶X射线确

The compound of BNTMBP wassynthesized by the condensation reaction between 4-chloronitrobenzene (4CNB) and 4, 4'-dihydroxy-3, 3', 5, 5'-tetramethyl biphenyl in the presence of potassium carbonate in the mixture solvents of N, N-dimethylformamide and tolune.

4， 4'-二羟基－3， 3'， 5， 5'-四甲基联苯、4-氯硝基苯(4CNB)和碳酸钾在N， N-二甲基甲酰胺和甲苯的混合溶剂体系中回流反应，合成得到了4， 4'-双（4-硝基苯氧基）－3， 3'， 5， 5'-四甲基联苯；随后，在Pd/C-水合肼的还原体系中，被进一步还原，得到了4， 4'-双（4-氨基苯氧基）－3， 3'， 5， 5'-四甲基联苯。

The Limit Oxygen Index also can be raised from 16.5 to 22 and 23 respectively.The Octaphenyl POSS is synthesized via the hydrolysis and condensation of phenyltrichlorosilane (PhSiCl_3) and the subsequent rearrangement reaction catalyzed by tetramethylammonium hydroxide. Poly are easily synthesized from Ph-POSS via bromination with Br_2/Fe system.

以苯基三氯硅烷为起始原料，通过水解缩合、催化重排的办法制备了八聚苯基笼型倍半硅氧烷，在Fe粉催化条件下将溴元素引入Ph-POSS的苯环得到Br-POSS；使用该种Br-POSS和Sb_2O_3的混合物(3∶1，质量比)作为聚苯乙烯树脂的添加剂，采用熔融共混法制备(Br-POSS+Sb_2O_3)／PS复合材料。

Organosilicon resin microparticles with phenyl and aminopropyl groups were prepared via the hydrolytic co-condensation of phenyltriethoxysilane,γ-aminopropyltriethoxysilane and diphenyldimethoxysilane under the catalysis of tetramethylammonium hydroxide.

在四甲基氢氧化铵水溶液的催化作用下，将苯基三乙氧基硅烷、γ-氨丙基三乙氧基硅烷和二苯基二甲氧基硅烷进行水解共缩聚制备氨丙基苯基有机硅树脂微粉。

The normal method was through the hydrolysis and poly-condensation process of tetravalent metal alkoxides and inside which rare earth dopants are simply performed by dissolving salts into initial sol, thus makes matrices being introduced a higher percent of hydroxyl groups, affects the resulting luminescence efficiency and balance of two phases.

普通的方法为将稀土盐导入金属烷氧基化合物的溶胶然后水解缩聚，这使得金属离子分离的最小化过程受限以及含羟基过多，极大影响了发射效率和两相均衡。

In order to obtain versatile ulitity of host molecules, three new chiral calix [4] crown ethers containing aza, thio atoms bearing two chiral sites provided by -cysteine ester were synthesized by the condensation of calix [4] arene diacid dichloride with oligoethylene glycol bridged bis-amino acid methyl ester. All new compounds were characterized by NMR, MS and elemental analysis.

以-半胱氨酸为手性源，利用多甘醇二氯醚在碱性条件下对半胱氨酸巯基进行烷基化反应，成功地合成了多甘醇醚链桥联的半胱氨酸衍生物，醚化反应后，在高度稀释条件下与对叔丁基杯[4]芳烃二乙酰氯进行双功能基缩合反应成功地合成了新型的手性杯[4]含氮、硫杂冠醚，并利用〓H NMR、MS等谱图手段对其结构进行了表征。

Methods:LPO content was determined by TBA-Acetic acid method. Samples included healthy serum, plasma, leakage and seepage fluid from thoracicoabdominal cavity and extract materials from cells, plasma before and after taking panax quinquefolium L, serum samples after peroxidation were also taken from healthy patients, coronary heart disease, non-insulin dependent diabetes mellitus, hypertension, edible vegetable oil and its smoke condensation oil.

用TBA-醋酸法检测正常人血清，血浆，胸腹腔渗、漏出液，各细胞提取物及服用西洋参前后的血浆和经过氧化处理后的正常人、糖尿病、高血压、冠心病患者的血清及食用油脂、相应烟雾冷凝油的过氧化脂质含量。

What would he tell Judith and the children?

他将怎样告诉朱迪丝和孩子们呢？

I this is at that time, the opinion with peacockish true girl is full of in a heart.

这就是当时的我，一个心中布满虚荣的女孩子真实的想法。