查询词典 condensation

2 Condensation of ketones with ethyl cyanoacetate catalysed by ammonium acetate-acetic acid results ethyl alkylidene cL-cyanoacetate in 3 l?.-89% yield under ultrasound irradiation at 4l-450C within

在超声波作用下，以芳香醛和丙二酸为原料，以膨胀石墨作催化剂，合成多种肉桂酸，于41～43℃反应3.5-10小时，产率65-97％。

This thesis mainly studied on sulfamic acid catalyzed Cross-Aldol condensation, direct amidation of benzhydryl alcohol; solid base catalyzed synthesis of bisindoles was also discussed.

本论文主要讨论了磺氨酸催化下的Cross-Aldol反应；二苯甲醇的胺化反应；固体碱氟磷灰石催化的双吲哚甲烷衍生物的合成。

The condensation of 3 carbethoxy isoquinol 4 one with carbamidine, amidine, carbamide and sulfocarbamide gave isoquinolo pyrimidine derivatives, respectively and isoquinolo quinoline derivatives were synthesized by the reaction of o aminobenzaldehyde or o aminopiperonal with isoquinol 4 one.

报道了利用 3 乙氧甲酰基异喹啉 4 酮分别与胍、脒、脲及硫脲类化合物缩合反应合成异喹啉并嘧啶衍生物，邻氨基苯甲醛、邻氨基胡椒醛分别与异喹啉 4 酮反应合成异喹啉并喹啉化合物。6个新化合物的结构通过元素分析、红外光谱、核磁共振氢谱和质谱予以证

The technology uses row materials of o aminobenzoic sulfonic acid, cyanuric fluorine, sodium carbonate etc. and the process contains diazotization, coupling, condensation, salting out, dring etc.

此项技术是以邻氨基苯磺酸、三聚氟氢、碳酸钠等为原料，经过重氮化、偶合、缩合、盐析、干燥等工艺过程，生产出新型活性染料。

The analogs of piracetum with the core of demethylclausenamide(III-4 and III-5) were prepared by condensation of demethylclausenamide with ethyl bromoacetate and hydrolysis or aminolysis there after.

3在兰培工作的基础上，选用O-乙酰-R--扁桃酸为拆分剂，成功的拆分了表黄皮酰胺前体5--4-苯基-1-甲基吡咯烷酮(Ⅱ-1)，和Ⅱ-1分别引入3位羟基得到和表黄皮酰胺。

In part one, the reactions of some active fluorine-containing compounds such as 2, 2-dihydropolyfluoroalkanoic acids and ethyl 2-hydropolyfluoroalkenoates were studied and various fluorine-containing heterocyclic compounds were synthesized. Using 2, 2-dihydropolyfluoroalkanoic acids as the starting material, 4-fluoroalkyl quinolin-2-ols, 2- [ -1-hydropolyfluoro-1-alkenyl] -4H-3, 1-benzoxazin-4-ones, 1-aryl -4, 9-dihydro-3-fluoro-alkyl-1H-pyrazo [3, 4-b] quinolin-4-ones, 5-fluoroalkyl-12H-quin olino [2, 1-b] quinazolin-12-ones, 4-fluoroalkyl-1, 3-dihydro-1, 5-benzodiazepin-2-ones and 4-fluoroalkyl-2H-pyrido [1, 2-a] pyrimidin-2-ones were synthesized through its condensation reaction with anilines, anthranilic acid, N'-aryl-o-aminobenzamides, o-nitro aniline, o-amino pyridine and their derivatives and the subsequent transformations. 5-Fluoroalkyl isoxazolidines, 3-fluoro-3-fluoroalkylisoxazolidino [4, 3-c] quinolin-4-ones, 3-fluoroalkylisoxazolino [4, 3-c] quinolin-4-ones and 2-aryl-3per fluoroacylindoles were synthesized by inter-and intramolecular 1, 3-dipolar cycloaddition of fluorine-containing olefins and nitrones.

第二部分，我们研究了α，α-二氟苄基卤类化合物的亚磺化脱卤反应、产物的转化及全氟烷基亚磺酸盐与芳环化合物的全氟烷基化反应，发现全氟苄基碘或溴及α，α一二氟苄基溴在保险粉等亚磺化脱卤试剂引发下可生成相应的亚磺酸盐；全氟苄基亚磺酸盐与氯气或溴反应可生成全氟苄基磺酰氯或磺酰溴；在烯烃存在下，全氟苄基碘则与烯烃发生加成反应，生成相应的1：1加成产物；在三价醋酸锰的作用下，部分芳香化合物如茴香醚，二甲氧基苯，吡啶，喹啉等可以和过量的全氟烷基亚磺酸盐发生双全氟烷基化反应，反应表现出一定的区域选择性，产率良好。

The dehydration reaction between squaric acid and primary arylamine are easity formed when heated in H_2O or H_2ODMSO(1∶2,Volume ration),it is quite different from the normal condition of dehydration condensation reactions.

与通常的脱水缩合反应条件不同，而以H2O或以H2ODMSO（1∶2，体积比）为介质，加热下方酸与芳伯胺之间可顺利实现脱水反应。

In the presence of ethanol- HCl solution, arylamine-HCl and w=37% aqueous formaldehyde solution or the condensation product of arylamine and formaldehyde are directly reacted with ethyl 3-oxo-2-phenylmethylenebutyrate to form l-aryl-2-phenyl-3-carbethoxy-4-piperidone.

2－苯亚甲基－3－丁酮酸乙酯与芳香胺和w＝37％甲醛水溶液或芳胺和甲醛的缩合物在氯化氢－无水乙醇存在下可直接发生的Mannich反应，得到1－对位取代芳基－2－苯基－3－羰乙氧基－哌啶－4－酮。

In the present study, tungsten oxide nanomaterials were synthesized by a modified plasma arc gas condensation technique. The effects of the plasma currents (70~90 A), chamber pressures (200~600 torr), production time（3~12 min）, oxygen partial pressure Ar:O2（1~6:1）and plasma including the hydrogen（0~10 %）on the preparation of tungsten oxide nanostructures were investigated. Pre-treatment on the tungsten oxide nanorods for surface modification was investigated by atmospherical plasma jet. The optical, filed emission, and gas sensing characteristics of tungsten oxide nanopowders were also examined.

本研究系利用电浆电弧气凝合成法来制备氧化钨奈米材料，分别探讨不同腔体压力（200~600 torr）、电浆电流（70~90 A）、制备时间（3~12 min）、氧分压Ar：O2（1~6：1）、电浆气含氢量（0~10 %）对於产物的形貌、相态影响，并使用常压低温电浆设备对氧化钨奈米棒进行表面处理，且针对氧化钨奈米材料的光学、场发射以及使用自行组装气体感测量测设备量测其气体感测特性。

Methods:We adopted the syndrome of blood stasis model of chronic myocardial ischemia by laying the Ameroid condensation ring surrounded the origainate region of the first septum of animals' front-fall branch of left coronary attery as the integrate illness with syndrome.

采用病证结合的方法即动物左冠状动脉前降支第一间隔支起始部远端放置Ameroid缩窄环的方法复制慢性心肌缺血血瘀证模型。

What would he tell Judith and the children?

他将怎样告诉朱迪丝和孩子们呢？

I this is at that time, the opinion with peacockish true girl is full of in a heart.

这就是当时的我，一个心中布满虚荣的女孩子真实的想法。