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Then studied on several clays affect on the stability of ferrate solution. The results show the addition of clays retarded the decomposition of ferrate in alkaline solution. Through analysed the results of test, we found this due to the silicium or polysilicium of clays and its increasing stabilizing effect on ferrate when the concentration of silicium or polysilicium increases.

接着作了粘土对高铁酸盐溶液的稳定作用的研究,结果表明粘土对高铁酸盐溶液有良好的稳定作用,通过实验分析得到其稳定作用是由于粘土中溶出的硅酸根或多聚硅酸根所致,且随着其浓度的增加对高铁酸盐的稳定作用增强。

METHODS: The concentration of ozone that was transmitted by ozone generator at different time was determined by using iodine titrimetric method. According to the bactericidal assay of quantitative vehicle, the bacteria on the ozonized vehicles and unozonized vehicles was washed, 50μl eluant was seeded on the TSA plates. The TSA plates were put into the anaerobiotic incubator (90% N2, 10% CO2, 37℃). After 24 to 48 hours, the CFU on the plate was counted.

用碘滴定法测定打开臭氧发生器不同机组及不同时间时的臭氧浓度,按载体定量杀菌试验,将经臭氧作用的载体与相同环境下未经臭氧作用的载体上的细菌洗下,各取洗脱液50μl,接种于TSA平板并置厌氧箱(90%N2, 10%CO2, 37℃)培养24~48h后,进行活菌菌落计数。

More and more attention is focusing on the safty of drinking water suply. In this paper, firstly, chloramine formation and the characteristics and kinetics of monochloramine autodecomposition were studied. Secondly, considering the high concentration of ammonia and the complication of organic matters in Shanghai Huangpu River, formation characteristics and rules of disinfection byproducts were reviewed during the breakpoint chlorination process, and on the basis of grading and clssification of organisms, the control effects of chloramination on DBPs formation were studied. Finally, the formation rules of 2-monochlorophenol, 2,4-dichlorophenol and 2,4,6-trichlorophenol from phenol chlorination were investigated, and related influencing factors and kinetics were analysed.

饮用水的安全供给受到越来越多的重视,本文首先进行了氯胺形态以及一氯胺自降解特性及其动力学研究;然后结合上海黄浦江水源氨氮浓度高、有机物成分复杂的特点,研究折点加氯过程中消毒副产物的生成特性和规律,以及在将有机物分级和分类的基础上,研究氯胺消毒对不同类别有机物生成消毒副产物的控制效果;最后考察了氯化苯酚生成2-一氯酚(2-MCP)、2,4-二氯酚(2,4-DCP)及2,4,6-三氯酚(2,4,6-TCP)的规律,并进行了影响因素和动力学分析。

It caused aggregation of purple membrane fragments at very low concentration. This effect might be attributed to its positive charges because cationic surfactant DTAB acted the same. On the other hand, melittin seemed to have behavior similar to CHAPS which has a rigid cholane ring,both had little effect on the conformation of retinal chromporphores.In consideration of the two-dimensional crystalline structure of purple membrane,melittin may form a rigid conformation such as α-helix on the surface of the membrane.

通过与三种在结构和电荷上不同的表面活性剂与紫膜的作用相比较,可以年出蜂毒作为带正电荷的分子与同样带正电的表面活性剂DTAB在引起紫膜凝聚方面表现相同;但在对紫膜可见光区的吸收光谱和圆二色谱的影响上却与具有刚性结构的CHAPS相似,表明蜂毒可在紫膜表面以一种刚性较大的构象存在,不能进入膜蛋白流水区的深层。

By flue gas of 2000m〓/h, some normal wastes (seawater, fly ash of power plant, basic waste water, etc) and lime are used on the research of dry, semi-dry, and wet FGD and its corresponding pressure and temperature decrease on stuffing tower, the effect of Ca/S ratio, inlet SO2 concentration, inlet flue gas temperature, and L/G ratio on desulfuration efficiency is analyzed, the instrument of dehumidify was studied by experiment and appropriate instrument of dehumidify was chosen.

在浙大热能所大约相当于1吨/小时出力的锅炉的尾部烟道上的多功能传热除尘脱硫一体化试验研究装置上,利用海水、电厂灰、碱性废水和石灰开展了半工业性的干法、半干法、湿法烟气脱硫研究,分析了Ca/S比、进口SO〓浓度、进口烟温、喷水量等因素对脱硫效率的影响,并探讨了湿法烟气脱硫中的烟温问题,对湿法烟气脱硫反应塔的阻力特性和除湿装置进行了试验研究,选取了合适的除湿元件。

Low concentration of NaCl solution could promote the growth on the shoot of seed germination. The growing length of roots and shoots of two halophytes treated by 100 mmol·L~(-1) NaCl reached the highest and the growing condition on shoots was best. Then some physiological and biochemical parameters including the content of Na~+, K~+, Ca~(2+), proline and plant leaf tissue water potential, the assays of membrane lipid peroxidation and antioxidant enzymes were determined with the two halophytic plants on salinity.

研究工作首先对盐爪爪和盐穗木在种子萌发阶段的耐盐性进行了比较研究,表明盐爪爪和盐穗木都是很耐盐的盐生植物,在种子萌发期,盐穗木比盐爪爪更耐盐;NaCl和等渗的聚乙二醇对种子的萌发都产生抑制作用,且PEG的抑制程度大于等渗的NaCl。

In the sixth chapter, according to our nations situations, a probing study on the development and application of natural mordenite was carried out at the aim to develop a new adsorbent carrier and reduce the cost of adsorbent preparation. The characters of natural mordenite were chemically changed by an acid. The effects of the acid solution concentration, temperature, mordenite size and treatment times on the physico-chemical characters of mordenite were undertaken. The adsorption equilibrium of CO on the character-changed natural mordenite was measured.

在第六章中,结合我国的实际情况,对天然丝光沸石的开发利用进行了探索性的研究,期望开发一种新的吸附剂载体,以降低吸附剂的制备成本,为此,对天然丝光沸石进行了酸化学改性,研究了酸溶液和浓度、温度和沸石粒度以及处理次数对丝光沸石物理化学性质的影响,测定了CO在改性丝光沸石上的吸附平衡。

Based on relative literatures,this part has included five resesearch aspects as below.1 Fifteen compounds were isolated and purified by extraction,column chromatography,and their structures were determined on the basis of spectral analysis: acteoside(Ⅰ-1),isoacteoside(Ⅰ-2),crenatoside(Ⅰ-3),cistanoside F(Ⅰ-4),sinapoyl-4-O-β-D-glucoside(Ⅰ-5),adenosine(Ⅰ-6),β-siterol(Ⅰ-7),oleanic acid(Ⅰ-8), succinic acid(Ⅰ-9),caffeic acid(Ⅰ-10),protocatechuic aldehyde(Ⅰ-11),p-hydro xybenzyl alcohol(Ⅰ-12),β-daucosterol(Ⅰ-13),D-galacitol(Ⅰ-14),D-mannitol(Ⅰ-15).Ⅰ-4~15 were obtained from this plant for the first time,andⅠ-6,7,9,and 13 were isolated from Orobanche genus for the first time.2 The scavenging test of DPPH showed that most compounds have comparative antioxidant activity as L-ascorbic acid and part of them show better activity such as the O.coerulescens extract and phenylethanoid glycosides.Acteoside showed potent free radical scavenging effects with a median inhibition concentration of 25.6μg/ml.3 The anti-HBV activities of acteoside,isoacteoside and crenatoside were measured,and all of them showed suppressive activity on the expression of HBsAg and HBeAg in the HepG2.2.15 cell line.

本论文在文献调研基础上对紫花列当化学成分及生物活性进行了研究,并从免疫抗病毒角度探讨紫花列当中特征性成分类叶升麻苷的肝保护作用及其机制。1采用大孔树脂、硅胶和Sephadex LH-20等色谱技术对紫花列当进行系统的植物化学研究,从中分离得到19个化合物,利用UV和NMR等波谱手段及理化性质鉴定了其中的15个化合物,分别为类叶升麻苷(Ⅰ-1)、异类叶升麻苷(Ⅰ-2)、crenatoside(Ⅰ-3)、cistanoside F(Ⅰ-4)、sinapoyl-4-O-β-D-glucoside(Ⅰ-5)、腺苷(Ⅰ-6)、β-谷甾醇(Ⅰ-7)、齐墩果酸(Ⅰ-8)、琥珀酸(Ⅰ-9)、咖啡酸(Ⅰ-10)、原儿茶醛(Ⅰ-11)、对羟甲基苯甲酸(Ⅰ-12)、β-胡萝卜苷(Ⅰ-13)、D-半乳糖醇(Ⅰ-14)和甘露醇(Ⅰ-15除化合物Ⅰ-1、Ⅰ-2和Ⅰ-3外,其余化合物均为首次从该植物中分离得到。2)通过大孔树脂富集该药材有效部位苯乙醇总苷,并采用HPLC测得其所含特征性成分类叶升麻苷的含量可达80%以上。3DPPH自由基清除试验显示紫花列当提取物及其所含的苯乙醇苷类化合物均具有较好的抗氧化能力,其清除DPPH自由基能力接近于抗坏血酸。4采用卡介苗整体致敏、脂多糖离体攻击构建大鼠原代肝细胞免疫性损伤模型,在体外观察类叶升麻苷的保肝作用。

The results showed that 0.01,0.05 and 0.10 g/ml extract of Saxifraga stolonifera Meerb had strong antimicrobial effect on S.aureus,but 0.25 and 0.50 g/ml extract had promotive effect on S.aureus.And the extract of Saxifraga stolonifera Meerb of different concentration had antimicrobial effect on E.coli.

结果表明,0.01、0.05、0.10g/ml 3种较低浓度的提取物对摇床培养的金黄色葡萄球菌生长具有较强的抑制作用,而0.25和0.50g/ml 2种较高浓度的提取物对摇床培养的金黄色葡萄球菌生长有较强的促进作用;这5种浓度的提取物均对摇床培养的大肠杆菌生长表现为抑制作用。

The researching content was as follows: 1. When AlClx/HY zeolite be used as catalyst, the effects of the ratio of 2-methylnaphthalene to tetramethyl benzene, catalyst concentration, reaction temperature and reaction time on the conversion (based on 2-methylnaphthalene), yield and selectivity (both based on 2,6-DMN) were discussed. In addition, by orthogonal experiment, the optimum reaction conditions were determined at the same time. The optimum reaction conditions : the molar ratio of 2-methylnaphthalene and tetramethyl benzene =1:1, reaction temperature was 400℃.

具体研究如下: 1、以AlClx/HY型分子筛为催化剂,研究原料配比(2-甲基萘与均四甲苯的摩尔比)、反应温度和反应时间对2-甲基萘的转化率、目的产物2,6-DMN的收率和选择性的影响,并通过正交实验确定了该催化剂体系下的最佳反应条件为:原料的摩尔比为(2-甲基萘:均四甲苯)=1:1,反应质量空速为6h-1,反应温度为400℃。

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In the negative and interrogative forms, of course, this is identical to the non-emphatic forms.

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