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Some conclusions were drawn: Oenanthe javanica grew normally when TN and TP concentrations in raw water were 7.05-9.99 mg/L and 0.29-0.73 mg/L respectively; with the hydraulic load being 0.5 m^3/(m^2d), the removal rates of NH3-N, TP, and TN from heavily polluted river water by Oenanthe javanica floating bed were positively related to water temperature, and it inhibited the growth of algae stably; the mean removal rate of nutritive salt increased with the concentration of raw water.

研究结果表明,进水ρ和ρ分别为7.05~9.99mg/L和0.29~0.73mg/L,水芹菜能正常生长,在水力负荷为0.5立方公尺/的条件下,水芹菜浮床对重污染河水中的NH3-N,TP,TN的去除率与水温正相关,对藻类的抑制作用稳定;营养盐的去除负荷随原水质量浓度的增加而增大。

The changing trend of progesterone during oestrous cycle resembles with that during the first 14d of early pregnancy. Its content reaches the peak value at lOd after oestrus and then declines. The estradiol peak appears at 3d of oestrous cycle, and the level rises again before oestrus. The concentration of LH declines after oestrus. The level of follicle stimulating hormone reaches the peak value at lOd after oestrus (2.40mIU/ml).

发情周期:民猪发情周期孕酮的含量与妊娠早期14天内的变化极其相似,在发情后第10天达峰值,而后开始下降;雌二醇水平在发情后第3天出现高峰,下次发情前开始升高;促黄体素在发情当天达最高水平,然后开始下降;促卵泡素在发情后的第10天达到峰值(2.40mIU/ml)。

Anaerobic biological deodorization system was able to work steadily even when COD concentration of influents reached 10000mg/L, olfactometry measurement was fitted 5-grade standard and volumetric loading rates were 10.58Kg. COD/; In the two combined UASB systems, Hydraulic Retention Time of the first UASB was 28h, olfactometry measurement of effluents was fitted 3-grade standard; and when HRT of the second UASB was 67h, olfactometry measurement was below 2-grade.

COD〓,厌氧反应器可稳定运行,并具有优良的除臭性能;对两级串联的UASB系统,一级水力停留时间为28h时,出水臭气强度可达3级;二级水力停留时间为67h时,二级出水臭气强度可在2级以下。

Based on relative literatures,this part has included five resesearch aspects as below.1 Fifteen compounds were isolated and purified by extraction,column chromatography,and their structures were determined on the basis of spectral analysis: acteoside(Ⅰ-1),isoacteoside(Ⅰ-2),crenatoside(Ⅰ-3),cistanoside F(Ⅰ-4),sinapoyl-4-O-β-D-glucoside(Ⅰ-5),adenosine(Ⅰ-6),β-siterol(Ⅰ-7),oleanic acid(Ⅰ-8), succinic acid(Ⅰ-9),caffeic acid(Ⅰ-10),protocatechuic aldehyde(Ⅰ-11),p-hydro xybenzyl alcohol(Ⅰ-12),β-daucosterol(Ⅰ-13),D-galacitol(Ⅰ-14),D-mannitol(Ⅰ-15).Ⅰ-4~15 were obtained from this plant for the first time,andⅠ-6,7,9,and 13 were isolated from Orobanche genus for the first time.2 The scavenging test of DPPH showed that most compounds have comparative antioxidant activity as L-ascorbic acid and part of them show better activity such as the O.coerulescens extract and phenylethanoid glycosides.Acteoside showed potent free radical scavenging effects with a median inhibition concentration of 25.6μg/ml.3 The anti-HBV activities of acteoside,isoacteoside and crenatoside were measured,and all of them showed suppressive activity on the expression of HBsAg and HBeAg in the HepG2.2.15 cell line.

本论文在文献调研基础上对紫花列当化学成分及生物活性进行了研究,并从免疫抗病毒角度探讨紫花列当中特征性成分类叶升麻苷的肝保护作用及其机制。1采用大孔树脂、硅胶和Sephadex LH-20等色谱技术对紫花列当进行系统的植物化学研究,从中分离得到19个化合物,利用UV和NMR等波谱手段及理化性质鉴定了其中的15个化合物,分别为类叶升麻苷(Ⅰ-1)、异类叶升麻苷(Ⅰ-2)、crenatoside(Ⅰ-3)、cistanoside F(Ⅰ-4)、sinapoyl-4-O-β-D-glucoside(Ⅰ-5)、腺苷(Ⅰ-6)、β-谷甾醇(Ⅰ-7)、齐墩果酸(Ⅰ-8)、琥珀酸(Ⅰ-9)、咖啡酸(Ⅰ-10)、原儿茶醛(Ⅰ-11)、对羟甲基苯甲酸(Ⅰ-12)、β-胡萝卜苷(Ⅰ-13)、D-半乳糖醇(Ⅰ-14)和甘露醇(Ⅰ-15除化合物Ⅰ-1、Ⅰ-2和Ⅰ-3外,其余化合物均为首次从该植物中分离得到。2)通过大孔树脂富集该药材有效部位苯乙醇总苷,并采用HPLC测得其所含特征性成分类叶升麻苷的含量可达80%以上。3DPPH自由基清除试验显示紫花列当提取物及其所含的苯乙醇苷类化合物均具有较好的抗氧化能力,其清除DPPH自由基能力接近于抗坏血酸。4采用卡介苗整体致敏、脂多糖离体攻击构建大鼠原代肝细胞免疫性损伤模型,在体外观察类叶升麻苷的保肝作用。

The catalytic transformation pathway can change to decrease the yield of hydrogen and yield methyl-contained sulfides such as methyl mercaptan, dimethyl sulfide and dimethyl disulfide, but overlarge concentration of methanol would holdback the transformation of isobutyl mercaptan. The transformation of isobutyl mercaptan was favorable if the volume ratio of methanol and benzene was 0.2.The addition of methanol assume certain effect on the catalytic cracking of di-n-butyl sulfide in solvent benzene but without changing the cracking reaction mechanism of di-n-butyl sulfide.

甲醇也可以使异丁硫醇的催化转化路径发生改变降低硫化氢的产率,生成甲硫醇、甲硫醚及二甲基二硫化物等含甲基硫化物,但甲醇的浓度过高会抑制异丁硫醇的转化,在反应体系中当甲醇的体积占到溶剂苯体积的20%时对异丁硫醇的转化较为有利;甲醇的添加对丁硫醚在溶剂苯中的催化裂化有一定影响,但没有改变丁硫醚的裂解反应历程。

In this research, we prepared Mo doped ZnO thin films on glass a substrate using co-sputtering to improve the conductivity of ZnO. The incorporated concentration of Mo atoms in ZnO was controlled by adjusting the aperture size of a shutter palaced in front of the Mo target. Textured morphology of ZnO film could be formed by attaching a metallic mask on the substrate.

本研究,欲以钼(Molybedeun, Mo)金属掺杂来提升氧ZnO薄膜之导电性,使用一般玻璃做为基板,利用射频溅射ZnO靶材及直流溅射Mo靶材进行共镀,Mo掺杂浓度是藉由钼靶前之挡板中的开口大小来控制,实验中改变基板温度(50℃、100℃、200℃、300℃)并进行镀膜后低压退火处理,藉此探讨Mo掺杂对於ZnO薄膜光电特性之影响,并找出最佳化制程参数。

On the basis of proving the influence of temperature,concentration of solution and stiring intension to the granularity of ammonium paratungstate,micron-level APT.

在探明温度、溶液浓度,搅拌强度对仲钨酸铵粒度影响的基础上,研究了表面活性剂制备微米级仲钨酸铵的工艺。

The minimal bactericidal concentration of PTKE on Escherichia coli, Staphylococcus aureus, Salmonella, Pasteurella multocida and Streptococcus agalactiae were 100, 25, 50, 25 and 50 mg/mL respectively. The isolation of EA, EB and EC had no antibacterial effect on Escherichia coli and Pasteurella multocida. MBC of EA on Staphylococcus aureus and Salmonella were 2.5 and 5 mg/mL, and MBC of EB on Staphylococcus aureus, Salmonella and Streptococcus agalactiae were 1.25, 5 and 2.5 mg/mL respectively, while MBC of EC on Staphylococcus aureus was 2.5 mg/mL. Polygonum taibaishanense Kung.

PTKE对大肠埃希菌、金黄色葡萄球菌、沙门氏菌、多杀性巴氏杆菌和无乳链球菌的最低杀菌浓度分别为100,25,50,25和50 mg/mL;而PTKE的分离物EA、EB和EC对大肠埃希菌和巴氏杆菌无抑菌作用,EA对金黄色葡萄球菌、沙门氏菌的MBC分别为2.5和5.0 mg/mL,EB对金黄色葡萄球菌、沙门氏菌和无乳链球菌的MBC分别为1.25,5.0和2.5 mg/mL,EC对金黄色葡萄球菌的MBC为2.5 mg/mL。

With the increase of concentration of aqueous extract from Peganum multisectum increased, root vigor, the contents of chlorophyll, soluble protein and nucleic acid in roots and shoots of alfalfa seedlings decreased, while the activities of protease and nuclease, the contents of O2ˉ, H2O2 and malondiadehyde increased, the activities of superoxide dismutase, catalase and peroxidase first increased and then decreased.

幼苗根系活力和叶绿素、可溶性蛋白质、核酸含量随水浸液浓度的提高而降低,蛋白酶和核糖核酸酶活性及超氧阴离子(O2ˉ)、H2O2和丙二醛含量则增加,超氧化物歧化酶、过氧化氢酶和过氧化物酶活性呈先升后降变化。

The regularities of the influence of various factors includingreaction temperature,reaction time,the ratio of formaldehyde to acetaldehyde,the quantity of alkali and the concentration of formaldehyde on the yieldsof pentaerythritol and dipentaerythritol were studied.

通过单因素实验,考察了反应温度、反应时间、甲醛与乙醛的配比等因素对单、双季戊四醇收率的影响。

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