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The diluent solution of glyoxylic acid and oxalic acid was used as the separation object.TOA (in n-octanol) was used as the solvent. The extraction characteristics of single acid and two-acid solution were studied,and the influence of pH and the concentration of complexing agent on the distribution coefficients were measured. The suitable mathematic models were proposed to describe the relationship between TOA and carboxylic acid based on assumed extraction reaction in organic phase.

摘 要:以草酸和乙醛酸的稀溶液为分离对象,采用三辛胺为萃取反应剂、正辛醇为稀释剂,研究了单溶质、双溶质有机酸的萃取分离特性,测定了溶液pH值、萃取反应剂的浓度等因素对双溶质有机酸萃取的影响,提出了萃取的化学反应发生在有机相中的假定,建立了TOA萃取草酸的数学模型。

The diluent solution of glyoxylic acid and oxalic acid was used as the separation object. TOA (in n-octanol) was used as the solvent. The extraction characteristics of single acid and two-acid solution were studied, and the influence of pH arid the concentration of complexing agent on the distribution coefficients were measured. The suitable mathematic models were proposed to describe the relationship between TOA and carboxylic acid based on assumed extraction reaction in organic phase.

以草酸和乙醛酸的稀溶液为分离对象,采用三辛胺为萃取反应剂、正辛醇为稀释剂,研究了单溶质、双溶质有机酸的萃取分离特性,测定了溶液pH值、萃取反应剂的浓度等因素对双溶质有机酸萃取的影响,提出了萃取的化学反应发生在有机相中的假定,建立了TOA萃取草酸的数学模型。

By analyzing these data,it was concluded that:1The combustion of wood,including rate of heat release,total heat release,effective heat of combustion,mass loss rate,smoke ratio,specific extinction area,concentration of CO_2 and the yield of CO_2Y_(CO2,were decreased considerably by the treatment of FRW;2There is a strong synergistic effect of fire retardance between GUP and boric acid;3The trend of MLR curve of FZ was similar to its RHR curve,weight loss and heat release were happened mainly in flaming phase;4Char formation of wood was markedly accelerated by FRW,which indicated that catalytic charring effect of FRW on wood is the primary side in its fire-retardation mechanism.

对于组成和结构变异性很大的木材而言,由于CONE实验所使用的样品量相对于其他分析方法要大得多,因而实验结果比较有代表性。此外,CONE实验可在模拟火灾条件下进行,这是该方法的又一突出的优点[5~6]。木材阻燃剂FRW主要由磷酸脒基脲和硼酸组成,此外还含有

Low concentration of NaCl solution could promote the growth on the shoot of seed germination. The growing length of roots and shoots of two halophytes treated by 100 mmol·L~(-1) NaCl reached the highest and the growing condition on shoots was best. Then some physiological and biochemical parameters including the content of Na~+, K~+, Ca~(2+), proline and plant leaf tissue water potential, the assays of membrane lipid peroxidation and antioxidant enzymes were determined with the two halophytic plants on salinity.

研究工作首先对盐爪爪和盐穗木在种子萌发阶段的耐盐性进行了比较研究,表明盐爪爪和盐穗木都是很耐盐的盐生植物,在种子萌发期,盐穗木比盐爪爪更耐盐;NaCl和等渗的聚乙二醇对种子的萌发都产生抑制作用,且PEG的抑制程度大于等渗的NaCl。

The hematolysis rate and biologic immunocompetence of pns-5 were detected with hemolysis test and experiment of splenocyte proliferation respectively.results:the hd50 of pns-5 was bigger than 8 mg/ml and it significantly increased concanavalin a and lipopolysaccharide-stimulated splenocyte proliferation in vitro in a concentration of 0.1 μg/ml.

结果:pns-5溶血性较小,其hd50大于8 mg/ml;pns-5(0.1 μg/ml)显著促进了con a和lps诱导的小鼠脾淋巴细胞增殖反应。结论:pns-5安全性好,能促进细胞和体液免疫。

With the theory of Hydrophile-lipophile Balance, it is found that the most suitable anion surfactant for preparation of PPy is heptanoic acid, and get a conclusion that there is a best matching relation between the concentration of surfactant and the state of the porous substrate.

根据亲水亲油平衡理论,找出了最适合制备聚吡咯薄膜的阴离子表面活性剂——庚酸,并且通过试验得出了表面活性剂浓度与基底不同的多孔状态存在最佳匹配关系的结论。

The optimum synthetic conditions of hexadecanoic acid diethanolamide used two-step method are as follows:(1)reaction temperature was 140℃, reaction time was 4.5hours and molar ratio of hexadecanoic acid to diethanolamide was 1:1.15.(2)reaction temperature was 80℃, molar ratio of hexadecanoic acid to diethanolamide was 1:1.55 and mass concentration of the catalyst was 0.8%, reaction time was 3 hours.

二步法合成十六酸二乙醇酰胺最佳合成工艺为:(1)反应温度140℃、反应摩尔比n十六酸∶n二乙醇胺=1∶1.15、反应时间4.5h;(2)反应温度80℃、反应总摩尔比n十六酸∶n二乙醇胺=1∶1.55、催化剂用量0.8%、反应时间3h。

To further investigate their roles in cell proliferation apoptosis and differentiation, three human leukemia cell lines (K562, U937 and HL60) exposed to various concentration of hexamethylene bisacetamide, a potent inducer of differentiation of transformed cells both in vivo and in vitro, were used as an in vitro model for the study of cell proliferation, differentiation and apoptosis.

为了进一步研究cyclin A和p21在白血病细胞增殖,分化,凋亡中的作用,我们用在体内,外均有抗肿瘤作用的药物六亚甲基二乙酰胺在体外抑制白血病细胞株K562,U937和HL60增殖,诱导其分化,成功地建立了与药物干预浓度呈剂量-效应关系的,具有不同增殖,分化,凋亡状况的实验细胞模型。

The kinetic behaviors of ethylene homo- olymerization and ethylene / l-hexene co-polymerization , catalyzed by the metallocene catalyst PS-DVB-MC in an 0.5 L stainless steel reactor , were studied. The effects of polymerization conditions on ethylene polymerization , such as concentration of catalyst , temperature of polymerization , pressure of ethylene , molar ratio of AI / Z r , etc ., were also investigated . Some leading results were as follows : the activity of the catalyst PS–DVB- MC for ethylene homo-polymerization was high ( 1.053 x 107 gPE / mol Zr·h ), but the molar ratio of AI / Zr was low ( 350:1 ); the catalytic ability for ethyleneα-olefin ( such as l hexene etc .) co-olymerization was great , and the corresponding activity come up to a maximum of 1.753 x 107 gPE / mol Zr·h while concenlration of l-hexene was 0.080 mol / L ; the molecular weight of polyethylene was about 180,000 , meanwhile the molecular weight distribution was narrow ( 2.19 ); the bulk density of polyethylene and ethylene / l-hexene co -polymer were 0.25 and 0.34 respectively .

采用0.5L高压不锈钢反应釜,对催化剂PS–DVB-MC催化乙烯均聚和乙烯/ l-己烯共聚合的动力学行为进行了研究,详细考察了催化剂浓度、反应温度、压力、Al/ Zr比、1-己烯浓度等因素对乙烯聚合反应的影响,得到如下主要结论:催化剂PS-DVB-MC具有催化乙烯均聚的高活性(1.053×107g PE / mo1 zr.hr),低Al / Zr比( 350:1 );具有良好的催化乙烯与α-烯烃(如1-己烯等)共聚的能力,在1-己烯浓度为0.080 mol / L时,催化活性达到最大(1.783×107 g PE / molZr.hr);乙烯均聚产物的分子量在18万左右,分子量分布窄( 2.19 )。

AIM: From the views of biochemistry, histology and molecular biology, this study observed the effects of 4-6 Hz vibration on concentration of hexosamine, the expression of mucin 5AC mRNA in gastric mucosa and histomorphology, and investigated the effects of body vibration on rats' gastric mucus secretion and mucosal structure.

邓 艳,陈伟华,宋小丹,张源淑南京农业大学动物医学院,农业部生理生化重点开放实验室,江苏省南京市 210095目的:从生物化学、组织学和分子生物学角度观察4~6 Hz振动对大鼠胃黏膜氨基己糖含量、黏蛋白5AC mRNA表达及其组织形态学变化,探讨振动对大鼠胃黏膜黏液分泌及形态的影响。

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