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To be different from the already chloromethylation catalyst, it has a certain amount of moisture wet, which will not produce huge amounts of doughtic cancerogenic chloromethyl methyl ether during and after the reaction.4,4\'-bisbiphenyl, 1,4-bisbenzene, 1,4-bis(chloro- methyl)-2,5-dimethylbenzene, 1,5-bis-2,4-dimethylbenzene, 4-(chlor- omethyl)-1,2-dimethylbenzene, 1,2-bis-4,5-dimethylbenzene, 5,8-bis-1,2,3,4-tetrahydronaphthalene, 3,3\',5-tris-4,4\'-bisbiphenyl and 3,3\', 5,5\'-tetrakis-4,4\'-bisbiphenyl were synth- esized by using this new catalyst. Results indicated that when the reaction temperature was 55～60℃, the reaction time was 12h, the catalyst which consists of the concentration of 80%H_2SO_4, HAc and Lewis acid, the amount of Lewis acid 0.15 mol(nLewis:nbiphenyl=1.5:1), yield of biphenyl chloromethylation product 4,4\'-bis(chrolomethylbiphenyl can reach a maximum 85%.

采用这种催化体系完成了4，4′-二氯甲基联苯、对二氯甲基苯、1，4-二氯甲基-2，5-二甲基苯、1，5-二氯甲基-2，4-二甲基苯、4-氯甲基-1，2-二甲基苯、1，2-二氯甲基-4，5-二甲基苯、5，8-二氯甲基-四氢萘、3，3'，5-三氯甲基-4，4'-二甲基苯和3，3'，5，5'-四氯甲基-4，4'-二甲基苯的合成，结果表明：在反应条件为：反应温度55～60℃，反应时间12h，选择80%H_2SO_4、冰醋酸和Lewis酸为催化剂，反应最佳反应Lewis酸用量是0.15mol(和原料比为1.5：1)，反应效果最好，联苯氯甲基化产物(4，4′-二氯甲基联苯)收率为85%；在反应条件为：反应温度70℃，反应时间8h，80%H_2SO_4、冰醋酸和Lewis酸为催化剂，反应最佳反应Lewis酸用量是0.1mol(和原料比为1：1)时，反应效果最好，苯的氯甲基化产物收(来源：ABd0C论文eded网www.abclunwen.com)率为75%；在反应条件为：在反应条件为：反应温度40℃，反应时间10h，60%H_2SO_4和Lewis酸为催化剂，反应最佳反应Lewis酸用量是0.1mol(和原料比为1：1)时，反应效果最好，对二甲苯氯甲基化产物(1，4-二氯甲基-2，5-二甲基苯)收率为78.5%；在反应条件为：反应温度35℃，反应时间10h，60%H_2SO_4、冰醋酸和Lewis酸为催化剂，反应最佳反应Lewis酸用量是0.1mol(和原料比为1：1)时，反应效果最好，间二甲苯氯甲基化产物(1，5-二氯甲基-2，4-二甲基苯)收率为81.5%。

The dependence of concentration of free sodium hydroxide,hydrolyzation ratio of sodium chloroacetate,degree of substitutionand solution viscosity of product on reaction conditions in the synthesis of polyanionic cellulosein various alcohol mediums are studied.

研究了溶剂法合成聚阴离子纤维素过程中游离碱浓度、氯乙酸钠水解率和产品取代度及其溶液粘度与反应条件的关系。

The deep origin of Kangjinla podiform chromitite is suggested by: that for the Kangjinla chromitite and the mantle peridotite rocks, the compositions of the chrome spinel, olivine and clinopyroxene are rather different, which indicates that the chrome spinel in the chromitite is neither the simple concentration of that in the host rocks nor with certain genic relation with mantle peridotite. Though the chromitite might be exotic for host rocks, both of them were carried from deep mantle to the shallow place by mantle plum.

康金拉铬铁矿石与矿体围岩地幔橄榄岩的铬尖晶石、橄榄石和单斜辉石等成分方面明显不同，认为矿石铬尖晶石并非是由副矿物铬尖晶石富集而成，与地幔橄榄岩也不存在成因联系，认为豆荚状铬铁矿床对于近矿围岩地幔橄榄岩而言为外来体，但两者可能均是由地幔深部被地幔柱带到上部。

The results show that the technical parameters and the concentration of sodium molybdate have obvious effect on the composition of the alloy. The crystal grain size is from 6.2 to 12.7 nm and changes with current density, temperature and the pH value of the electrolyte.The crystalline growth of the alloy accords with the model of three-dimensional growth. The surface morphology is mainly determined by the rate competitions between the growing direction of vertical surface and the expanding direction along the surface towards circumambient. The results of the X-ray data show the presence of the multiphase containing solid solution and intermetallic compound in the deposits. The deposit phases alter from the FeNi and FeMo solid solution to the FeNi and MoNi4structure at 3 A/dm2. The deposits internal stress increases linearly with the decrease of the grain size. The lattice parameter of the deposits are slightly distorted

结果表明：工艺条件和钼酸钠浓度对合金组成的影响较大；所得合金晶粒尺寸为6.2~12.7 nm，并随电流密度、温度和电镀液的pH值的改变而变化；合金的晶体生长符合晶核三维生长模型，镀层表面形貌由平行和垂直于基体的生长速度的相对大小决定；镀层物相为固溶体和金属间化合物的多相结构，当电流密度为3 A/dm2时，镀层物相由FeNi和FeMo固溶相转化为FeNi和

The matrix effect was corrected by theoretical a influence coefficient method. Moreover, flux dilution rate and fusion time were discussed. The mass ratio of sample to flux was chosen as 1 to 15. The fusion time of sample closen was 15 min. The concentration of the sample in the flux was proved to be suitable for the XRF determination of both components of macro and micro amount.

对稀释比、熔样时间等进行了探讨，结果表明，试样和熔剂的质量比以1：15、熔样时间以15 min为好，所得试样在熔剂中的分散度适当，可同时适合试样中高、低含量组分的测定。

In this investigation,the composition of copolymer P(AM- co -NaAMPS) of acrylamide and 2-acrylamido-2-methyl-propanesulfonate sodium has been determined with the aqueous solution of cetyl trimethyl ammonium bromide as titrant at a concentration of 0.001 mol·L-1 by conductometric titration method.

与元素分析进行比较的结果表明，上述复合作用电导滴定法可作为测定水溶性大分子链中磺酸盐单体含量的方便而又准确的方法，而且预计还可用作为测定水溶性大分子链中其它离子性基团含量的简捷方法。

Result of thermogravity analysis showed that the thermal stability of polyvinylamine chloride lowers with increasing in amination degree. Moreover, properties of dilute aqueous solutions of three types of poly chloride with different amination degree were compared by use of viscosimetric, conductometric, and potentiometric measurements. Results showed that both the electrostatic interaction of neighboring groups on the chain and the reduced viscosity of poly chloride are increased with increasing the degree of amination of poly . The equivalent conductivity is decreased with the increasing the concentration of poly chloride and increased with the increasing the amination degree of poly .

研究了聚乙烯胺盐酸盐的热稳定性和水溶液性质，发现：随着胺化度的提高，聚乙烯胺盐酸盐的对热稳定性逐步降低；聚乙烯胺盐酸盐是一种典型的聚电解质，其水溶液的pH值随平均分子量的变化并不明显，而随着聚乙烯胺胺化度的升高，pH值降低；随着聚乙烯胺盐酸盐的平均聚合度由82.3增加到201.8，它的m值（用于表征聚电解质侧链基团之间相互作用大小的常数）从5.13升高到5.58，而当聚乙烯胺盐酸盐的平均聚合度增加到311.4时，它的m值反而降低到了5.48；随着胺化度由55.65%升高到82.36%，m值由3.65提高到5.50；随着聚乙烯胺盐酸盐的平均聚合度的提高，聚乙烯胺盐酸盐的平均解离常数由7.48降低到7.26，同时随着胺化度的提高，聚乙烯胺盐酸盐的平均解离常数也由8.33降低到7.37；随着聚乙烯胺盐酸盐浓度的提高，溶液的摩尔电导率逐步降低，随着聚乙烯胺胺化度和聚合度的提高，溶液的摩尔电导率有所升高；在pH值为4左右时，聚乙烯胺盐酸盐的比浓粘度分别达到极值，而与聚合度的大小关系不大；聚乙烯胺盐酸盐的特性粘数明显高于其原料聚丙烯酰胺的特性粘数，分子量对特性粘数的影响十分明显，胺化度对特性粘数的影响并不显著。

The Pipaji is one of the drama works of the Chinese first-rate, there are a lot of articles or works about it since Ming Qing ,.Method that that is different, angle that is different, there is some contestation problems under basically and affirmative premise, such as how to evaluate the mian role Caibojie, how to judge its topic, how to evaluate its praise or its mistake in melodies and writings .and the contend for Pipaji and Xixiangji, the relation of Pipaji with Ming and Qing dramas etc. It\'s general concentration of these problems is text originally of analysis and hold up.

《琵琶记》是中国古典戏剧的名著，明清以来有众多的文章、专著论及到了这部作品，方法不同，角度各异，在基本肯定的前提下一直存在一些争议性的问题，如对其主要人物蔡伯喈的评价，对它的主题的判断、对其音律和辞采的褒贬、《琵琶记》与《西厢记》的优劣之争、《琵琶记》与明清传奇的关系等相关问题，这些问题一般集中在对其文本的分析和把握上。

A kind of chemical reagent AH was chosen , the effects of the concentration of AH ,the reaction temperature ,thereaction time and pH on dampproof of leather protein powderwere discussed by means of orthogonal design .

通过正交设计讨论了AH用量、反应温度、反应时间及pH等因素对水解蛋白防潮防粘效果的影响，得到了最佳反应条件。

Effects of addition quantity of O3,concentration of O3,temperature and PH value of solution on the decolorization efficiency of AO Ⅱ were investigated.

研究了臭氧的填加量、浓度，和温度、pH 值的影响因素对脱色效果的影响。

She gently rebuff ed him, but agreed that they could be friends

她婉言拒绝了，但同意作为朋友相处。

If in the penal farm, you were sure to be criticized.

要是在劳改农场，你等着挨绳子吧！