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The photodegradation rate of M-PPV 1 was constrained by DABCO that quenches the triplet state of M-PPV; 2increased when the solvent changed from benzene to deuterated benzene in whichthe lifetime of triplet state is longer than that in benzene; 3 was improveddramatically with high concentration of M-PPV triplet state was generated by energytrasfer from biacetyl.

发现:1能猝灭M-PPV的三重态的1,4-二氮二环[2.2.2]辛烷也能有效地抑制光氧化反应的进行;2能提高M-PPV三重态寿命的氘代溶剂也能使M-PPV光氧化降解速率加快,3丁二酮和M-PPV间的能量传递能够提高M-PPV三重态的浓度,这和丁二酮作三重态敏化剂敏化光氧化M-PPV时,M-PPV的光降解速率大大增加也是一致的。

The results showed that the bioaccumulation coefficient of cadmium and zinc in aboveground parts of Bidens tripartite and Solanum nigrum was not less than 1 respectively, and the concentration of Cd and Zn in aboveground parts was higher than that in roots, denoting basic characteristics of hyperaccumulators.

结果表明:狼把草、龙葵地上部Cd和Zn的富集系数均大於1,且地上部Cd和Zn的含量大於根部Cd和Zn的含量,具备了重金属超富集植物的基本特徵。

RESULTS: The growth speed, weight, developmental uniformity, bionergy and fecuncity of the Bombyx silkworm descent dramatically as they eat the feed that the concentration of 2,4-DCP over 0.8 mmol L~-1 or NP exceed 0.500 mmol L~-1. But the effect on reproductive capacity vary with gender difference, it's more obvious on the late-stage of development and periods of metamorphosis such as ecolysis, pupation, edosion. There may be cumulative effect inside the Bombyx siliworm.

结果 家蚕幼虫食下含0.8 mmol·L~(-1)以上浓度的2,4-DCP或0.500 mmol·L~(-1)以上浓度的NP饲料,生长速度、生长量、发育整齐度、生命力和生殖能力都明显下降;生殖能力所受影响应性别而不同;家蚕发育后期和蜕皮、化蛹、羽化等变态时期影响更加明显,在蚕体内可能有累积作用。

The well-documented chelating properties of bipyridine and the sensitivity of the optical properties of AuNPs have been employed to detect low concentration of metal ions in water.

因为联吡啶具有好的钳合能力,加上金奈米粒子的灵敏的光学性质,所以可以用来侦测水中低浓度的金属离子。

The factors which affect the average molecular weight of the polymer of AM and DMDAAC were investigated. The optimal reaction conditions are as follows: the concentration of monomer AM was 30%, while DMDAAC was 5%; the reaction temperature was 30℃, the amount of initiators at the low temperature stage was 0.05‰(compared to the weight of the monomers joining the polymerization), while V-50 was 0.025‰, the weight ratio of potassium persulphate to sodium bisulphite is 1:1, the amount of carbamide was 40‰, and complexing agent was 0.05‰, besides, aerate nitrogen gas for 8min, then the high molecular weight polymer (M=1.217×10^7) could be got after 16h reaction.

研究了影响AM与DMDAAC共聚物的平均分子量的因素,得到了优化条件为:单体浓度为30%,DMDAAC与AM摩尔比为5:95,聚合温度为30℃,低温段引发剂用量为0.05‰,K2S2O8与NaHSO3质量比为1:1,偶氮二异丁基脒盐酸盐(V-50)用量为0.025‰,尿素用量为40‰,乙二胺四乙酸二钠(EDTA-2Na)用量为0.05‰,在此优化条件下聚合反应16h后得到分子量为1.217×10^7的阳离子型聚丙烯酰胺。

The new progresses:(1)the anatomic studies on the leaves, stems and cones of 25 species Late Mesozoic conifers, particularly those very similar to the living genera, such as Athrotaxites, Torreya, Taxus, Cephalotaxopsis, Cunninghamia and the cheirolepidaceous conifers, such as Brachyphyllum and Psudofrenelopsis;(2) the distribution and evolution of the Late Mesozoic conifers, the relationship between the concentration of CO2 of the atmosphere and the stoma index of the gymnosperms during the Middle Jurassic and Early Cretaceous;(3) the characters, compositions and ages of the Jurassic floras of Yabula Basin, and Erlian Basin of Inner Mongolia and the Early Cretaceous floras and Jiuquan basin and Beishan Area of Gansu.

对12属25种中生代松柏类的枝叶、球果及茎干化石进行了解剖研究,特别是对与现生松柏类相似的Athrotaxites, Torreya, Taxus, Cephalotaxopsis, Cunninghamia及可能属于掌鳞杉科的Brachyphyllum, Psudofrenelopsis等的研究较为深入,发现了4个新种;总结了中国晚中生代松柏类的特点及分布,讨论了重点属的起源和演化问题;研究了中侏罗世、早白垩世及现代裸子植物包括松柏类气孔与大气CO2浓度关系,发现气

Guangdong college of pharmacy,guangzhou,guangdong 510006,china;henan university of traditional chinese medicine,zhengzhou,henan 450008,chinaabstract:objective to establish a method for the determination of the content of total alkaloid in nao mai tong recipe.methods acid dye colorimetry was used in the determination with bromocresol green buffer solution as the color developing agent with absorbance was determined at the detection wavelength of 417 nm.results the calibration curve of the absorbance was linear with the concentration of ligustrazine in the range of 0.031~0.153 mg/ml(r=0.9998).the average recovery of ligustrazine was 100.95%,rsd=1.75%.

作者单位:广东药学院中药化学与分析教研室,广东广州 510006;河南中医学院,河南郑州 450008 目的建立脑脉通有效部位中总生物碱的含量测定方法。方法采用酸性染料比色法,以溴甲酚绿缓冲液作为生物碱的显色剂,测定样品溶液在417 nm波长处的吸收度。结果对照品川芎嗪质量浓度在0.031~0.153 mg/ml的范围内与吸光度呈良好的线性关系,r=0.9998。平均回收率为100.95%,rsd为1.75%。精密度和稳定性良好。

Resonance light scattering spectrum of cadmium- phenanthorline- bromophenol blue system has been studied. The effects of interference substances and optimization of procedure have been investigated. In the presence of Tris-HCl(pH=9.60),Cd2+ reacts with Phen to form the chelate cation, which further reacts with acid dye of BPB to form an ion-associated complex. Then, the complex molecules are accumulated to particles by virtue of hydrophobic forces and other molecular forces. This results in significant enhancement of RLS intensity, and the enhanced intensity of RLS at 638nm is proportional to the concentration of Cd~(2+).

研究了镉-邻菲罗啉-溴酚蓝体系在碱性条件下的共振光散射光谱特征,考察了体系的影响因素和最佳反应条件,研究表明,在pH=9.60的Tris-HCl介质中,镉与邻菲罗啉形成络阳离子,再与酸性染料溴酚蓝形成离子缔合配合物,在疏水力等分子间作用力下,缔合物分子聚集形成缔合微粒,溶液的共振散射光显著增强;在638nm处RLS增强程度与镉浓度成线性关系,线性范围为0-3.20mg/L,检出限为4.50ug/L。

Based on the absorbance change of indicators with the concentration of hydrogen ion released from the enzyme-catalyzed reaction, a convenient colorimetry method is established for the assay of acidic phospholipase 〓 and glycogen phosphorylase b Brilliant yellow and bromothymol blue are chosen as indicators for assays of acidic phospholipase 〓 and glycogen phosphorylase b by following the absorbance changes at 495 nm and 615nm respectively The method is simple, sample-saving, sensitive and valid for a wide range of enzyme concentrations.

为了研究糖原磷酸化酶的激活动力学和酸性磷脂酶〓的复性过程,我们根据酶催化反应中释放氢离子浓度的变化引起相应的指示剂的光吸收发生变化的原理,建立了一种简捷的比色法,用于测定酸性磷脂酶〓和糖原磷酸化酶b的活性。选用亮黄和溴麝香草酚兰分别作为酸性磷脂酶〓和糖原磷酸化酶b测活的指示剂,在495 nm和615 nm处检测二者的光吸收值的变化,可以测定酶活。本方法的优点是,可在比较宽的酶浓度范围内进行活力测定,而且操作简单、节省样品、灵敏度高。

Thunberg Fritillary Bulb is one of the most popular Traditional Chinese herbs. Some trials in vivo and animals indicated that Peimine and Peiminine, extracted from Thunbery Fritillary Bulb, have the function of reversing MDR of two different kinds of mechanisms. They can improve the cytotoxic of ADR to cancer cells by 5~10 folds under concentration of 10% cancer cell growth inhibitory rate. Peimine and Peiminine not only feather typical character of modifier of MDR, but also differ from other moldifiers such as Calcium channel blocker, Cyclosporines in chemical structure, they belong to cevine groups alkaloid, a subgroup of C-Nor-D-homosteroid alkaloid.

浙贝母是临床常用中药,体外及动物试验证明,浙贝母中的有效活性成分贝母甲素和贝母乙素具有逆转肿瘤细胞MDR的作用,而且能逆转两种不同机制的多药耐药肿瘤细胞的耐药性,在无明显细胞毒剂量下,可使阿霉素对耐药肿瘤细胞的杀伤活性提高5-10倍,不但具备明确的多药耐药逆转剂的特征,而且在化学结构上属异甾类生物碱中的瑟文类生物碱,完全不同于钙离子拮抗剂、免疫抑制剂和其它现有的耐药逆转剂,具有作用靶点宽、化学结构独特的特点。

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