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Use of lower wavelengths, such as those available with the mercury lamp lines isolated by means of filters of maximum transmittance at approximately 578, 546, 436, 405, and 365 nm in a photoelectric polarimeter, has been found to provide advantages in sensitivity with a consequent reduction in the concentration of the test compound.

使用较低的波长,例如那些利用光电旋光计过滤掉汞灯线在578、546、436、405、365nm的最大能见度所产生的,已经被发现有利于增加检验敏感性,并最终导致供试品浓度的降低。

The influence of different assembled condition such as assembly method, concentration of zirconium source and pH value on the effectiveness of assembly were evaluated via DSC-TG, FT-IR, Uv-vis and SAXRD et al. It showed that the assembly effectivness of uncalcined 3 Si/Zr_10# sample was best.c The optical characteristic, which including light-conduction in infrared band and polarity in visible band, of dip-coating film and membrane assembled zirconia after processing parameters of assembly optimized were observed via FT-IR and Uv-vis. The polarity was characterized by polarizing angle through calculation from light-transmittance, light-reflectance and fresnel coefficient. qualitative analysis showed that the polarity of Si/Zr_10 # dip-coating film assembled was best.d Adopting zirconium oxychloride as zirconium source, CTAB as template, employing different CTAB adding sequence, two mesoporous zirconia samples were prepared. The template effect of two samples was discussed. It showed that the effect of the sample which CTAB adding sequence was same as mesoporous silica film was better. The light-conduction in infrared band of these samples was also studied, which offered comparison to the polarity of zirconium dioxide assembled within mesopore.

结果显示:组装条件优化后的uncalcined 3 Si/Zr_10#厚膜样组装效果最好,其组装液对应的pH值最利于该锆源离子模板交换组装; c选用FT-IR、Uv-vis对组装条件优化后纳米氧化锆/介孔氧化硅厚膜、纳米氧化锆/介孔氧化硅薄膜包括红外导光性、可见光区内的偏光性在内的光学特性进行了分析,其中偏光性以膜层透光性、反光性及菲涅耳系数计算出的偏振角即布儒斯特角表征,定性分析显示,Si/Zr_10#ZrO_2/介孔氧化硅厚膜偏光性最好; d以氧氯化锆ZrOCl_2·8H_2O为锆源,CTAB为模板剂,采用不同的模板剂加入顺序,探索性地制备两介孔氧化锆样,分析了两介孔氧化锆样的模板效果,得出模板剂加入顺序同介孔氧化硅薄膜时介孔氧化锆样的模板效果较好,并分析了所得样品的导光性,为锆氧粒子引起的附加光学特性分析提供了参考和对比。

By means of a system of nutrient solution culture under greenhouse, the effects of different concentration of exogenous silicon on anti-oxidative system, reactive oxygen species, soluble protein and praline content, root activity and ion content in leaves and roots of Cabernet Sauvignon seedlings were investigated under salt stress condition (50 mM NaCl).

mM浓度的外源硅,研究了不同浓度外源硅处理对盐胁迫(50 mM NaCl)下赤霞珠幼苗叶片中抗氧化酶系统、活性氧代谢、可溶性蛋白质和游离脯氨酸含量,根系活力,根系及叶片中离子含量的影响,以期为外源硅在葡萄抗盐生产上的合理利用提供一定的理论依据。

Through the experiments on hydration of AH in the following sulphate(Li_2SO_4、MgSO_4 、 Al_2(SO_4)_3 、MnSO_4 、CuSO_4 、CoSO4 、CdSO_4 、ZnSO_4 、NiSO_4 、FeSO_4), dissoluble sulfate hydrate origining from hydration process of AH affects it's hydrous rate, hydrous rate of AH does not connect with Z/R of cation in stimulation, theory that Z/R affect hydrous rate of AH does not exist. Third, hydration of AH in dissoluble sulfate complies with dissolve-nucleate -grow theory, concentration of Ca~2+ from dissolving of CaSO_4 is higher than one of CaSO_4·2H_2O, calcium sulphate dihydrite gets a motivity of crystallization. dissoluble sulfate takes the following function: double-salt or dissoluble sulfate hydrate from hydration of AH in it becomes heterogeneous particle and a kind of nucleation catalyzer, and reduces surface barrier when DH becomes crystal because the crystal of DH precedently appears in uneven place. Results indicate hydration of AH does not conform with double-salt theory, but it conform with this mechanism: dissolve-nucleate-grow, formation of DH is an uneven nucleation and crystalizaion process.

通过对CaSO_4在Na_2SO_4 、K_2SO_4 、Rb_2SO_4 、Cs_2SO_4 、(NH_4)_2SO_4溶液中水化过程,以及CaSO_4·2H_2O、CaSO_4与以上硫酸盐反应速度、产物的研究,说明复盐理论不正确;CaSO_4在(Li_2SO_4、MgSO_4 、 Al_2(SO_4)_3 、MnSO_4 、CuSO_4 、CoSO_4 、CdSO_4 、ZnSO_4 、NiSO_4 、FeSO_4)溶液中水化,水化过程中硫酸盐水合物的析晶影响着无水硫酸钙水化,与激发剂阳离子Z/R值大小无关,阳离子的Z/R参数影响水化率的规律并不存在; 3、无水硫酸钙在可溶性硫酸盐中的水化按照溶解-成核-生长理论进行,CaSO_4达到溶解平衡时Ca~2+的浓度大于CaSO_4·2H_2O溶解平衡的Ca~2+的浓度,CaSO_4·2H_2O获得结晶的驱动力,可溶性硫酸盐起到形成晶核的作用:水化过程与CaSO_4生成复盐或析出水合物所形成的细小物相,作为异质微粒使母相中存在不均匀性,这些不均匀性有效地降低成核时的表面能位垒,使CaSO_4·2H_2O晶核优先地在这些具不均匀性的地方形成,因此这些物质起成核催化剂作用。

The baihua forest park of provincial forest park, this project is a national industrial development policy, one is closely supported by national and local industry, twois natural and geographical conditions, historic natural landscape, attracted a lot of all the guests, There are baihua forest park is qingming martyr cemetery TaChun grave, but also people leave the concentration of sightseeing, Four is the baihua forest park also can be used as mount wudang, shennongjia, ancient prime tourist scenic spot of gold, five is the forest eco-tourism industry into forestry development planning.

百花山森林公园属省级森林公园,该项目一是紧扣国家产业发展政策,是国家和地方重点扶持产业;二是自然地理条件较好,自然景观古迹,吸引了不少的四方来宾;三是森林公园内有烈士陵园是人们清明踏春扫墓的集中地,也是人们休假观光的佳地;四是百花山森林公园也可作为武当山、神农架、古隆中景区旅游的黄金节点;五是森林生态旅游业已纳入林业发展规划。

In addition nC〓, nC〓, two isomers of C〓 sterene and three isomers of C〓 isoprenoid hydrocarbons were also identified from aliphatic fraction of pyrolyzed product at 200℃. After pyrolyzed at 300℃, the main aliphatic hydrocarbons were normal alkanes ranged from C〓 to C〓, with C〓 as the main peak and C〓 as the second main peak. Meanwhile, pristane, phytane and C〓 sterane were also detected. In the pyrolysates at 400℃ and 500℃, the content of saturated hydrocarbons decreased, the range of normal alkanes distribution became narrow and the main peak was nC〓. Low concentration of C〓-C〓 steranes was detected and the content of C〓-C〓 increased more.

在200℃热模拟产物饱和烃馏分中除检测出两种长链烯烃外,还检测到正十九碳单烯烃、正三十五碳双烯烃、两个碳二十八甾烯的同分异构体和三个C〓类异戊二烯烷烃化合物同分异构体。300℃模拟产物饱和烃主要为正烷烃,正烷烃的碳数分布范围为C〓-C〓,以C〓为主峰、C〓为次主峰;另外,样品中还检出姥鲛烷、植烷和C〓甾烷等化合物。400和500℃热模拟产物中的饱和烃含量下降,正烷烃系列碳数分布范围变窄,主峰碳后移至C〓,检测到低浓度的C〓-C〓甾烷系列化合物,另外,C〓-C〓藿烷系列化合物含量进一步增加。

Chemometric method were used to analyze UV spectrum of TCAS-heavy metal complex, pure UV spectrum of TCAS-heavy metal complex and TCAS-heavy metal complex distribution curves toward concentration of heavy metals in solution were gained. Finally, complex constants of TCAS towards Cu, Zn, Cd and Pb were got to be 9.79、8.72、6.87 and 5.00, respectively.

采用化学计量学分析TCAS络合重金属的紫外光谱,获得了TCAS-重金属络合物的纯紫外光谱,以及TCAS、TCAS-重金属络合物随重金属浓度变化的分布曲线,并最终解析得到TCAS与Cu、Zn、Cd和Pb的络合常数分别为9.79、8.72、6.87和5.00。

The result showed that the assembly of the constructed molecules agreed with the actual mid-boiling points, the concentration of structural groups, average molecular weights, and the ring and side chain distributions. The correlation of properties between pure compounds and complex mixtures of heavy oils could be built by the proposed method.

验证结果表明,除个别结构基团的摩尔质量误差较大外,构建分子系综中沸点、统计结构基团的摩尔质量、相对分子质量、环和侧链分布均与实测值相近,与重油组成具有等效性。

The effects, such as the acidity of leaching system, the temperature and the concentration of the sodium chloride, on oxidation and leaching of copper-bearing gold ores were analyzed. The results show that the sequence of sulfide ores oxidized and dissolved are pyrrhotite firstly, sulphide secondly, then chalcopyrite, pyrite lastly.

结果表明:硫化矿的氧化溶解首先是磁黄铁矿,其次是铜的次生硫化矿,再次是黄铜矿,最后是黄铁矿;载金黄铜矿的氧化首先是铁从黄铜矿的晶格中氧化溶解出来,生成中间产物CuS2和CuS;较高的酸度和氯化钠浓度有利于单质硫的生成、三价铁的水解和铜的浸出,进而有利于金浸出率的提高。

The role of the oxidant used was considered to be a quencher of the semiquinone radical anion of HA to its parent quinone to increase the relative concentration of HA so that the generation of SO~3^- via the electron transfer interaction between Hypocrellins and SO~3^2^- was accelerated.

氧化剂在这一反应中的作用为:将产生的竹红菌素半醌负离子自由基氧化至其母体醌,增加反应物的相对浓度,同时使竹红菌素与SO~3^2^-之间的电子转移循环进行,加速SO~3^-的产生。

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