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Among them, 7 compounds were firstly found from Trollius chinensis and 4 compounds were firstly found from the genus of Trollius. Most isolated compounds were flavonoid, and few were organic acid. The quality standard studies were conducted by determining the total flavonoids in the flowers of Trollius chinensis at different flowering time and deciding the optimum harvesting time.

在对其质量标准的系统研究中，以总黄酮为指标，对不同花期的金莲花进行了含量测定，确定了最佳采收期；对不同产地10个样品中总黄酮、荭草苷等活性成分进行了含量比较，结果表明金莲花中黄酮类成分含量稳定，适于在制定质量标准时作为含量测定的指标成分；通过对不同产地10个样品指纹图谱的比较，确定了21个共有峰所代表的化合物为金莲花的药效物质基础。

They were two new compounds, [cyclo(Pro-Val-Phe-Phe-Pro-Val-Phe-Ser-Leu),7],[2-N-(1-methoxycarbonylethyl)guanosine, 10], and eight known compounds,(p-hydroxybenzoic acid, 1),(methyl succinate, 2),(russulaceramide, 3),(phenylalanine, 4),(guanine, 5),(β-carboline, 6),(uridine, 8), and (adenosine, 9). All the compounds were isolated from Amanita exitialis for the first time.

分别为：对羟基苯甲酸(p-hydroxybenzoic acid，1)、丁二酸二甲酯(methyl succinate，2)、神经酰胺(russulaceramide，3)、苯丙氨酸（phenylalanine，4）、鸟嘌呤核苷(guanine，5)、β-咔啉(β-carboline，6)、环（脯氨酸-缬氨酸-苯丙氨酸-苯丙氨酸-脯氨酸-缬氨酸-苯丙氨酸-丝氨酸-亮氨酸） [cyclo(Pro-Val-Phe-Phe-Pro-Val-Phe-Ser-Leu)，7]、尿嘧啶核苷(uridine，8)、腺嘌呤核苷(adenosine，9)、2-N-(1-甲氧羰基乙基)鸟苷[2-N-(1-Methoxycarbonylethyl)guanosine， 10]。10个化合物均为首次从致命鹅膏中分离得到，其中化合物7和10为新化合物。

The results show that the compounds have highβvalues of 5.60×10~(-28) and 5.76×10~(-28)esu at 1064 nm wavelength, respectively. The maximum absorption wavelengths of the compounds were less then 600 nm, and their critical wavelengths below 710nm. These compounds were thermally stable with the decompounded temperature of 224 and 216℃, respectively, and consequently they could be considered to be better choices for the preparation of NLO materials.

结果表明：两种噻唑类生色分子具有较高的β值，在波长1064nm处，β分别为5.60×10~(-28)和5.76×10~(-28)esu，其最大吸收波长都未超过600nm，截止波长均小于710nm，生色分子的热分解温度分别为224℃和216℃，具有较好的热稳定性，可用于制备性能优异的非线性光学材料。

The application, proposed hydrotalcite-like compounds as a new type of environmentally friendly solid catalysts in the aldol condensation, nitrile hydrolysis, epoxide ring-opening reaction of the oxidation of aromatic compounds, alcohols oxidation, reduction of nitro compounds, and many other important reactions in organic synthesis has an important application potential, and with little pollution compared to conventional catalysts, easy separation of advantages of high reactivity.

叙述了水滑石类化合物作为固体酸碱催化剂、氧化还原反应催化剂、催化剂载体等方面的应用情况，提出了水滑石类化合物作为一类新型的环境友好的固体催化剂，在醇醛缩合、腈类水解、环氧化物的开环反应、芳烃类化合物的氧化、醇类氧化、硝基化合物的还原等许多重要的有机合成反应具有重要的应用前景，并且与传统催化剂相比具有污染小、易分离、反应活性高等优点。

Firstly, headspace solid-phase microextraction was established to determine AITC by orthogonal design. Extraction temperature, stir speed, extraction time, and desorption time were set at 40℃, 900r/min, 30min, and 5min, respectively. Under these optimal conditions, volatile flavor compounds in mustard oil, wasabi, and 'Chongcai'leaf mustard product were identified by SPME/GC/MS. In these three samples, 6,12,17 constituents were identified respectively; Allyl isothiocyanate was the main flavor compound, which accounted for 73.45%, 64.25%, 32.74% of total volatile compounds, respectively. Carbon disulfide, a hydrolysis product of AITC, accounted for 14.37% 25.40%, 51.67% of total volatile compounds respectively. There were some other isothiocycannates, such as butane, 1-isothiocyanato-, isobutyl isothiocyanate, 1-benzene, 4-isothiocyanato-, benzene (2-isothiocyanatoethyl)-, etc.

首先采用正交实验设计优化固相微萃取技术的前处理条件，结果表明，以萃取温度40℃、搅拌速度900r／min、萃取时间30min、解吸时间5min为最佳条件；在此最优条件基础上，利用SPME／GC／MS联用技术分析芥末油、青芥辣、冲菜的挥发性风味成分，分别检出6、12、17种化合物，主要风味物质均为AITC，相对丰度分别为73.45％、64.25％、32.74％；AITC的水解产物二硫化碳的相对丰度分别为14.37％、25.40％、51.67％；还检测到了其它几种异硫氰酸酯，如异硫氰酸丁酯、异硫氰酸异丁酯、异硫氰酸丁烯酯、2-苯乙基异硫氰酸酯等。

There are some isomeric compounds of hydroxypyridinone. The compounds of 2-hydroxy-6-pyridinone have been used to dyestuff and pesticide widely. The compounds of 3-hydroxy-2-pyridinone and 3-hydroxy-4-pyridinone are paid attention to, because they are very useful heavy metal chelations. Especially, they are wonderful candidate medicament for the toxicosis of depleted uranium, so they can settle the DU jeopardize to the people.

羟基吡啶酮化合物有不同的同分异构体，2-羟基-6-吡啶酮已被广泛用于染料和农药行业，而3-羟基-2-吡啶酮和3-羟基-4-吡啶酮也引起了人们的重视，因为这两种异构体的化合物是非常理想的重金属络合剂，尤其重要的是，它可作为解决贫铀中毒的候选药物，有望解决战争中由于贫铀中毒带来的危害。

Phytochemical investigation on the acetone extract of the stems of K.oblongifolia led to the isolation of 49 compounds and 31 of them were identified.They were 20 lignans,(including 11 dibenzocyclooctadienes,8 spirobenzofuranoid dibenzocycloocta -dienes,1 other lignan),9 flavones,and 1 nortriterpenoid.Among them,4 were new compounds,1 was new natural products,and 8 compounds were isolated from this family for the first time.

通过对冷饭藤的藤茎化学成分的研究，从丙酮提取物中分离得到49个化合物，鉴定了31个化合物，包括木脂素类化合物20个(联苯环辛烯类木脂素11个，螺苯骈联苯环辛烯类木脂素8个，其他类型木脂素1个)，黄酮类化合物9个，降三萜类化合物1个，其中。4个为新化合物，1个新的天然产物，8个为本科首次报道。

Totally, 147 flavor compounds, which comprised of 17 acids, 12 alcohols, 16 aldehydes, 36 esters, 12 furans, 13 ketones, 14 miscellaneous compounds, 8 phenols, 6 pyrans, 4 pyrazines, 3 pyrroles, 6 sulfur-containing compounds, were identified.

共鉴定出147种风味化合物，其中酸类17种、醇类12种、醛类16种、酯类36种、呋喃12种、酮类13种、杂环化合物14种、酚类8种、吡喃6种、吡嗪类4种、吡咯3种、含硫化合物6种。

This dissertation aims at finding anticancer and antibacterial polynuclear complexes targeting DNA with high activity and low toxicity. Sixteen compounds were synthesized, and characterized by means of X-ray single crystal diffraction, elemental analysis, molar conductivity and IR, and the influencing factors on structures of the compounds have been investigated. The actions of these compounds to DNA were also investigated by spectral, electrochemical and hydromechanical methods.

本论文以DNA为靶点，以寻找新结构类型的高效、低毒的抗癌、抗菌多核配合物为目标，从分子设计出发，共合成得到了16个化合物的单晶结构，对其进行了结构表征，探讨了结构影响因素，并研究了其超分子结构；采用紫外-可见吸收光谱法、荧光光谱法、电化学和粘度法，从分子水平上研究了所得配合物与DNA的相互作用；在细胞水平上，研究了草酰胺桥联双核配合物的抗菌和抗肿瘤活性。

Amount of total phenolic compounds, total flavones and DPPH scavenging activity for different kinds of vinegars were compared. The results indicate that (1) DPPH scavenging activity of different kinds of vinegars has a positive correlation with amount of total phenolic compounds, total flavones, the correlation coefficients were 0.9523 and 0.8691, respectively,(2) the higher content of phenolic compounds and flavones in Zhenjiang aromatic vinegar respond for its higher scavenging activity.

对不同品种食醋总酚含量、总黄酮含量、DPPH自由基清除活性的比较分析表明：(1)不同品种食醋自由基清除活性与醋中的总酚含量、总黄酮含量存在正相关性，相关系数分别为0.9523、0.8691；(2)镇江香醋中由于总酚含量、总黄酮含量较高因而自由基清除作用较强。

Neither the killing of Mr Zarqawi nor any breakthrough on the political front will stop the insurgency and the fratricidal murders in their tracks.

在对危险的南部地区访问时，他斥责什叶派民兵领导人对中央集权的挑衅行为。

In fact,I've got him on the satellite mobile right now.

实际上 我们已接通卫星可视电话了