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Sheet-like particles are mainly aluminosilicates and calcium compounds on which iron compounds are attached, and the majority of floccule particles contain calcium compounds.

片状颗粒主要是附有铁化合物的铝硅酸盐和钙盐，絮状颗粒则主要含钙化合物。c不同采样点单个颗粒的形貌、组分有明显差异。

Compounds 1 and 2 were new xanthones, and compound 3 was isolated as a natural product for the first time, and compounds 4 and 6 were isolated for the first time from this genus. The antioxidant activities of all compounds were evaluated by ABTS,FRAP and DPPH assays respectively. Compound 9 showed significant activity by the ABTS and FRAP assays. Compound 1 showed significant activity with IC50 value of 0.31 mg·L-1 in DPPH assay.

化合物1，2为新化合物，化合物3为新天然产物，化合物4，6为首次从该属中获得；化合物9在ABTS和FRAP模型中显示出显著的抗氧化活性；化合物1清除DPPH自由基能力的IC50为0.31 mg·L-1。

Compounds 1 and 2 were new compounds, compounds 3 and 9 were isolated from this genus for the first time.

其中化合物1和2为新化合物，化合物3和9为首次从该属植物中分离得到。

In this paper we reported the results of 4 antimony cyclic-mercaptides and 2 corresponding tincompounds and 1 organomercury compounds,3 stibonic acids and related compounds,4 bis(p-aminophenoxy)- thiaalkanes,4 EDTA-chelates of antimony,tin,mercury and bismuth,"TWSb", hexachloroethane,tetrachloroethylene and some other antimony,tin and mercury compounds.

本文报告32种有机化合物对于日本血吸虫病的动物实验治疗的结果，包括：二硫锑环状化合物4种及其相应的 Sn 化合物2种及 Hg 化合物1种、酸类3种、双硫间烷类化合物4种、EDTA 与 Sb，Sn，Hg 及 Bi4种螯合盐、"TWSb"、CCl_3—CCl_3、CCl_2=CCl_2以及一些其他 Sb，Sn 及 Hg 的衍生物。

Among them, the antioxidant compounds can effectively remove free radicals and esters peroxygen compounds inside the body, and interdict the powerful cancerogenic substance N-ammonium nilrite compounds. It can not only greatly enhance the body's immunity, but also with effective functions in moisturizing the skin, anti-fatigue and anti-aging; the bamboo fiber contains the amino acid necessary for human body, having distinctive health-care functions on the skin; the bamboo cellulose, bamboo honey and pectin have the effects of moisturizing the skin and fighting fatigue. They can increase the body's microcirculating blood, activate the histiocyte, enable the body to produce heating effects, effectively regulate the nervous system and unclog the meridian; the bamboo fiber has no free electric charge, antistatic and relieves itching.

其中，抗氧-化合物能有效清除体内的自由基和酯-过氧化合物，阻断强致癌物质N一亚-酸氨化合物，不仅能显著提高机体免-能力，而且具有滋润皮肤和抗疲劳、-抗衰老的生物功效；竹纤维含有多种-体必需的氨基酸，对皮肤具有独特的-健功能；竹纤维素、竹密、果胶具有-滋润皮肤和抗疲劳的功效，能增加人-的微循环血流，激活组织细胞，使人-产生温热效应，能有效调节神经系统-，疏通经络；竹纤维不带自由电荷，-静电，止瘙痒。

In order to find active pesticide leading compounds, thinking about that triazolothiadiazoles had various biological activities, this paper designed and synthesized 11 novel title compounds from 3-substituted-4-amino-5-mercapto-1,2,4-triazoles with heterocyclic carboxylic acid via cyclization in the presence of phosphoryl chloride by the princple of combination of active strucural moieties. The structures of the title compounds were characterized by melting point, IR, 1HNMR and elemental analysis.

为了寻找高活性农药先导化合物，考虑到三唑并噻二唑衍生物具有广泛的生物活性，本文利用活性亚结构拼接原理，将活性基团分别引入1，2，4-均三唑并[3，4-b]-1，3，4-噻二唑杂环的3位和6位，合成了未见文献报道的3，6-二取代均三唑并[3，4-b]-1，3，4-噻二唑类化合物11个，并用IR、1HNMR及元素分析测试技术对其进行了结构表征。

Methods In view of the selective accumulation of porphyrin derivatives in tumor tissue, three ftorafur-porphyrin compounds and three metal compounds were designed, and the target compounds were synthesized with satisfied yield via a four-step procedure starting from pyrrol and substituted benzaldehydes.

根据卟啉对肿瘤组织的选择性滞留作用，设计了3个卟啉替加氟化合物及3个金属络合物，并以吡咯和取代苯甲醛为原料经4步反应以满意的收率得到目标化合物。

Synthesis of target compounds namely: to vanillic acid as the starting material with methanol under reflux conditions for 4 - hydroxy -3 - p-methyl, then ether, and nitration, reduction, cyclization reaction 6 - methoxy -7 - benzyloxy-quinazoline -4 - one, and then by the chloride in place of aniline, benzyloxy-off, such as etherification reaction of the target compounds; target compounds with the second and third occurrence of substitution reactions of amines by the TM1, that is, 4 - amino-benzene -6 - methoxy -7 - [2 - hydroxy -3 -(N, N-diethyl amino) oxy c] quinazoline; with ether occurred Ornidazole reaction of TM2, namely, 4 - amino-benzene -6 - methoxy -7 - [2 - hydroxy -3 -(2 - methyl -5 - nitroimidazole) C oxy] quinazoline.

本论文以嘌呤类似物喹唑啉为母核，分别在其4位和7位引入结构多样的取代苯氨基和柔性侧链，设计了一系列4-取代苯胺基-6-甲氧基-7-(2-羟基取代丙氧基)喹唑啉类化合物。目标化合物的合成即：以香草酸为起始原料，与甲醇回流条件下得到4-羟基-3-甲氧基苯甲酸甲酯，然后经过醚化、硝化、还原、环合反应得到6-甲氧基-7-苄氧基喹唑啉-4-酮，然后再经氯化、取代苯胺、脱苄氧基、醚化等反应得到目标化合物；目标化合物与二乙胺发生胺取代反应得到了TM1，即4-苯氨基-6-甲氧基-7-[2-羟基-3-丙氧基]喹唑啉；通过与奥硝唑发生醚化反应得到TM2，即4-苯氨基-6-甲氧基-7-[2-羟基-3-(2-甲基-5-硝基咪唑)丙氧基]喹唑啉。

The synthesis of the pentacyclic skeleton of Et-743 and the construction of the five chiral centers thereof.1. The core pentacyclic skeleton of phthalascidin was constructed with L-dopa as the starting material via thirteen steps. First, two basic synthons, the C-1 functionalized tetrahydroisoquinoline compounds 8 and N-protected Z-dopa derivative 9, were prepared from L-dopa. They were coupled via amide bond to form the dipeptide compounds 10, which were the first key intermediates. Then the primary hydroxyl groups were transformed into the corresponding amino aldehydes 11 via Swern oxidation. Followed by the intramolecular Pictet-Spengler cyclization, the pentacyclic compounds 12 were synthesized.

五环骨架的构建及五个正确手性中心的确立：1.1我们以L-多巴为起始原料，经过多步官能团保护和转化合成了基本结构单元8然后和苯丙氨酸衍生物9，通过缩合反应生成酰胺中间体10，经Swern氧化得到醛化合物11，然后再次利用分子内改良的Pictet-Spengler反应一步构建c，d两环，得到五环骨架化合物12，最后，实现了21-位羰基向氰基的转化，得到了C-1位官能化的化合物14，化合物14不但具有和Et-743一致的五环骨架，而且分子中五个手性中心立体构型也与其完全相同：其中，3，位和13，位的手性中心由原料L-多巴带入，而1，位，11，位和21，位手性中心则通过不对称诱导而确立。

The result showed that caffeic acid (PA4) and 3-O-coumaroyl-β-sitosterol (PE1) appeared to be most synergistic compounds for combining with other compounds and chlorogenic acid (PA6) was the most antagonistic compound with other compounds on the growth inhibition of A549, a human lung cancer cell line; while any 2-compound combinations of palmitic acid, 5-hydroxy-7-methoxy- 4'-acetylisoflavone and stigmasterol (S1) appeared to be synergistic on the growth inhibition HT-29, a human colorectal cancer cell line.

由两种化合物组合的结果发现，咖啡酸(caffeic acid；PA4)或3-O-coumaroyl-β-sitosterol (PE1)与其他化合物组合时，对於抑制A549细胞增生方面有相乘的作用，另一方面，绿原酸(chlorogenic acid；PA6)与其他化合物组合时，有强烈的拮抗作用。

Neither the killing of Mr Zarqawi nor any breakthrough on the political front will stop the insurgency and the fratricidal murders in their tracks.

在对危险的南部地区访问时，他斥责什叶派民兵领导人对中央集权的挑衅行为。

In fact,I've got him on the satellite mobile right now.

实际上 我们已接通卫星可视电话了