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Compounds 1 and 2 were new xanthones, and compound 3 was isolated as a natural product for the first time, and compounds 4 and 6 were isolated for the first time from this genus. The antioxidant activities of all compounds were evaluated by ABTS,FRAP and DPPH assays respectively. Compound 9 showed significant activity by the ABTS and FRAP assays. Compound 1 showed significant activity with IC50 value of 0.31 mg·L-1 in DPPH assay.

化合物1,2为新化合物,化合物3为新天然产物,化合物4,6为首次从该属中获得;化合物9在ABTS和FRAP模型中显示出显著的抗氧化活性;化合物1清除DPPH自由基能力的IC50为0.31 mg·L-1。

Guards against the facture and the correlation stipulation based on the air pollution defines, the air pollutant may divide into four big projects, respectively be the gaseity pollutant (including sulfur oxide compound bucket carbon monoxide, nitrogen oxide compound, hydrocarbon, chlorine, gasified hydrogen, fluoride, chlorhydrocarbon and so on), the granular pollutant (including suspended particulate matter, golden bureau coal smoke, black smoke, acid fog, falls dust and so on), two pollutant (refers to pollutant to pass through photochemical reaction in air to have pollution again, including photochemistry fog, photochemistry high oxide compound and so on) and odor matter (including chlorine, hydrogen sulfide, curing methyl, sulfur alcohol type, methyl amines) and so on.

依据空气污染防制法及相关规定所定义,空气污染物可分为四大项目,分别为气状污染物(包括硫氧化物勺一氧化碳、氮氧化物、碳氢化合物、氯气、气化氢、氟化物、氯化烃等)、粒状污染物(包括悬浮微粒、金局煤烟、黑烟、酸雾、落尘等)、二次污染物(指污染物在空气中再经光化学反应而产生之污染,包括光化学雾、光化学性高氧化物等)及恶臭物质(包括氯气、硫化氢、硫化甲基、硫醇类、甲基胺类)等。

Goal compound synthesis namely: Take the vanillic acid as outset raw material, obtains 4- hydroxyl - 3- anisole methyl formate with the methyl alcohol reflux conditions, then after the etherification, the nitration, the return to original state, the ring closure response obtains 6- methoxy - 7- animal pen oxygen radical kui zuo lin - 4- alkone, then passes through the chlorination, the substitution aniline, to escape responses again and so on animal pen oxygen radical, etherification to obtain the goal compound; The goal compound and the diethylamine had the amine substitution reaction to obtain TM1, namely 4- benzene amino - 6- methoxy - 7- [2- hydroxyl - 3-(N, N- two ethyl aminos) third oxygen radical] kui zuo lin; Through zuo has the etherification with the Austria niter to respond obtains TM2, namely 4- benzene amino - 6- methoxy - 7- [2- hydroxyl - 3-(2- methyl - 5- nitryl imidazole) third oxygen radical] kui zuo lin.

目标化合物的合成即:以香草酸为起始原料,与甲醇回流条件下得到4-羟基-3-甲氧基苯甲酸甲酯,然后经过醚化、硝化、还原、环合反应得到6-甲氧基-7-苄氧基喹唑啉-4-酮,然后再经氯化、取代苯胺、脱苄氧基、醚化等反应得到目标化合物;目标化合物与二乙胺发生胺取代反应得到了TM1,即4-苯氨基-6-甲氧基-7-[2-羟基-3-丙氧基]喹唑啉;通过与奥硝唑发生醚化反应得到TM2,即4-苯氨基-6-甲氧基-7-[2-羟基-3-(2-甲基-5-硝基咪唑)丙氧基]喹唑啉。

Morphology and Ultrastructure of Compound Eyes in the larval stages of Cherax quadricarinatus Morphology and Ultrastructure of Compound Eyes was investigated by TEM and SEM in the larval stages of Cherax quadricarinatus. The result is indicated: Morphology of compound eye and ommatidium in the larval stage were similar to that in adult stage. The area of the ommatidia increases from 906±29. 6μm〓 in larva Ⅰ(1. 5cm long) to 967±53. 3um〓 in larva Ⅲ(3cm long) and 3724±230.3μm〓 in adult (16cm long).

扫描电镜结果表明:刚离开母体的仔虾(体长约1cm)复眼和小眼的形态已接近成体,小眼的平均表面积由1.5cm仔虾的906±29.6um〓增长为3cm仔虾的967±53.3um〓和16cm成体的3724±230.3um〓;小眼个数也从体长1.5cm仔虾的1001个增加到3cm仔虾的1238个和16cm成体的5652个,红螯螯虾复眼的增大是由于小眼面积的增加和小眼数目的增多而引起的。

Methods:the preparation procedure of β cyclodextrin inclusion compound of pennyroyal was studied by orthogonal test with 3 factors: pennyroyal, temperature and time.the inclusion compound was proved by thin layer chromatography and microscope.results:the optimum preparation conditions for inclusion compound were established as :pennyroyal 2.5 ml ,inclusion temperature was at 50℃ and for 3.5hr.

用正交实验法研究配比、温度、时间三个因素对薄荷油β环糊精包合物的饱和水溶液法的制备工艺的影响,考察包合物的收率,并用tlc、显微影像验证包合物的形成。结果:最佳的工艺条件薄荷油2.5 ml,包合温度50℃,包合时间3.5 h。

The mechanism of photosensitivity and phototaxis was studied with optical andelectrophysiological method. The results are as follows:1 among three kinds of Chysopa peral. of the compound eyes show little daily change in Chrysopa sinica Tjedar .The model and color of psesudpopupil show significant daily change in Chrysopa septempzhbybimctata Wesmacl and Chrysopa formosa Brauer, color and diameter of the psesudpopupil of the compound eyes in Chrysopa septempunctata Wesmacl make rapid change at noon, afternoon ,night are similar ,but make little change in the morning and the next morning. Diameter of psesudpopupil of compound eyes is the biggest in the afternoon, which of Chrysopa formosa Brauer, is the biggest at noon.

本文应用光学及电生理学方法对棉铃虫优势种天敌—中华草蛉、大草蛉和丽草蛉3种草蛉的感光和趋光机制进行了研究,主要研究结果如下: 1、中华草蛉、大草蛉、丽草蛉复眼伪瞳孔大小、颜色昼夜间有节律性变化,且种间具有不同的变化模式。3种草蛉中,中华草蛉复伪瞳孔大小昼夜节律变化不明显,其模式和颜色上亦基本无变化,中间为一小黑点,其外围是绿色,最外层为红色,形状为正六边形:大草蛉、丽草蛉的复眼伪瞳孔大小昼夜间不同,大草蛉的复眼伪瞳孔在中午、下午、晚上变大,早晨和次日早晨基本一致,但次日早晨稍小些。

In complex 1,Cucan be described as a four-coordinated square planar geometry.Compound 8 is the sodium salt of plumbagin and exists as ionic compound.Compounds 9-16 are the rare earth complexes of plumbagin with La,Y,Dy,Sm,Gd,Nd,Erand Eu.Compound 17 is binuclear Y complex.18 is mononuclear Ycomplex with plumbagin and another ligand from Plumbago Zeylanica.Compounds 19-21 are the ternary complexes with plumbagin and 2,2\'-bpy and phen as assistant ligand.In 19, the geometry of Cucan be described as five-coordinated distorted square pyramid that exists in a dimer through the weak bonding,and 1-D chain structure is formed by intermolecular hydrogen bonds.

化合物1的单晶结构分析表明1具有四配位平面四边形结构,化合物8是白花丹素的Na盐,以离子化合物形式存在;化合物9~16为白花丹素的La,Y,Dy,Sm,Gd,Nd,Er,Eu的稀土金属配合物;化合物17是白花丹素的双核钇结构;化合物18为白花丹素的单核钇结构,该配合物除了含白花丹素外,还有来自白花丹植物中的另一个单体化合物也参与配位;化合物19~21是以2,2\'-联吡啶和邻菲咯啉等含N配体为辅助配体,具有白花丹素—含N配体—金属离子的三元配合物,化合物19是白花丹素和2,2\'-联吡啶与Cu的配合物,具有五配位的四方锥构型,通过Cu…O弱的成键作用形成二聚体,再通过分子间的氢键作用进一步形成一维链状结构,化合物20和化合物21是白花丹素分别与2,2\'-联吡啶和邻菲咯啉的Zn配合物,都具有六配位八面体构型的双核锌配合物,呈一维链状结构,化合物20中链与链之间的大量氢键将一维链扩展成二维层,分子间的π-π堆积作用进一步形成三维结构。

Magnificent inside and outside the province to recruit well-known expert group set up fertilizer experts, mainly the production of compound fertilizers, compound fertilizers, mixed fertilizers, organic one inorganic compound fertilizers, ecological fertilizer, long-acting nitrogen fertilizer, nitrophosphate , particulate ammonium bicarbonate, potassium sulfate particles, red fertilizer, foliar fertilizer, etc..

商丘市雄壮肥业有限公司聘请省内外知名肥料专家成立专家组,主要生产复混肥料、复合肥料、掺混肥料,有机一无机复混肥料、生态肥、长效氮肥、硝酸磷肥、颗粒碳铵、颗粒硫酸钾、冲施肥、叶面肥等肥料。

Intra-family comparison resulted in the findings of the four developmental stages of the indicative supplemental structure of the Tibeto-Burman group from primitive, adhesive, compound, adhesive-compound (single or no structural auxiliaries), adhesive-compound (frequent use of structural auxiliaries with syntactical value).

通过语族范围内述补结构的比较,根据各语言述补结构的特点将藏缅语的述补结构的发展归纳为四个阶段:萌芽状态的述补结构阶段,粘合式述补结构阶段,组合、粘合式述补结构阶段第一级,组合、粘合式述补结构阶段第二级(结构助词丰富,有重要的句法地位)。2、揭示汉、藏缅、壮侗、苗瑶各语族述补结构的异同及这些异同产生的机制。

Intra-family comparison resulted in the findings of the four developmental stages of the indicative supplemental structure ofthe Tibeto-Burman group from primitive, adhesive, compound, adhesive-compound (single or no structural auxiliaries), adhesive-compound (frequent use of structural auxiliaries with syntactical value).

通过语族范围内述补结构的比较,根据各语言述补结构的特点将藏缅语的述补结构的发展归纳为四个阶段:萌芽状态的述补结构阶段,粘合式述补结构阶段,组合、粘合式述补结构阶段第一级,组合、粘合式述补结构阶段第二级(结构助词丰富,有重要的句法地位)。2、揭示汉、藏缅、壮侗、苗瑶各语族述补结构的异同及这些异同产生的机制。

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According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm~150rpm时取得最大值,此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世,形体几无变化。

When I was in school, the rabbi explained everythingin the Bible two different ways.

当我上学的时候,老师解释《圣经》用两种不同的方法。