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By using two-stage separations indicates that, the content of total ketones compound by one stage separation is 12.14%, far lower than 54.95% by two-stage separations, and the content of pulegone and menthone increases from 3.37% and 3.46% by one-stage separation to 19.34% and 22.95% by two-stage separations respectively. But the content of the long chain unsaturated fatty acid and its ester ingredient reduces from 41.58% and 18.88% by one stage separation method to 29.06% and 9.86% by two-stage separations method respectively, also the phenol compound by two-stage separations method can been separated completely.

对荆芥挥发油采用两级分离的研究表明:酮类化合物的总含量由二级分离的54.95%远高于一级分离的12.14%,其中胡薄荷酮和薄荷酮的含量分别由一级分离的3.37%和3.46%增加到二级分离的19.34%和22.95%,而长链不饱和脂肪酸及其酯类成分含量分别从一级分离法的41.58%和18.88%降低到二级分离法的29.06%和9.86%,且二级分离法已完全除去酚类化合物。

The compound can simply and rapidly get into living cells, which has a reaction with free active mercapto group in cells, and fluorescence intensity of the compound is led to be obviously enhancing, thereby the fluorescent probe can be used in fluorescent measurement or fluorescent image of fluactive mercapto group (such as glutathione and the like) in living cells.

该化合物可简单迅速地进入活细胞,与细胞内游离的活性巯基基团发生反应,导致化合物的荧光强度显著增强,进而可以用于活细胞中活性巯基的荧光测定和荧光成像。

During preparation, mercapto ethanol isooctanoate, alkyl or ester tin chloride and organic solvent are first heated and refluxed while adding catalyst; organic layer is then obtained through separating liquid and decompression distilled; and through further steps, the compound is obtained. The synthesis process of the present invention is simple, and has conversion rate higher than 95 %, normal pressure and low reaction temperature, low power consumption and less pollution, and the prepared compound has high reaction activity and low toxicity.

制备时,将异辛酸巯基乙醇酯、烷基或酯基氯化锡和有机溶剂加热回流,同时加入催化剂,然后通过分液,保留有机层,再对有机层进行减压蒸等步骤制得所述化合物;本发明合成工艺简单,转化率大于95%,反应在常压条件下,反应温度低,从而降低了能耗,减少了污染,所制备的化合物具有反应活性高和毒性小的特点,使用安全。

Compared with heparin,the wave-lenght of the light absorbed by the metachromatic compound of the polysaccharide and azure I is longer,is 530 nm,and the stability of the metachromatic compound is less.

樊绘曾等人进一步提出了对多糖类与有机染料异染性质的观察有助于在化学药理水平上比较多糖的结构与活性的差别,可能为多糖药物的筛选提供一种方法[5]。

All sorts of service function test result makes clear, what mix into added PR series additive to cause compound water certain property and microtherm function is small drop, however relatively the high temperature capability that improved compound substantially, agree with to be used below the circumstance of burden high temperature.

各种路用性能试验结果表明,掺加PR系列添加剂造成了混合料水稳性能和低温性能的小幅下降,却较大幅度地提高了混合料的高温性能,适合于在重载高温的情况下采用。

The experiments of the biological activity for target molecula were accomplished. The experiment results of inhibiting activity against COX-2 indicated that the compound TM-II-5f had the highest inhibition rate, up to 95.59%, and yet the compound TM-II-5g exhibits weakly inhibiting activity.

对目标产物TM-II-5a~5g进行了生物活性研究,人环氧酶-2(COX-2)活性抑制实验结果表明:目标产物TM-II-5f对人环氧酶-2(COX-2)有很强的抑制活性,抑制率高达95.59%,目标产物TM-II-5g具有较弱的抑制率(0.61%)。

The present invention provides a multinuclear half metallocene compound in which two or more of transition metals of groups 3 to 10 on periodic table are connected through bridge ligand simultaneously containing Pi-ligand cycloalkandienyl group and Alpha-ligand functional group and its preparation, and a process for preparing styrene polymer using the compound as a catalyst.

本发明提供了一种其中的两个或更多元素周期表第3-10族过渡金属通过同时包含π-配体环烷基二烯基团和α-配体功能基团的桥配体连接的多核半金属茂络合化合物及其制备方法,及使用本化合物为催化剂的苯乙烯聚合体的制备工艺。

The selective quenching by Hg2+ of the fluorescence of compound 1 was rationalized in terms of the formation of a nonfluorescent Hg2+-1 complex with enhanced intramolecular charge transfer compared to compound 1 itself.

基于等摩尔连续变化法、红外光谱和核磁滴定实验结果提出了传感分子1与Hg2+的1∶1型结合模式,其中1-位S原子和2-位胺N原子为Hg2+配位原子;结合光谱变化讨论了Hg2+结合显著增强分子内电荷转移的荧光猝灭机理。

In pH=2.0 sulfuric acid solution, 2,2′bipyridine, an almost nonluminescent compound was transformed into a highly fluorescent compound (λex=340 nm,λem=430 nm) when attacked by ·OH generated by Fenton reaction.

在酸性介质中,Fenton反应产生的羟基自由基能将几乎无荧光的2,2′-联吡啶氧化成强荧光物质,羟基化产物的最大激发和发射波长分别是340 nm和430 nm。

DH level, CD4+ T lymphocyte count below 100 × 106/L, and interstitial pneumonia or ground-glass shadow in chest images, the diagnosis of PCP could be made presumptively. It is difficult to make a nosogenic diagnosis of PCP, but TBB considerably increases the positive rate of pneumocystis. Compound sulfamethoxazole is recommended as the first selected drug. In severe cases, corticosteroid and assisted mechanical ventilation combined with compound sulfamethoxazole could remarkably improve the prognosis of PCP.

当AIDS患者出现发热、咳嗽、呼吸困难、低氧血症、LDH增高及CD4+T淋巴细胞<100×106/L时,结合胸部影像间质性肺炎或磨砂玻璃样改变,临床需考虑PCP;病原学诊断困难,但TBB肺孢子菌检出率高;治疗首选SMZ-TMP,重症病例辅以糖皮质激素和机械辅助通气可改善预后。

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According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm~150rpm时取得最大值,此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世,形体几无变化。

When I was in school, the rabbi explained everythingin the Bible two different ways.

当我上学的时候,老师解释《圣经》用两种不同的方法。