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The main object of this research is to investigate synthesis of Cu23Cl Cu and CuO nanoparticles through electrospinning and heat-treated method The research is mainly focused on preparative parameter and the change of heat-treated temperature to form the nanoparticles inlaid in silicon fibers the shape and color change are dicussed First of all to prepare the Polyvinyl butyral and silica dioxide complex nanofiber by electrospinning and then to investigate different heat-treated temperature and reactive time to being an influence on the products The results detected by SEM XRD TEM EDS FTIR combined sol-gel process and electrospinning can prepare Polyvinyl butyral and silica complex nanofiber The experimental result is found when heat-treated temperature is 100~4750C it can produce Cu23Cl nanoparticles; Above 4750C~ 4900C it can produce Cu nanoparticles; Above 450~7000C it can produce CuO nanoparticles And the viscosity is lain between 20~40cp and the sol-gel process time is 3hr it can produce the thinner fibers The average diameter of the fibers are 107 88±21 01nm;Due to the nanoparticles inlaid in the silica fibers the thinner fibers can be inlaid the smaller nanoparticles so this is the result that the experiment is expected To calcine the complex fibers is to produce surface silica fibers contain Cu23Cl Cu and CuO nanoparticles due to surface plasma resonance it make the color of the fibers become yellowish green from light white green turn into the red nuclear finally As the experimental result to utilize sol-gel process combine electrospinning can produce porous silica fibers contain Cu23Cl Cu and CuO nanoparticles

本研究旨在探讨「利用放电纺丝和热处理法来合成Cu23Cl、Cu和CuO奈米粒」之研究,实验著重在制备参数与热处理温度变化对所形成的奈米粒镶嵌在二氧化矽纤维中的形态与颜色变化探讨。首先,利用放电纺丝法制备出聚乙烯醇缩丁醛及二氧化矽之奈米纤维,比较不同的热处理温度与反应时间的改变对产物生成产生影响,进而研究不同热处理温度和时间对生成奈米粒的影响。产物经由SEM、XRD、TEM、EDS和FTIR等仪器分析结果显示,结合溶胶-凝胶法(sol-gel process)和放电纺丝法可产生聚乙烯醇缩丁醛及二氧化矽复合奈米纤维。实验结果发现,若热处理温度在100~4750C下可得到Cu23Cl奈米粒,475~4900C 可得Cu奈米粒,450~7000C以上可得 CuO奈米粒。而黏度介於20~40cp间和溶胶-凝胶时间为3hr时,可产生直径比较细的纤维,纤维直径为107 88±21 01nm;且由於奈米金属颗粒镶嵌在二氧化矽纤维中,直径比较细的纤维,可以得到比较小的奈米金属颗粒,这与实验预期相符。而锻烧此复合物产生多孔的二氧化矽纤维并包含Cu23Cl、Cu和CuO奈米微粒时,由於表面电浆子共震关系,而使纤维颜色由淡白黄绿色变成黄绿色,再变红褐色。由实验结果得知,利用溶胶-凝胶法(sol-gel process)结合放电纺丝法和不同热处理温度,可产生Cu23Cl、Cu和CuO奈米粒镶嵌在二氧化矽纤维。

In terms of Cauchy s integral formula of analytical complex function and the three order spline function of complex variable, a general boundary solution method is presented for solving the complex potential field of the flow field around a 2D semi infinite body .

采用复解析函数的Cauchy积分公式和物面复势三阶样条函数逼近,提出了一种求解二维半无限体势流绕流问题复势的通用方法。

ESI-MS results showed that α-CD could form 3: 1 specific complex with cinchonine in solution and they formed"sandwich"structure type 〓 inclusion complex when β-and γ-CD were blended simultaneously with cinchonine. Semi-empirical AM1 calculations indicated that the H bonds formed between CD and cinchonine played an important role to stabilize the complex in gas phase.

电喷雾质谱研究发现α-CD与辛可宁在溶液中可以形成特异性的3:1型复合物,当β,γ-CD与辛可宁同时混合时它们可以形成"三明治"型〓包合复合物,半经验AM1方法计算显示氢键的形成对这些复合物的稳定起到重要的作用。

Because the information in groupware system has Characteristic of complex, various, large quantity, non-structure or structure complex, close relativity of information, etc, and the traditional relational database can hardly handle these complex and various information. This paper aims at the problems that groupware system meets in application, put forward the research on groupware system based on object-oriented database management system.

由于群件系统中所处理的信息具有复杂、多样、量大、非结构化或结构复杂以及信息间的相关性紧密等特征,而传统的关系型数据库很难处理这些复杂多样的信息,因此,本文针对群件系统对数据库的应用需求,提出了基于面向对象数据库管理系统的群件系统的研究。

Based on similarity science and complex systems theory, this paper studies the principle of diversity analysis for complex mechanical products system. Based on similarity measure, diversity measure method of parts unit and complex machine is presented.

基于相似性科学和复杂系统理论,研究了复杂机械产品系统差异性分析原理,提出了以相似性度量为基础的零部件单元和复杂机械产品系统的差异性度量方法。

In this paper,at first we transformed the nonlinear elliptic system of 2m first order equations into the complex form, then by use the results on the Riemann-Hilbert problem for nonlinear elliptic complex equation of first order, the method of continuity, the Schauder fixed-point theorem and the Leray-Schauder theorem, we proved that the modified Riemann-Hilbert boundary value problem for the complex system with some conditions is solvable.

本文先将较一般的多个未知函数的一阶椭圆型实方程组化为复方程组,然后讨论这些复方程组在某些条件下的一些边值问题的可解性。这里所考虑的方程组既包含线性的,也包含非线性的,比广义超解析函数所满足的方程组还要广,又本文主要研究较一般的Riemann-Hilbert边值问题,先给出这种边值问题解的先验估计式,然后用参数开拓法及Leray-Schauder定理证明这种边值问题的可解性结果。

And the preparing method has the steps of: fixing the charge transfer complex on a scanning tunnel microscope, starting up the cut mode of the scanning tunnel, controlling the motion of pointer of the scanning tunnel, applying a voltage pulse between the charge transfer complex and the pointer, writing the information hole array in the charge transfer complex.

按如下过程进行制备:将电荷转移复合物固定于扫描隧道显微镜上,启动扫描隧道显微镜的刻写模式,控制扫描隧道显微镜的针尖的运动,在电荷转移复合物和针尖之间施加电压脉冲,在电荷转移复合物上写入信息孔阵。

The taxonomic studies of B. dorsalis complex by morphological and genetic characters are reviewed. It is helpful to apply the molecular approach to taxonomic and phylogenetic analysis for the complex. And the outlook of phylogenetics and behavioral study of the complex will be focuse...

文章概述基于形态学和遗传学特征基础上的橘小实蝇复合体的分类鉴定及系统发育研究进展,介绍近年来分子生物学技术在橘小实蝇复合体分类及系统发育研究中的应用情况,展望系统发育和行为学研究是橘小实蝇复合体未来研究的重点领域。

There is one kind of phenomenon appearing during children's psychological development, namely,children start to split from the integral relationship with their mothers at the age of three and cast their emotion onto their fathers, they even go so far as to compete with their mothers for enjoying their fathers exclusively, this is known as the Oedipus Complex, also known as Electra Complex[2], it was fair to say that Sijia actually had the Electra Complex.

儿童心理发展有一种现象,即到了3岁时开始从自己和母亲的一体关系分裂出来,并且把情感投在父亲身上,甚至要和母亲竞争而独占父亲,称为俄底浦斯情结,又叫恋父情结[2]。

It employs the complex-valued step function to build neural model, then constructs network structure and decides the number of neurons; it adopts complex-valued Hebbian rules and inner product way to calculate the net weight matrix; then it analyzes the convergence of the network by taking advantage of the definition of energy function. In the image pre-processing stage, 2-dimensional Fourier Transform and Euler's formula are used, respectively, to transfer a gray-scaled image into phase information needed by the complex-valued neural network when stores the traffic sign. In the image post-processing stage, phase inverse transformation is used to change the phase image to gray-scaled image.

采用复数阶跃函数构建了神经元模型,建立了复数Hopfield神经网络结构,并且确定了网络中神经元的个数;借助复数Hebbian学习规则和复数内积法给出了网络权值的确定方法;借用复数网络能量函数的定义,说明了复数识别网络的收敛性;在前期的图像数据处理部分,分别使用离散二维傅里叶变换和欧拉公式,给出了将灰度图像数据转化为复数网络所需要的相位信息的方法,实现了网络对路牌的记忆存储;在后期的图像还原部分利用相位逆变换的方法,实现了相位图到灰度图转化。

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相关中文对照歌词
The Tugboat Complex Pt. 3
The Tugboat Complex
Beta Complex
Complex By Degree
Regular And Complex (Gnb)
Complex
The Achilles Complex (Explode!)
My Oedipus Complex
Complex Hate Crimes
Complex Simplicity
推荐网络例句

Neither the killing of Mr Zarqawi nor any breakthrough on the political front will stop the insurgency and the fratricidal murders in their tracks.

在对危险的南部地区访问时,他斥责什叶派民兵领导人对中央集权的挑衅行为。

In fact,I've got him on the satellite mobile right now.

实际上 我们已接通卫星可视电话了

The enrich the peopling of Deng Xiaoping of century great person thought, it is the main component in system of theory of Deng Xiaoping economy, it is a when our country economy builds basic task important facet.

世纪伟人邓小平的富民思想,是邓小平经济理论体系中的重要组成部分,是我国经济建设根本任务的一个重要方面。