查询词典 colloidal solution

This dissertation involves the study of the growth dynamics of colloidal particles under unequilibrium and irreversibility condition. Firstly, it is of interest to investigate whether the ideal diffusion or reaction-limited aggregation universal behavior can be observed for the initially polydisperse practical system of basic yttrium carbonate as well. The fractal structure of basic yttrium carbonate aggregate cluster was observed using transmission eletron microscopy. The aggregation kinetics of basic yttrium carbonate colloids was studed using dynamic 1ight-scattering techniques. At 1.00mol/l NaCl solution the fast diffusion-limited aggregation behavior was observed with an increase in the aggregate size over time described by a power law. The aggregates are characterized by a fractal dimension D=1.82. The disordered and ramified cluster is consisted of primary colloidal particles and tenuous and more open. These are in good agreement with those observed for other colloidal system such as colloidal gold (1.86), silica (1.85) and polystyrene latex (1.82) in diffusion-limited aggregation from the static and dynamic light scattering by Lin. Therefore ideal diffusion-limited aggregation behavior can be observed in practical polydisperse system as well. Smoluchwski and fractal theories were used to obtain the aggregation rate constant for initially polydisperse system for the first time.

本论文研究胶粒的非平衡不可逆聚集动态学，分为两个部分，第一部分是通过实验研究一个新的初始多分散的碱式碳酸钇胶粒实际体系中，聚集标度性质的普适性，即使用透射电子显微技术观测聚集粒子簇的分形结构，使用动态激光光散射研究碱式碳酸钇胶粒的聚集动力学，胶粒带电而产生静电排斥作用使得碱式碳酸钇胶粒处于稳定状态，当加入电解质NaCl溶液时，碱式碳酸钇胶粒间的Debye-Hückel屏蔽距离缩短，从而降低静电排斥能垒，引起胶粒发生不可逆聚集，加入电解质NaCl的浓度为1.00mol/l时，碱式碳酸钇胶粒进行快速聚集，经历扩散控制聚集机理，形成结构疏松、更为开放的分形聚集粒子簇，其分形维数为1.82，碱式碳酸钇胶粒聚集增长动力学遵循幂函数增长规律，与Lin等使用静态激光光散射和动态激光光散射测量硅胶(1.85)、金胶(1.86)和聚苯乙烯胶乳(1.82)在扩散控制聚集状态形成聚集粒子簇的分形维数值以及粒子簇聚集增长的动力学规律相一致，表明胶粒聚集标度性质的普适性质在初始多分散的实际体系中也是存在的，首次由动态激光光散射的实验数据得到初始多分散胶粒分形粒子簇的聚集速率常数，并且其值与Smoluchowski聚集速率理论预期相符。

The invention relates to a way to prepare nickel, manganum and cobalt hydroxide. The method includes making the mixed solution a coprecipitate with mixed solution B in base solution C. The mixed solution A contains nickel salt, manganese salt and cobalt salt, the mixed solution B is a strong base solution, the base solution C is aqueous ammonia solution. The solution A also contains ammonium salt while solution B also contains aqueous ammonia; besides, after being mixed, the molarity of ammonia in solution A and solution B is the same with that in solution C.

一种镍锰钴氢氧化物沉淀的制备方法，该方法包括将混合液A和混合液B在底液C中进行共沉淀反应，所述混合液A中含有镍盐、锰盐、钴盐，所述混合液B为强碱溶液，所述底液C为氨水溶液，其中，所述混合液A中还含有铵盐，混合液B中还含有氨水，并且参于等当量反应的混合液A中的铵盐与混合液B中的氨水在混合液A和混合液B混合后氨的摩尔浓度与底液C中氨的摩尔浓度相等。

Single component and multi\|component of iron system colloidal catalyst \Ali\|Bu\-3CH\-2CHCH\-2Cl\ were mixed by different ratios in hydrogenated gasoline medium at 25℃.This paper studied the relationship between the nonaqueous systematic electroconductivity and the concentration of catalyst components.In combination with Tyndall effect,polymerization experimental results,Ali\|Bu\-3 existed in associated state and dissociated into ionpair.The reaction between Ali\|Bu\-3 and Fenaph\-2 was the main reaction which formed colloidal core.Ali\|Bu\-3 reacted on CH\-2CHCH\-2Cl and Ali\|Bu\-2Cl was yielded which joined the formation of active center on the surface of colloidal core.The excessive Ali\|Bu\-3 was dissociated into ionpair which formed double electrode layer,and the double electrode layer kept the colloidal particles relatively stable.

研究了在25℃加氢汽油介质中，铁系胶体催化剂［Fenaph2Ali-Bu3―CH2==CHCH2Cl］单组分、多组分按不同配比混合，非水体系电导率与浓度的关系，结合Tyndall效应，聚合实验结果，得出Ali-Bu3以缔合状态存在并解离成离子对它同环烷酸亚铁的作用是形成胶核的主要反应，与氯丙烯反应生成的氯化异丁基铝，在胶核表面参与形成活性中心由过量Ali-Bu3解离的离子对形成的双电层结构，使胶粒保持相对稳定。

The method comprises the procedures as follows:(1) the surface of a base plate is treated:(2) colloidal solution is prepared: and (3) the base plate is put into a vessel and the colloidal solution is added into the vessel; the colloidal solution volatilizes under the constant temperature of 20 DEG C to 70 DEG C; the photonic crystal is taken out until no substance volatilizes, and the photonic crystal is made.

本发明方法如下：一、基板的表面处理；二、胶体溶液的配置；三、将基板放入容器中，然后加入步骤二配置的胶体溶液，然后在温度为20℃-70℃的恒温条件下使胶体溶液挥发，待无物质挥发取出基板，即得到光子晶体。

Analysis and discussion on the function of triethanolamine in the colloidal solution are given from the investigation results on the conversion of reaction system into colloidal solution of TEA-Sb〓O〓 and the spectral determinations of the colloidal product.

通过对H〓O〓氧化法制备的TEA-Sb〓O〓胶体溶液的氧化成胶过程的研究，对TEA-Sb〓O〓胶体产物进行光谱检测，分析和讨论了三乙醇胺在胶体溶液中的作用。

The invention discloses an InP quantum point preparing method, comprising the steps of:(1) mixing InCl3 with trioctylphosphine oxide, and preserving heat at 90-110DEG C to prepare a solution whose In content is 0.1-0.3mol/L;(2) raising temperature to 130-180DEG C, and charging argon gas;(3) injecting PSi(CH333 into InCl3-TOPO compound in the molar ratio of 1 to 1-1 to 2;(4) when the solution color turns into transparent red or orange, raising temperature to 260-270DEG C and preserving heat;(5) lowering temperature to 90-110DEG C and injecting dodecyl amine, decyl amine or mercaptan;(6) dissolving reacting mixture in nonpolar solvent to form transparent colloidal solution, then adding in polar solution until the colloidal solution is muddy, and centrifugally separating and obtaining deposits and supernatant; and (7) centrifugally separating the supernatant, where the above steps (1)-(5) are performed.

本发明公开了一种InP量子点的制备方法，其步骤为：①将InCl 3 与三辛基氧膦混合，在90～110℃保温制得In含量为0.1～0.3mol/L的溶液；②升温到130～180℃，通入氩气；③将PSi(CH 3 3 3 注射入InCl 3 -TOPO复合物中，其摩尔比为1∶1～1∶2；④待溶液颜色变为透明的红色或橙红色，将升温260～270℃保温；⑤降温到90～110℃，注入十二胺、癸胺或硫醇；⑥将反应混合物溶于非极性溶剂，形成透明的胶体溶液，然后加入极性溶剂，直至胶体溶液出现混浊状，然后离心分离获得沉积物和上层清液；⑦取上层清液进行离心分离。上述步骤①～⑤在保护气氛下进行。

By the binding of two colloidal particles in Brownian Dynamics Simulation binding, colloidal particles, Brownian dynamics simulation, the two particles, diffusion tensor, hydrodynamics, methods, low Reynolds number, aqueous solution, distance, colloidal suspensions, since correlation function, cross correlation function,...

受束缚的两个胶体粒子的布朗动力学模拟束缚，胶体粒子，布朗动力学模拟，两个粒子，扩散张量，流体力学，方法，低雷诺数，水溶液，距离，胶体悬浮系统，自相关函数，互相关函数，。。。

The intermediates of manufacturing process include the hydrolyzed solution, the aqueous solution of Radix Isatidis extraction, the aqueous solution of Fructus Gardeniae extraction, the aqueous solution of Flos Lonicerae Japonicae extraction, the aqueous solution of baicalin, the alcohol solution of mixteure composed by cholic acid and hyodeoxycholic acid, 4-blended solution, 6-blended solution, the blended solution of baicalin and ASFLJE and 8-blended solution.

清开灵注射剂处方由胆酸、猪去氧胆酸、水牛角、黄芩苷、板蓝根、栀子、金银花和珍珠母组成，其生产过程中间体包括水解液、板蓝根液、栀子液、金银花液、黄芩液、四混液、胆酸混合液、六混液、银黄液和八混液。

We optimized reaction system for labelling-antibody in which the optimal amount of the purified anti-Stx2B IgG conjugated with colloidal gold beads was 60μg/mL, the purified antibody for E.coli O157 was 57μg/mL, the optimal pH was 8.2, the size of colloidal gold partical was 20nm, the optimization of stabilizing agent was BSA, the optimization buffer was boracic acid buffer with pH 8.2, the optimization of preserving fluid and eluant was boracic acid buffer with pH 8.2 including 5mM NaCl-1%BSA, confining liquid for NC membrane was 0.01% PBST with 3%BSA, the amount of polyclonal antibody against E.coli O157 and Stx2 conjugated with colloidal gold beads for conjugate pad was 3μg respectively, the amount of anti-Stx monoclonal antibody for test line was 0.1μg and 1μg for E.coli O157, the amount of goat anti rabbit IgG for control line of both GICA were 1μg.

测定了胶体金颗粒的最优化反应体系：胶体金颗粒的大小为20nm；抗体与胶体金溶液结合的最佳pH约为8.2；最佳蛋白结合量分别为抗大肠杆菌O157 IgG为57μg/mL，抗重组Stx2B IgG为60μg/mL；最佳稳定剂为BSA；最佳缓冲液为pH8.2硼酸溶液；最佳金标保存液和洗涤液为5mM NaCl-1%BSA的pH 8.2的硼酸缓冲液；NC膜的封闭液为3%BSA的0.01mol/L PBST；Stx2试纸条和大肠杆菌O157试纸条的质控线上的羊抗兔IgG的多克隆抗体最佳点样量均为1μg，其检测线的抗Stx2的单克隆抗体的点样量为0.1μg、抗大肠杆菌O157的单克隆抗体的点样量为1μg，结合垫上的金标抗大肠杆菌O157和重组Stx2B多克隆抗体点样量均为3μg。

Pneumophila serogroup 5 antibody to develop two immuo-colloidal gold tests respectively. Main works listed below as:1、Preparation and identification of polysaccharide antigen of L. pneumophila Bacteria of LP1 ~ 7,9 and 10 were cultured on yeast agar buffer activated carbon for three to five days at 37℃, 5%CO2. Protein-free polysaccharide antigens were obtained after harvest in cells, extraction, deproteinization, dialysis and other steps. Their immunogenicities were verified by ultraviolet spectrophotometer full-wavelength scanning and Western blotting.2、Preparation and identification of rabbit anti-LP1 antibodies and rabbit anti-LP5 antibody Rabbit anti-LP1 and anti-LP5 antibodies were purified after rabbits were immuned with antigens isolated as described above. The purities of both antibodies were above 80% and the titer of blood serum 1:32 tested by double antibody sandwich assay.3、Development of colloidal gold immunochromatographic assay kit The size of colloidal gold particles in the kit was 25nm. The optimal concentrations for antibodies were 30μg/ml and the sensitized concentrations of NC membrane were 5 mg/ml.

主要研究工作从以下几个方面进行：1、LP1~7、9和10型多糖抗原的制备与鉴定将LP1~7、9和10型菌株分别接种在缓冲活性炭酵母琼脂培养基上，37℃、5%CO2的条件下培养，3~5天后洗下菌苔，经抽提、除蛋白、透析等步骤后得到基本无蛋白的LP多糖抗原，经紫外分光光度仪全波长扫描及Western blotting验证其抗原良好。2、兔抗LP1抗体和兔抗LP5抗体的制备与鉴定分别用LP1、LP5型多糖抗原免疫家兔，采用琼脂糖双向扩散试验检测，两种抗体血清效价均为1：32；饱和硫酸铵法提取抗体，SDS-PAGE检定其抗体纯度均达到80%以上。3、胶体金免疫层析检测试剂的初步研制采用柠檬酸三钠还原法制备约25nm大小的胶体金颗粒；分别制备兔抗LP1抗体、兔抗LP5抗体的金标探针，两种抗体的最适标记量均为30μg/ml；选择适当孔径的微孔滤膜为载体包被两种抗体，NC膜包被浓度均为5mg/ml。

The network space is the typical form of abstract space when it comes to the digital stage.

网络空间是抽象空间数字化阶段的典型形式。

The Notarial System,as the system of judicial certification in our country,is both the constructor and the defender of social credit system,It has its special value and function in the social honesty.

公证制度作为我国司法证明制度，既是社会信用体系的建设者，同时也是社会信用的捍卫者，在诚信中有其特殊的价值和功能。