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The conclusions were as follows: theνO-H andνC=O IR absorption maxima shifted towards higher wave numbers after imprinting 17β-estradiol on TFMAA-co-TRIM copolymer with the red shift of theνO-H groups being apparent after precipitation polymerization for 16h while that forνC=O groups being observed after polymerization for 24h. A strong interaction between TFMAA and 17β-estradiol was confirmed by the high selectivity for 17β-estradiol, as indicted by the values of the separation factor of isomers of 17β-estradiol/17α-estradiol (2.28) and the imprinted factor (3.01). Particle diameter of TFMAA-co-TRIM polymer was between 300 nm and 1.5μm, which suited well for solid phase sorbent throughout at low column pressure. The recognition of imprinting TFMAA-co-TRIM polymer for sterol molecules was driven by enthalpy eluted with acetronitile, and low temperature was in favor of the separation of sterol structure analogues on imprinting column. TFMAA-co-TRIM polymer possessed of determinate anti-heat stability, with melting point beginning at 255.84℃, Tp=257.40℃, control TFMAA-co-TRIM polymer and imprinting TFMAA-co-TRIM polymer were respectively decompounded at 267.79℃and 343.11℃, and solid micro-extraction noddle prepared by the special polymerization also showed definite recognition for 17β-estradiol by GC/MS detecting at 270℃. By selection of various washing and elution solvents, elution reagents of close polymerization system were of more advantage in template molecules retention and recognition on molecularly imprinted solid phase extraction column. At a certain extent, progesterone, 17α-estradiol, 17β-estradiol and 4-androstene-3, 17-dione could be intercepted on the MISPE column. Especially, MISPE had high selectivity for progesterone, and imprinting TFMAA-co-TRIM polymer could achieve adsorption balance within 50 min by absorption kinetics test for 17β-estradiol. However, MISPE column showed better selectivity and enrichment property for 17β-estradiol than C18 and CSPE columns according to the data from HPLC and GC/MS analyses. Recovery of 17β-estradiol on MISPE column was up to 85.5% while when prime extracting solution of milk powder was sampled, the recovery of CSPE and C18 columns were 43.7% and 30.7%, respectively.

通过研究阐明:紫外聚合产物TFMAA-co-TRIM中的νO-H振动吸收峰在聚合16h后红移,νC=O振动吸收峰在聚合24h后红移;TFMAA-co-TRIM对雌二醇异构体的印迹因子达到了3.01,α为2.28,优于其它功能单体参与得到的聚合物识别特性;TFMAA-co-TRIM聚合物粒径介于300 nm至1.5μm之间,作为色谱固定相具有良好的通量和低的柱压;在乙腈流动相中,TFMAA-co-TRIM分子印迹固定相的分离过程主要被焓驱动,低温有利于分子印迹固定相分离甾醇结构类似物;TFMAA-co-TRIM分子印迹聚合物在255.84℃时开始熔融,Tp=257.40℃,聚合物CP的降解温度在267.79℃,MIP降解温度在343.11℃,制备的固相微萃取头初步经GC/MS 270℃的耐热性测定;不同的洗提溶剂筛选证明了选择接近聚合溶剂的洗脱体系更有利于MISPE发挥识别效应;分子印迹固相萃取柱对孕酮、17α-雌二醇、17β-雌二醇和雄烯二酮都具有不同程度的保留特性,可作为此类化合物的吸附材料,特别对孕酮强保留的富集特性,可作为孕酮的选择性识别吸附剂,其分子印迹聚合物对17β-雌二醇的吸附动力学测定显示在50 min内基本达到吸附平衡,具有作为传感器核心敏感材料的潜力;对比萃取奶粉中17β-雌二醇性能,MISPE柱比非分子印迹固相萃取柱和C18柱具有更高的保留,回收率依次为85.5%,43.7%和30.7%。

Edge in the joint International Trade Co., Ltd. and China Minmetals Group, China Steel Group in both the business maintained good cooperative relations, and Japan Metals and Minerals Co., Ltd., Japan Yan Gu, Inc. maintained a long-term business in the domestic market, we Company and the Tangshan, Tianjin, Shanxi and many other outstanding domestic enterprises to establish a stable cooperation, in India, Iran, such as iron ore projects in Thailand and three in Shanxi Science and Technology Development Co., Ltd., Heng On Tangshan Industry Co., Ltd., Shanxi money Steel Co., Ltd., Shanxi Dynasty Iron and Steel Co. Ltd. to establish a long-term cooperation in the iron oxide powder with the Tangshan overseas trade center established a strategic cooperative projects. Edge in the joint International Trade Co., Ltd.

中边联合国际贸易有限公司与中国五矿集团、中国中钢集团均保持着良好的业务合作关系,同时与日本五金矿产株式会社,日本岩谷产业株式会社保持着长期的业务,在国内市场方面我们公司与唐山、天津陕西等多家国内优秀企业建立了稳定的合作,在印度、伊朗铁矿等项目中与山西三泰科技发展有限公司、唐山恒安实业有限公司,山西金元钢铁有限公司,山西王朝钢铁有限公司建立了长期的合作,在氧化铁粉方面与唐山海外贸易中心建立了战略合作项目。

Long-term supply contract on ship deck hatch covers and roll-on-roll-off ship equipments with the total value of 130,233,205 USD as concluded before July 1, 2007 with foreign clients by MacGREGOR Group OEM Enterprises 48,249,183 USD by Nantong Rainbow Heavy Industries Co., Ltd., 32,284,275 USD by Nantong COSCO Ship Steel Structure Co., Ltd., 13,960,905 USD by Nantong Jiaolong Heavy Industry Group Co., Ltd., 16,131,786 USD by Shanghai Keyon Marine Equipment Co., Ltd., 14,085,111 USD by CSSC Jiangnan Heavy Industry Co.,Ltd., 369,629 USD by Chongqing State-owned Chuandong Shipyard, 530,000 USD by Zhangjiagang Hejia Steel Structure Co., Ltd., and 1,859,316 USD by ZhangJiaGang AnYuan Steel Construction Co.

麦基嘉集团定牌生产企业(南通虹波重工有限公司48249183美元、南通中远钢结构有限公司32284275美元、南通蛟龙重工发展有限公司13960905美元、上海凯航通力船用设备有限公司16131786美元、中船江南重工股份有限公司14085111美元、重庆国营川东造船厂369629美元、张家港市禾佳钢结构有限公司530000美元、张家港市安远钢结构有限公司1859316美元)在2007年7月1日之前与外国客户签订的总金额为130233205美元的船甲板舱口盖和滚装船设备的长期供货合同。

In this study, the constant volume visual method is used to measure the critical point properties of CO 2+toluene, CO 2+cyclohexane, CO 2+ n butyraldehyde, CO 2+ i butyraldehyde, CO 2+methanol and CO 2+ethanol binary systems.

采用固定体积可视观察法测定了 CO2 +甲苯、CO2 +环己烷、CO2 +正丁醛、CO2 +异丁醛、CO2 +甲醇及 CO2 +乙醇二元体系的临界点性质,为超临界萃取和化学反应提供基础数据。

Under all levels partys and government's concern, the enterprise has become a diversification group integrating producing, scientific research, management with trade into one unity. It has more than 400 employees and the total area reaches 160 acreages. There are several subordinates: Pinhu Tianyi cybernate sanitary science and technology co., ltd. Pinhu Tianyi cybernate gas appliance science and technology co., ltd. Shanghai Tianyi sanitary co., ltd. Pinhu Xingcang gas station. Pinhu Tianyi petrochemical co., ltd. Pinhu Jinxing liquid gas co., ltd. Zhongke Tianyi lightening co., ltd,etc. The network of the key products---brand Yingjiesha series cybernate steaming shower room, gas appliance, soot-removal machine has covered all the main cities and areas of the country. To 2007, the sales income of the whole enterprise reaches 250 millions Yuan.

10余年来,企业在各级党委、政府的大力关怀下,现已成为一家集生产、科研、管理、工贸于一体的多元化的集团型企业,拥有职工600余名,总占地面积约180亩,下属企业有:平湖市天一电脑洁具科技有限公司、浙江天一厨卫制造股份有限公司、上海天一洁具有限公司、平湖市新仓加油站、平湖市天一石油化工有限公司、平湖市金新液化气有限公司、浙江中科天一照明有限公司、江苏淮安天诚科技有限公司等,核心产品"英洁莎"牌中高档电脑系列蒸汽淋浴房、燃气具、油烟机等已远销欧美等国家,2007年全企业实现销售收入2.5亿余元。

After three years working experience, we has achieved many design projects successfully includes, the second stage landscape engineering design of Huankou Garden developed by Wuhan Real Estate Investment Group, the planning design and architecture design of Zonglian International Residential District developed by Wuhan Zonglian investment Co., Ltd, Phoenix Town developed by Wuhan Huayi Real Estate Co., ltd, Chutian Thermal Spring Hotel developed by Liannin Jingjiang Tourism company, Enshi Genevese Amorous District, the landscape design for new office building of Wuhuan Tech joint-stock co., ltd, landscape design for headquarter of Zhongye Southern Engineering Technical Co., Ltd, office and technical research building of Zhongtie 11 bureau, landscape design for the Xiangshan Minyuan developed by Yichang Hongxiang group Co., Ltd, planning for the Tingtao Guanhai district developed by Wuhan Hongyu Industry Co., Ltd and etc. all of the projects above got the good estimate form our clients.

公司成立三年以来,出色地完成了多项设计工作,其中包括武汉地产开发投资集团的汉口花园二期景观工程设计、武汉众联投资有限公司的众联国际小区的规划、建筑设计、武汉市华盈房地产有限公司的凤凰城、咸宁锦江旅业公司的楚天温泉假日大酒店、恩施日内瓦风情小区、五环科技股份有限公司新办公大楼景观设计、中冶南方工程技术有限公司总部景观设计、中铁十一局集团有限公司办公科研楼、宜昌弘洋集团公司的香山铭苑景观设计、武汉宏宇实业有限公司的听涛观海的规划、建筑与景观设计等项目,深受各开发商和业主的好评。

By use of the Fischer-Tropsch reaction in a C-H-O system, we discussed the relationships between inorganic CO〓 and some physical chemistry conditions, such as Oxygen flee degree , temperature, pressure, other objects consistency and catalyzer. a when T=200K~2000K, if f〓>0, the reaction of generating CO〓 will be dominant, CH〓 hardily exists; b when T>1000K, CH〓 is not propitious to exist, carbon in system almost exists in form of CO〓; c the more pressure, the more CO〓 is propitious to exist; d the more consistency of CO, O〓 and H〓O, the more CO〓 is propitious to exist, the more consistency of H〓, the more CH〓 is propitious to exist.

依据C-H-O体系费托反应的简化模型,讨论了氧逸度、温度、压强、其它物质浓度、催化剂等物理化学条件对无机成因CO〓生成的影响,从理论上讨论了在地质环境中,无机成因CO〓存在的物理化学条件:1在T=200K~2000K的温度范围内,体系中一旦氧逸度>0,生成CO〓的反应将占绝对优势,CH〓几乎不可能存在;2T>1000K时,不利于CH〓形成,使体系中的碳主要以CO〓的形式存在;3体系压强越大,越有利于CO〓的形成;4反应物CO、O〓、H〓O的浓度越高,越有利与CO〓的存在,H〓的浓度高有利于CH〓的形成。5地质成藏作用可以经历很长的地质年代,这足以补偿矿物岩石中的Ni、Mo、Fe、Co、Ru等催化性能的降低及其它动力学条件的不足,使得费托反应可能发生,从而生成无机成因的CO〓和烃类。

The company now possesses Zhejiang Zeen Fasteners Co., Ltd., Zhejiang Zeen Metal Products Co., Ltd., Zhejiang Alite Machinery Co., Ltd., Shaoxing Commercial Real Estate Development Co., Ltd., Hangzhou Far East Steel Co., Ltd., Zhejiang Hongfei Zeen Holding Co., Ltd., etc.

现己拥有浙江泽恩标准件有限公司、浙江泽恩金属制品有限公司、浙江艾耐特机械有限公司、绍兴商业房地产开发有限公司、杭州远东钢铁有限公司、浙江泽恩控股有限公司、浙江泽恩实业集团有限公司、浙江泽恩投资有限公司等多家控股、参股公司。

Firstly, the basic concept of software/hardware co-design and the present research situation worldwide is introduced, the techniques are also discussed separately in the thesis, which is in the system description stage, system architecture design stage, hardware/software design and implementation stage. Secondly, combined with three representative methods of hardware/software co-design systems: POLIS、VULCAN and CORSAIR, the main steps of co-design are studied and analyzed including system description, hardware/software partitioning and hardware/software implementation-synthesis, and some new ideas are given here. Thirdly, UML and modeling technology of embedded systems using UML are described clearly, a handheld terminals is a good example for this, furthermore, the algorithm of how to convert the UML diagram into SystemC codes is mainly concerned on in this thesis. Fourthly, the basic concept of SystemC is described, and the SystemC Modeling platform and simulation mechanism are analyzed, software/hardware co-design methods using SystemC are discussed. Finally, by applying co-design ideas using UML and SystemC, software/hardware co-design system using UML and SystemC is preparatorily implemented, which is to establish a development environment for designing embedded system.

本文首先介绍了软硬件协同设计的基本概念和国内外研究现状,并分别论述了系统描述阶段的技术、系统结构设计阶段的技术、软硬件设计与实现阶段的技术;接着结合POLIS、VULCAN和CORSAIR 三种有代表性的软硬件协同设计方法,对系统描述、软硬件划分、软硬件实现综合等几个主要设计步骤进行了研究与分析,并提出了新的方法和思路;然后详细介绍了UML及基于UML的嵌入式系统建模技术,并以嵌入式手持终端系统来举例说明,重点研究将UML的视图转换成SystemC代码的算法;其次介绍了SystemC的基本概念,分析了SystemC 的建模平台和仿真机制,并对基于SystemC 的软硬件协同设计方法进行探讨;最后应用基于UML和SystemC的软硬件协同设计的设计思路,初步实现基于UML和SystemC的软硬件协同设计的设计系统,目的是建立一个用于嵌入式系统设计的开发环境。

The present number of 368 corporate employees, annual sales of 80,000,000 yuan, annual production of more than 12,000 tons of various casting and foundry equipment production, the main production facilities, such as the United States Hunter production line in Zhejiang round of the Bank of Machinery Co., Ltd., Zhejiang Leo shares Ltd., the first Shanghai Textile Machinery Plant, China Precision Machine Tool Plant Jack, Warner, Ningbo and Taizhou of good casting Co., Ltd., Suzhou Wujiang David Weir Iron Foundry Co., Ltd., Xianju Hydraulic Casting Plant, Sally Home Shuangshi foundry, Xianju Hengxi machinery plant, Linhai City, a strong metal Manufacturing Co., Ltd., Zhejiang Province made a total of Linjiang Casting Co., Ltd., Taizhou ......, Bo Li Machinery Co., Ltd. and Italy for the meat grinder, Spain pumps, water pumps Perkins Germany, the United States Cummins customers abroad pumping facilities and so on.

本企业现有职工人数368人,年销售8000万元,年生产各类铸件12000多吨及铸造设备制作,主要生产配套,如美国亨特生产线、浙江银轮机械股份有限公司、浙江利欧股份有限公司、上海第一纺织机械总厂、中国杰克精密机床厂、宁波华纳公司、台州通顺铸造有限公司、苏州吴江市震堰球铁铸造有限公司、仙居液压件二厂铸造公司、仙居双狮铸造厂、仙居横溪机械厂、临海市坚强金属制造有限公司、浙江临江共发铸造有限公司、台州博立机械有限公司。。。。。。,并为意大利绞肉机、西班牙水泵、德国帕金斯水泵、美国康明斯水泵等国外客户配套。

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