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The synthetic route starts from penicillin G, peroxyacetic acid(8.5%) as Oxidizing Agent to get penicillin G sulfoxide; esterifided with p-nitrobenzyl bromine to synthesize penicillin G sulfoxide ester; we synthesize 3-exomethylenecepham sulfoxide ester with phthalimide potassium and 4A molecular sieve as acid scavenger to open the ring, SnCl_4 as catalyzation to close the ring. The yield is over 60%.
本研究采用的合成路线为:以青霉素G钾盐为原料,选用工业过氧化氢制备的过氧乙酸(22.3%)稀释至8.5%为氧化剂,氧化得青霉素亚砜;采用对硝基溴苄为酯化试剂,制备青霉素亚砜酯;以NCP(N-氯代邻苯二甲酰亚胺)为开环试剂,酞酰亚胺钾和4A型分子筛为酸清除剂,顺利开环;再经无水SnCl_4催化闭环得3-环外亚甲基头孢亚砜酯,最终产率在60%以上。
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During these events, the potassic volcanic rocks of Oulituozi were produced during extension stage of the rift with subsequent fractional crystallization and derived from basaltic magma. The genesis of the volcanic rocks possibly had a close relation with partial melting of the subducted slab of Pacific Plate oceanic crust.
欧利坨子富钾质火山岩的形成是裂谷期岩石圈伸展作用的产物,是玄武质岩浆经过大比例分离结晶作用的产物,可能与晚中生代太平洋板块俯冲残片的部分熔融有密切关系。
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Relative contents of four main cellular proteins corresponding to MALDI-TOF-MS peaks m/z 4466, m/z 6455, m/z 6514, and m/z 7772 were all found to be close correlated with the concentration of melamine, although their up- and/or down-regulations showed different patterns when the concentration of melamine changed. Support vector regression leave-one-out method, with the optimized polynomial kernel function and a poly-degree of 3, was chose to evaluate the correlation between the alteration of Tetrahymena pyriformis main proteins'relative contents and the concentration of melamine in the culture medium.
支持向量机软件中支持向量回归support vector regressi(来源:A3cBC17论b1文网www.abclunwen.comon, SVR留一法预报结果表明,选用幂指数为3的多项式核函数进行建模,相对误差的平均值为7.238%,说明梨形四膜虫主要蛋白质相对含量的变化与培养基中三聚氰胺浓度变化相关。
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Results Resinic artificial teeth deposited with 50nm amorphous diamond film after pretreated with polarization are most close to the natural enamel. Conclusion Nanometer amorphous diamond film improves significantly the wearing resistance of resinic artificial teeth.
结果:纳米非晶金刚石薄膜能显著提高树脂人工牙耐磨性能;两种预处理方法中,极化法实验组的耐磨性能明显优于紫外光照法实验组;极化处理后镀膜50nm的人工牙的耐磨性能最接近于天然牙釉质。
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In this study, we use Computer Aided Diagnosis Axiogragh recorded condylar movement of normal occlusion and Angle class two division one subdivision malocclusion with mandibular retrusion every twenty-five during mandible open and close, protrusion and retrusion, and medio-free movement. Then we analysis the deference in order to find out the characteristic of condylar movement of Angle class two division one subdivision malocclusion with mandibular retrusion and the change regularity among befor and after functional appliance treatment.
本研究以正常牙合和下颌后缩型安氏Ⅱ类1分类错牙合各25名为研究对象,采用髁突运动轨迹轴图描记仪(Computer Aided Diagnosis Axiogragh)记录其下颌在开闭口、前伸后退和侧方运动时髁突的运动情况,对比分析下颌后缩型安氏Ⅱ类1分类错牙合的髁突运动轨迹特征及其功能矫治前后髁突运动轨迹的变化。
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The main point of this paper lies in the research on the microstructure of the mullite—cordierite sagger, which has been used in the production of Jingdezhen ceramic industry in large quantities for many years, by means of a polarization microscope with ultrathin section together with close connection of the process in the sagger manufacture.
本文主要是利用偏光显微镜和超薄光薄片并紧密结合匣钵的制造工艺,对景德镇市多年来一直在陶瓷生产上大量使用的&莫来石—堇青石质匣钵&进行了显微结构的研究,发现这种匣钵材料的主晶相是堇青石,次晶相是刚玉和莫来石,并发现其中各晶相成团聚状分布;另外在磨制超薄光薄片过程中,发觉其结构较疏松。
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I had been close friends with them since my boyhood days when I had played badminton and tennis with Mrs. Hooi Seah
我和刘太太陈君玉从小一起打羽球和网球
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Level set method introduced by Osher and Sethian is a numerical method, which translates the problem of evolution of 2-D (3-D) close curve into the evolution of level set function in the space with higher dimension. Level set is an accurate and steady algorithm; it can treat with the change of topology naturally.
水平集方法是由Osher和Sethian提出的一种数值计算方法,它将二维的闭合曲线的演化问题转化为高维空间中水平集函数曲面演化的隐含方式来求解,具有拓扑结构可自然变化、计算精度高、算法稳定的特点。
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The first to the market to buy a 3.3 jin of Solen, the school had a fair balance, not lack of weight (easily took the hands of the scale, the hawkers did not lack the basic weight), rushed to the 168 before 4:30, LG said, Let me Inside, and so on, he went outside to see the 168 selling price of seafood, the young girl to go out at the same time we bought Solen to the woman outside the wash (later know her as the young girl close to the checkout She handed over the money), I married a curious look on the outside to wash her, did not expect to see them sent to wash and burn the whole process of their guests to the Solen Add Taipen together, and mix with the other, one by one After the water washed into another Dapen months, and then look at the list of weight, you remove a few scales of the two, this is the Solen-after guests, because our Solen she is, she did not see I have to stand behind LG, when we raised objections, she said the amount was more or less the same now that you are both 2.7, 6, are the two intestines, comrades, 3.3 Solen two of her final with water scale Only two were 2.7, we get to the stomach, how many ah!
第一次是在市场买了3.3斤的竹蛏,学校有一个公平的平衡,而不是缺乏重量(轻松了手中的规模,小贩都缺乏基本的重量),送往168前4: 30日, LG电子表示,让我内,因此,他走到外面看到168售价海鲜,年轻姑娘走出去的同时,我们买的女子竹外洗(后来知道她的作为年轻的姑娘接近结帐她交出钱),我嫁给了一个奇怪的外观外洗她,没想到看到他们送到清洗和烧伤的全过程,他们的客人的竹蛏购买Taipen在一起,与其他组合,一个又一个的水清洗后,到另一个Dapen个月,然后看看名单重量,您删除一些尺度的两个,这是竹蛏,后客人,因为她是我们的竹蛏,她没有看见我站在后面LG电子,当我们提出异议,她说,数额大致相同,你现在都7月2日, 6日,是两个肠子,好同志, 3.3竹两个她最后与水规模只有两个是2月7日,我们到达胃部,有多少啊!
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In the company, German fast original output equipment was introduced, and the company was equipped with computer systems of CAO/CAM/CAE,PRO/E,UG,SOLIO,WORKS, and close cooperation in product research and development, and technical cooperation were established with lighting technology research institutes and international top experts in Germany, Spain, Hong Kong.
1998年,东莞市三立灯饰有限公司成立,三立集团再次投资近亿元在广东省东莞市建立起面向世界的研发,生产基地,引进德国快速原型输出设备,配备CAO/CAM/CAE,PRO/E,UG,SOLIO,WORKS等电脑系统,并与德国,意大利,西班牙,香港等照明技术研发机构和国际顶级专家,建立起紧密型的产品研发和技术合作关系。
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I am accused of being overreligious," she said in her quiet, frank manner,"but that does not prevent me thinking the children very cruel who obstinately commit such suicide.""
客人们在卡罗利娜·埃凯家里,举止就文雅一些,因为卡罗利娜的母亲治家很严厉。
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Designed by French fashion house Herm è s, this elegant uniform was manufactured in our home, Hong Kong, and was the first without a hat.
由著名品牌 Herm è s 设计,这件高贵的制服是香港本土制造,是我们第一套不配帽子的制服。
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Do not 'inflate' your achievements and/or qualifications or skills .
不要 '夸大' 你的业绩或成果,条件或者技能。