查询词典 chromatography

Ferritin from the liver of a salt water fish, Dasyatis akajei, herein called DALF, was isolated and purified by thermal denaturation, ammonium sulphate fractionation and ammonium reverse extraction, Sephacryl S-300 gel filtration and DEAE- cellulose anion exchange chromatography.

通过热变性处理、硫酸铵分级沉淀、排阻层析和离子交换层析等技术，分离纯化了魟鱼肝铁蛋白Liver ferritin of Dasyatis akaiei。

In present study, a liquid-liquid extraction method was employed to extract the volatile components in mulberry fruit sparkling wine. The analysis with gas chromatography-mass spectrometry detected 69 peaks, among which 63 volatile components were identified. The first 9 volatile components with high relative content were benzyl alcohol, 2-methyl-1-butanol, mono-(2-ethylhexyl)-1, 2-benzene dicarboxylic acid, 3-methyl-1-butanol, toluene, acrylic acid butyl ester, 1H-indole-3-ethanol, isodecyl octyl phthalate and decyl octyl phthalate.

采用液－液萃取法提取桑椹汽酒中的挥发性成分，经气相色谱－质谱联机分析，共检测出69个峰，鉴定出63种挥发性化合物，其相对含量排在前9位的挥发性化合物分别是苯乙醇、2-甲基－1-丁醇、1，2-苯二酸单（2-乙基）己酯、3-甲基－1-丁醇、甲苯、丙烯酸丁酯、1H-吲哚－3-乙醇、邻苯二甲酸异癸基辛基二酯、邻苯二甲酸癸基辛基二酯。

The invention discloses a method for extracting polysaccharide from chiretta and an application, which comprises breaking dry chiretta via a breaker into powder, arranging into an extraction pot, adding ligarine to reflux and defat, adding distilled water into defatted residues to extract, processing alcohol precipitation and centrifugation to obtain deposits, removing protein, processing acid hydrolysis and gel chromatography separation, freezing and drying to obtain active chiretta polysaccharide.

本发明公开了一种从当归中提取多糖的方法及应用。干燥当归用粉碎机粉成粉末，置入提取罐中，加入石油醚回流脱脂，向脱脂后的残渣中加入蒸馏水提取，醇沉、离心得沉淀，除去蛋白、酸解、凝胶色谱分离、冷冻干燥得到活性当归多糖。

Single dibasic acid can be identified by infrared spectroscopy while mixed dibasic acids have to be differentiated by paper chromatography in isopro-panol-ammonia system.

单一的二元酸可用红外光谱法鉴定，而混合二元酸则必须在异丙醇-氨水展开剂中用纸层析来鉴别。

Single dibasic acid can be identified by infrared spectroscopy while mixed dibasic acids have to be differentiated by paper chromatography in isopro-pan...

用顺丁烯二酸酐固化的环氧树脂经水解与分离后得到的主要是反丁烯二酸和少量顺丁烯二酸，前者的含量随固化温度的提高而增多，因而确证这一顺-反异构化反应是在固化过程中受热，而不是在水解，酸化时受化学试剂的作用产生的。

This study developed a new method on the determination of carcinogenic disinfection by-products-trace dichloroacetic acid and trichloroacetic acid in tap water by ion chromatography-electrospray-tandem mass spectrometry(IC-ESI-MS/MS).

建立了一种采用离子色谱-串联电喷雾四级杆质谱联用技术检测自来水中可致癌的饮用水消毒副产物二氯乙酸和三氯乙酸的方法。

The epoxide groups of the column were modified by a reaction with diethylamine that affords ionizable functionalities required for ion exchange chromatography.

用该柱对白介素-18进行了分离，同时考察了不同固定相、缓冲液体系、pH值、盐的类型以及有机添加剂对白介素-18分离效果的影响。

Methods: water decocting method for extracting method, ether as extraction solvent with high performance liquid chromatography, as the means, to test content of methanol 0-3 % diethylamine (73:27) as mobile phase, 242nm detected wavelength, according to the packing: Hypersil BOS C18 5 muon m size: 6 mm (4): 25 mm, standard curve basic linear, precision, accuracy, good stability and.

以水煎煮法作为提取方法，乙醚作为萃取溶剂，以高效液相色谱作为含量检测的手段，以甲醇-0。 3 %二乙胺(73∶27)作为流动相，检测波长242nm，依利特填料：Hypersil BOS C18 5μm 尺寸：4。 6 mm ×250 mm ，结果：标准曲线基本呈线性，精密度，稳定性和准确度良好。

The epoxide groups of the column were modified by a reaction with diethylamine that affords ionizable functionalities required for ion exchange chromatography. The influences of the contents of the cross-linker and porogen on column pressure were investigated.

考察了交联剂及致孔剂用量对色谱柱压力的影响，发现：随着交联剂用量的减小，致孔剂用量的增大，柱压下降；当交联剂和致孔剂用量达到一定水平后，柱压变化不再明显，但柱体机械强度降低。

High performance liquid chromatography-photodiode array detection-elctrospray ionization mass spectrometry (HPLC-PAD-ESI-MS) method was used to determine secoisolariciresinol diglucoside qualitatively and quantitatively. Precision, stability, limits of quantification, SDG recovery and sample preparation method were studied.

采用高效液相色谱－二极管阵列检测－电喷雾质谱(HPIC-PAA-ESI-MS)法对开环异落叶松树脂酚二葡萄糖苷进行定性和定量检测，研究方法的精密度、稳定性、定量检测限及加样回收率，并考察样品制备方法对定量检测结果的影响。

And Pharaoh spoke to Joseph, saying, Your father and your brothers have come to you.

47：5 法老对约瑟说，你父亲和你弟兄们到你这里来了。

Additionally, the approximate flattening of surface strip using lines linking midpoints on perpendicular lines between geodesic curves and the unconditional extreme value method are discussed.

提出了用测地线方程、曲面上两点间短程线来计算膜结构曲面测地线的方法，同时，采用测地线间垂线的中点连线和用无约束极值法进行空间条状曲面近似展开的分析。