查询词典 chromatography

Omeprazole racemate was resolved respectively by simulated moving bed chromatography and batch chromatography with the coated cellulose triphenylcarbamate as chiral stationary phase and ethanol containing 0.1% diethylamine as mobile phase.

用纤维素三苯基氨基甲酸酯涂敷型手性固定相和含0.1%二乙胺的乙醇溶液，研究了模拟移动床色谱和间歇色谱对奥美拉唑对映体的拆分。

The antimicrobial test and researched was done on wide distillation of different solvents on Terpenoid, polarity separation of ethanol distillable substance, thin layer chromatography of different polarities and distillation of amylase. The results showed that the active substance distilled by 95% ethanol and V methanol: toluene=3:1 had stronger antimicrobial activity on Agaricus blazei Murrill. The antimicrobial activity of ethyl acetate was stronger than wide distilling substance with ethanol, but the water part has not antimicrobial effect. Two straps of ethyl acetate phase（Rf0.57、Rf0.63）(0.1g/ml)had stronger antimicrobial activity on Agaricus blazei Murrill, the antimicrobial zone on Pseudomonas was 19.3mm. The bacteriostatic activity of chromatography strap of water phase was rather weaker, the water solution (0.5g/g) of amylase had better effect on pathogenic fungus of Agaricus blazei Murrill, its antimicrobial zone on Aspergillus niger, Citrinin, Trichoderma viride were 10.8 mm, 7.9 mm, 5.3 mm.

通过对日本凹顶藻以不同溶剂的粗提、乙醇提取物的极性分离、不同极性的薄层层析和多糖的提取，进行抗菌试验的研究，发现95%乙醇和V甲醇：甲苯为3∶1的提取的活性物质具有较强的抗姬松茸的病原细菌活性，乙酸乙酯相对病原细菌的抑菌强于乙醇的粗提物，而水相基本无抑菌效果，乙酸乙酯相的两个带（Rf0.57、Rf0.63）浓度为0.1g/ml具有较强抗姬松茸病原细菌的活性，对假单孢杆菌抑菌圈达到19.3mm，水相层析带的抑菌活性较弱，多糖的粗提物配成0.25g/g的水溶液对姬松茸病原真菌有较好的抑菌效果对黑曲霉、桔青霉和绿色木霉的抑菌圈分别达到10.8 mm、7.9 mm、5.3 mm。

The antifungal activities of these materials were investigated and build foundation to develop low poison plant antifungal products. In experiment, polyphenols were extracted by reflux ectraction method which applyed petroleum ether to degrease and methyl alcohol solvent. Phenolic hydroxyl were examined and inspected by colour-developing reaction and the content of total polyphenols was determined by UV-spectrophotometry. Screening test were performed to the antifungal activities of polyphenol extraction by the tube dilution method to the selected ten pathogenic fungus such as Dothiorella gregaria, Rhizoctonia solani, Phyllosticta pirina, and the minimal inhibitory concentration were measured. The column chromatography and thin layer chromatography were applyed to separate and analyse cortex extracts of Dracaena cochinchinensi Lour.

实验部分采用以石油醚脱脂，甲醇为溶剂的回流提取法来提取植物多酚，用显色反应检识酚羟基；采用紫外分光光度法对多酚粗体物进行总多酚含量的测定；选取了聚生小穴壳菌、立枯丝核菌、梨叶点霉等10株常见农林业致病真菌，采用试管液基稀释法对多酚粗提取物进行了抗真菌活性筛选试验，并测定其最低抑菌浓度；采用柱层析法和薄层层析法对其中抑菌效果较好的龙血竭进行分离分析，根据其中3种化合物的光谱数据UV、IR、~(13C-NMR、1H-NMR和MS鉴定其结构。

Alpha-fetoproteinhas been separated and purified from 3～5 months embryon by using salting out, gel chromatography and affinity chromatography.

甲胎蛋白（Alpha-fetoprotein，AFP）可从胎儿组织、胎儿心血、胎儿肝脏、羊膜液、脐带血清、肝癌患者血清和腹水等多种材料中分离获得，分离纯化方法国内外已有不少报道［1～6］。

Y. Wu et Hsuan gave twenty two compounds by the separation methods of column chromatography and preparation thin layer chromatography.

我们从紫花野芝麻的乙醇提取物中分离得到了22个化合物，运用化学和波谱学方法鉴定了其中的20个化合物的结构，这些化合物均首次从该植物中分离得到。

Methods Isothiocyanic acid base phenyl ester pre-column derivatization was used for the determination of three kinds of amino acids contents in the glu-ala-glycine chewable lablet by high performance liquid chromatography,the chromatography condition was inertsil ODS-3V4.6×250mm,5μm

方法谷丙甘氨酸咀嚼片中3种氨基酸含量测定采用异硫氰酸基苯酯柱前衍生化高效液相色谱法。色谱条件：色谱柱为Inertsil ODS-3V4.6mm×250mm，5μm

Methods:The green peel of Juglans Mandshurica were extracted by 95% ethanol and then separated and purified by silica gel column chromatography and gel column chromatography.

核桃楸青果皮，用95%乙醇提取，然后用硅胶柱色谱、凝胶柱色谱进行分离纯化。

MethodsHigh Performance Liquid Chromatography was performed Diamonsil C18. The chromatography conditions were as follows: methanol - 0.1mol/L monobasic potassium phosphate (50∶50) as mobile phase, flow rate being 1.0ml/min and detecting wavelength was 290nm.

方法采用高效液相色谱法，色谱柱为Diamonsiltm C18柱；流动相：甲醇-0.1 mol/L磷酸二氢钾水溶液（50∶50）；流速：1.0 ml/min；检测波长：290 nm。

The work comprises five chapters in the light of its framework and hierarchy, here all of parts are discussed respectively as following.? First, in chapter one, the concept of Chemstation is reviewed, and the applications of the software are illustrated. Then the background and the value of work are discussed in brief.? Next, there are three parts in chapter two. In first part, the main function and characteristics of chemstation are introduces in details. In the second part, the method of the object-oriented, the features of UML and Rose served as the visual development environment of UML are summarized. In the last part, some standards and criteria of chromatography data are mentioned, such as unified chromatography data style technology and GLP(Good Laboratory Practice for Nonclinical Laboratory Studies).?

从总体结构上分为五大部分，这几个部分的主要内容有：●在第一章中，简述了色谱数据处理软件和它的应用范围，然后简要的说明了选题背景和意义●在第二章中，首先以色谱工作站N2000为例，介绍了色谱工作站的主要功能和特点；然后概括了面向对象的方法和UML统一建模语言以及可视化开发环境Rose的特征；最后介绍了与色谱数据相关的标准和规范，如统一的分析数据和质量信息标准和GLP(非临床优良实验研究规范)。

The recombinant protein was purified by Ni-NTA affinity chromatography and gel filtration chromatography. The inbred C57BL/6 strains and outbred KM strains of mice were subcutaneously immunized with the protein formulated by either adjuvant ISA720 or aluminium hydroxide.

表达产物通过Ni-NTA亲和层析和凝胶过滤层析方法纯化，再分别与ISA720和Al3佐剂乳化后，免疫C57BL/6和昆明小鼠，通过尾蚴膜反应和ELISA反应检测特异性抗体。

And Pharaoh spoke to Joseph, saying, Your father and your brothers have come to you.

47：5 法老对约瑟说，你父亲和你弟兄们到你这里来了。

Additionally, the approximate flattening of surface strip using lines linking midpoints on perpendicular lines between geodesic curves and the unconditional extreme value method are discussed.

提出了用测地线方程、曲面上两点间短程线来计算膜结构曲面测地线的方法，同时，采用测地线间垂线的中点连线和用无约束极值法进行空间条状曲面近似展开的分析。