查询词典 chromatographic

Different chromatographic parameters including elution profiles, column temperature were investigated in order to optimize separation conditions of different fatty acid phenacyl ester derivatives. A gradient elution using methanol/acetonitrile (90:10, V/V)-water as mobile phase at 0.35 mL/min, detection wavelength at 246 nm, and column temperature of 35℃ were chosen.

经优化确定以(90：10)-水为流动相梯度洗脱，在检测波长246 nm，柱温35℃，流速0.35 mL/min的色谱条件下，18 min内能完成对13种脂肪酸衍生物的分离检测。

The separation of 1-(2,6-dichlorophenyl)-2 - indolone and related materials in the synthesis of medical intermediate DC I from 2,6-dichlorophenol and phenylamine was investigated with high performanc e liquid chrom atography under different chromatographic conditions.

应用高效液相色谱方法研究了以2，6-二氯苯酚和苯胺为起始原料合成药物中间体1-(2 ，6-二氯苯基)-2-吲哚酮过程中，DCI及相关物质在不同色谱条件下的分离情况。

Twenty-seven compounds were isolated from the methanol extract of the stems of Pinus massoniana by means of chromatographic methods, and their structures were elucidated as 8(14),15-Pimaradien-19-oic acid (1), Pimaric (2), Podocarpic acid (3), 12-Hydroxydehydroabietic acid (4), Dehydroabietic acid (5), 15-Hydroxydehydroabietic (6), 3β-Methoxyserrat-14-en-21-one (7), 3β-Hydroxy- serrat- 14-en-21-one (8), 3β-Methoxyserrat-14-en-21-one-30-al (9),(24R)-Stigmst- 4-ene-3-one (10),β-sitosterol (11),-3-Hydroxy-5-methoxy-stilbene(12), 4-Hydroxy-3- methoxycinnamaldehyde (13),-Ferulic acidtetracosyl ester (14), Alkylferulates (15), Pinocembin (16), Coniferaldehyde (17), Matairesinol (18),-Nortrachelogenin (19), Balanophonin (20), Cedrusin (21),-Pinoresinol (22), Tanegoside (23), 1,2-Bis-(4-hydroxy-3- methoxyphenyl)-propane-1,3-diol (24),(1S*, 2S*)-1-(4- Hydroxyphenyl) glyceri...

同时对马尾松枝条的甲醇提取物利用各种色谱技术进行了分离纯化，并利用现波谱技术鉴定了27个化合物的结构，分别为：8(14)，15-Pimaradien-19-oic acid (1)、海松酸(2)、罗汉松酸(3)、12-羟基脱氢松香酸(4)、脱氢松香酸(5)、15-羟基-脱氢松香酯(6)、3β-甲氧基-锯齿石松-14-烯-21-酮(7)、3β-Hydroxyserrat-14-en-21-one (8)、3β-Methoxyserrat-14-en-21– one-30-al (9)、(24R)-豆甾-4-烯-3-酮(10)、-3-羟基-5-甲氧基-二苯乙烯(12)、4-Hydroxy-3-methoxycinnamaldehyde (13)、-Ferulic acidtetracosyl ester (14)、Alkylferulates (15)、Pinocembin (16)、Coniferaldehyde (17)、罗汉松树脂酚(18)、 Balanophonin (20)、tanegoside (23)、1，2-Bis-(4-hydroxy- 3-methoxyphenyl)-propane- 1，3-diol (24)、(1S*，2S*)- 1-(4-hydroxyphenyl)glycerins (25)、(1R*，2R*)-1-(4-hydroxy- phenyl)gly-cerins (26)和赤松素(27)。

Cyclization: cyclization occurs at 100℃in polyphosphoric acid for 4h in the mass ratio of 3-(4-methoxyanilino) propionic acid to PPA with 1:8, and 6-methoxy-2,3-dihydro-4-quinolone is formed in 50.5% yield with a method of rapid chromatographic column, c.

成环反应：质量比[3-(4-甲氧苯氨基)丙酸∶多聚磷酸]=1∶8，反应温度为100℃，反应时间4h，柱层析纯化后6-甲氧基-2，3-二氢-4-喹啉酮的收率为50.5％；c。

In this paper,experiments for measuring absolute adsorption of N 2, CO 2 and natural gas on 8 different artificial cores using an accurate porosimeter and an precise chromatographic instrument under room temperature (283～292°K) and low pressure (0 167～0 3MPa) have been studied.From these experiments,the following result...

实验结果表明：用 N2 测得的吸附气量在原始气中所占的比例为0 。4 %～ 4 %不等，CO2 的为 1 %～ 5%不等，天然气的为 3%～ 6%不等；吸附前后自由天然气的摩尔组成有显著的差异，表明岩心对天然气有明显的吸附；天然气各组分间存在竞争吸附，重质组分的相对吸附量大于轻质组分。

Study on adsorption in porous media of reservoir is very important for phase equilibrium calculation of condensate gas and the right way of insight at the gas or condensate gas reservoir.In this paper,experiments for measuring absolute adsorption of N2, CO2 and natural gas on 8 different artificial cores using an accurate porosimeter and an precise chromatographic instrument under room temperature (283～292°K) and low pressure (0.167～0.3MPa) have been studied.From these experiments,the following results can be obtained:i.

利用高精度孔隙度测定仪和气相色谱分析仪，采用恒体积法，测定了室温(283～292K)、低压(0.167～0.3MPa)下N2、CO2和天然气在8个不同的岩心孔隙内表面的吸附量，对于天然气，还测定了吸附前后自由气体的摩尔组成，被吸附气体的摩尔组成和天然气各组分的相对吸附量。

ACD/Labs creates innovative software packages that aid chemical research scientists worldwide with spectroscopic validation of structures, chromatographic separation, medicinal chemistry, preformulation of novel drug agents, and chemical patenting and publication.

它研制出创新的套装软件，在以下方面给全世界的化学研究科学家提供帮助：结构的光谱验证，色谱层析分离，药物化学，新特药制剂的处方设计前工作，以及化学品专利和公布。

The results of intrinsic viscosity,elemental content and gel permeation chromatographic analyses showed the extent of biodegradation during the biological treatment increased with the content of pyridinium group in the polymer.

生物耗氧处理过程中该阳离子聚体片材的特性粘度、元素含量和凝胶渗透色谱分析的结果表明：聚合物中吡啶盐含量越大者，其生物降解性就越显著。

The chromatographic behaviour of anions and canons on the mixed-bed column has been investigated using pyromellitic acid as eluent.

显然，如果在相同的色谱条件下，一次进样能将阴阳离子同时分离和定量，则既可节省分析时间，又可降低分析成本。

Calcium carbide method ; chromatographic analysis ; water content ; sodium pyrosulphate

电石法；色谱分析；水分；焦亚硫酸钠

And Pharaoh spoke to Joseph, saying, Your father and your brothers have come to you.

47：5 法老对约瑟说，你父亲和你弟兄们到你这里来了。

Additionally, the approximate flattening of surface strip using lines linking midpoints on perpendicular lines between geodesic curves and the unconditional extreme value method are discussed.

提出了用测地线方程、曲面上两点间短程线来计算膜结构曲面测地线的方法，同时，采用测地线间垂线的中点连线和用无约束极值法进行空间条状曲面近似展开的分析。