查询词典 chromatographic

A novel reversed-phase ion-pair high performance liquid chromatographic method was developed for separation and determination of sodium iron ethylenediaminetetra-acetate in iron-fortified soy sauce.

建立了用反相离子对高效液相色谱法分离和测定铁强化酱油中的铁营养强化剂乙二胺四乙酸铁钠的方法。

Institute of Pharmacy, Hebei Medical University, Shijiazhuang 050017, ChinaAbstract: A rapid and simple ion-pair reversed-phase high performance liquid chromatographic method has been established for the routine analysis of zoledronic acid and its related substances.

河北医科大学药学院，河北石家庄 050017摘要：采用反相离子对高效液相色谱法研究了唑来膦酸及其有关化合物的色谱分析与分离方法。

Objective To investigate the chemical constituents from the seeds of Mirabilis jalapa. Methods Various chromatographic techniques were used to separate the chemical constituents.

目的 研究紫茉莉子的化学成分方法利用各种色谱技术进行分离和纯化，通过理化方法及NMR、IR和MS 等方法解析其化学结构。

A reversed phase high performance liquid chromatographic method for simultaneous determination of 18 amino acids is described.

测定氨基酸的方法很多[1，2 ] ，仅用于反相高效液相色谱检测氨基酸的柱前衍生试剂就有近 10种。

The optimization of chromatographic conditions for obtaining the high recoveries of both mass and bioactivity of Lys was investigated in detail.

为了提高Lys的质量及活性回收率对所用色谱条件进行了优化研究，当蛋白起始浓度为20.0mgmL^(-1)时，Lys的质量回收率和活性收率分别为97.8%和95.4%。

Two methods based on chromatographic simulated distillation for measuring closed cup flash point of aviation kerosene are introduced.

介绍了直接计算法和间接计算法两种基于色谱模拟蒸馏技术的闭口闪点测定方法。

In the gas-liquid phase reaction of catalytic oxidation of mesitylene by air to synthesize trimesic acid and the related process,an analysis method of reaction components was proposed,which includes chromatographic analysis,mass spectral analysis,IR spectrum,atomic absorption spectrophotometer and chemical titration for the purpose of analyzing reaction groups.

针对均三甲苯气液相催化空气氧化合成均苯三甲酸的反应及相关的工艺过程中，反应产物均苯三甲酸的分析问题，提出以色谱分析、质谱分析、红外光谱分析、原子吸收光谱分析及化学滴定为主要分析手段对反应组分进行分析，重点研究并建立了相关的分析方法。

METHODS: The oxidative damages of erythrocyte induced by CSE were evaluated through biochemical assays of malonaldehyde, methemoglobin and reduced glutathione levels, hemolytic rate, SDSPAGE of membrane proteins and chromatographic analysis of membrane phospholipids.

以市售香烟提取CSE，然后作用于红细胞，通过测定细胞溶血率、膜脂质过氧化水平、细胞内高铁血红蛋白以及还原谷胱甘肽含量、膜磷脂组成和膜蛋白谱变化等指标，对CSE导致的红细胞膜损害进行评估。

The chromatographic column is Nucleosil the C18 column (4.6mm×250mm,5μm); Flowing for methyl cyanide - water =1∶2; The speed of flow is 0.8ml/min; The examination wave length is 205 nm; The speed is 0.4mm/min.

色谱柱为Nucleosil C18柱(4.6mm×250mm，5μm)；流动相为乙腈-水＝1∶2；流速为0.8ml/min；检测波长为205 nm；速度为0.4mm/min。

The method on trans fatty acids analysis in food is very important. The effects of methylate sodium, potassium hydroxide, sulfuric acid and boron trifluoride in methanol and their different concentration and dosage on TFA analysis were studied. The chromatographic condition and the influence of time and temperature on the esterifation of TFA using boron trifluoride in methanol were optimized. A method for analyzing TFA were established by GC based on boron trifluoride in methanol and RT-2560(100m×0.25mm×0.2μm) capillary column.

研究了甲醇钠－甲醇、氢氧化钾－甲醇、浓硫酸－甲醇和三氟化硼－甲醇4种甲酯化试剂的浓度、用量及甲酯化时间和温度对反式脂肪酸检测的影响，优化了色谱条件，建立了以三氟化硼－甲醇法甲酯化，RT-2560(100m×0.25mm×0.2μm)毛细管柱为基础的反式脂肪酸气相色谱检测方法，C18：1-9 t， C18：1-11 t， C18：2-9 t， 12 t和C22：1-13 t 4种反式脂肪酸的最小检出浓度在0.774.08 mg/kg之间。4种反式脂肪酸不同添标浓度回收率为98.44%101.23%，重复测定的相对标准差在0.22%1.31%之间，有较好的准确度和重现性。

And Pharaoh spoke to Joseph, saying, Your father and your brothers have come to you.

47：5 法老对约瑟说，你父亲和你弟兄们到你这里来了。

Additionally, the approximate flattening of surface strip using lines linking midpoints on perpendicular lines between geodesic curves and the unconditional extreme value method are discussed.

提出了用测地线方程、曲面上两点间短程线来计算膜结构曲面测地线的方法，同时，采用测地线间垂线的中点连线和用无约束极值法进行空间条状曲面近似展开的分析。