查询词典 chloroacetic acid

This paper introduces in detail the factors influencing the yield of the amino acetic acid with the chloroacetic acid ammonolysis process, and connecting with the production procedures, makes deep analysis, and puts forward some corresponding methods for increasing the yield.

详细介绍了氯乙酸氨解法氨基乙酸生产过程中影响收率的因素，并结合生产过程进行了深入分析，有针对性地提出了提高收率的办法。

The results show, there are many methods for Chloroacetic acid production, but only the Catalytic Chlorination of acetic acid is extensively applied.

结果表明，氯乙酸的生产方法很多，但只有乙酸催化氯化法实现了广泛应用。

Chapter two 4-Hydroxybenzoic acid is connected with PEG6000 through defoliant DCC at rooom temperature, then the product is refluxed with chloroacetic acid in acetone to afford PEG-bound phenyloxyacetic acid, which is reacted with thionyl chloride, ammonium thiocyanate and arylamines in turn to give PEG-bound disubstituded thioureas. After the cleavage with sodium methoxide in methanol, the eleven disubstituted thioureas are obtained.

第二章 利用PEG6000作载体，通过脱水剂DCC在室温下将对羟基苯甲酸以酯键连接在PEG6000上，再与氯乙酸在较温和的条件下生成PEG6000支载的芳氧乙酸，然后，依次与亚硫酰氯、硫氰酸铵、芳胺反应，生成PEG6000支载的硫脲，最后用甲醇钠的甲醇溶液切割PEG，得到了十一种1，3-二取代硫脲。

Esterification of terpineol with oxalic acid, chloroacetic acid and trichloroacetic acid by solid superacid MoO3/TiO2 was studied.

研究了MoO3/TiO2固体超强酸催化剂催化松节油与草酸，氯乙酸，三氯乙酸反应的规律。

The optimum synthetic conditions of ethyl chloroacetate are: molar ratio of chloroacetic acid to ethanol is 1:8, the quantity of catalyst[Fe2(SO4)3 xH2O] is 10% of the mass of chloroacetic acid, reaction time is 1 hour, 5A zeolite was used as dehydrating agent. In these conditions, the yield of ethyl chloroacetate was up to 73%.

用Fe_2(SO_4)_3·xH_2O作为催化剂合成氯乙酸乙酯的较佳反应条件是：酸醇物质的量之比为1：8，催化剂用量为氯乙酸质量的10％，以5A分子筛作为脱水剂，回流时间1h，收率达73％以上。

Optimal process conditions for preparing 2-oxo-1, 4-piperazine diacetic acid(3-KP): 2-oxo-1-piperazine acetic acid was combined with chloroacetic acid at a mole ratio of 1 to 1.1, at temperature 40℃for 8 hours.

通过单因素分析，合成3-KP 的最佳反应条件为：反应温度为40℃，反应时间为8 小时，氯乙酸∶S-KP 的摩尔比为1.1∶1。

N,N'-ethylenediamine diacetic acid was prepared by condensation of ethylenediamine, formaldehyde and potassium cyanide. Then 2-oxo-1-piperazine acetic acid was prepared from N,N'-ethylenediamine diacetic acid. In addition, 2-oxo-1, 4-piperazine diacetic acid(3-KP) was prepared from 2-oxo-1-piperazine acetic acid with chloroacetic acid.

本文用乙二胺、甲醛和氰化钾合成了N，N′—乙二胺二乙酸，然后由N，N′—乙二胺二乙酸合成了2—氧—1—哌嗪乙酸，再由2—氧—1—哌嗪乙酸和氯乙酸合成了2—氧—1，4—哌嗪二乙酸(3-KP)。

In consideration of the competition of reactions between acetic acid, chloroacetic acid, dichloroacetic acid andchlorine, a competition factor was introduced for the improvement of fitting accuracy between calculated and experimental value of concentration.

结果表明，加入&竞争因子&的平行-连串宏观动力学模型能准确地反映己酸光氯化合成三氯乙酸的反应动力学规律。

Up to day, the batch process of producing chloroacetic acid is still extensively used in our country, by which byproduct dichloroacetic acid comes out while chloroacetic acid beingproduced.

控制反应体系中氯乙酸含量不超过30%，最终所得产品氯乙酸含量达98.5%，二氯乙酸含量小于0.5%，以目前实验装置24小时可得氯乙酸2.938kg。

The extraction of Pr3+was studied by using heptane containing bis(2-ethylhexyl)phosphinic acid in sodium perchlorate,chloroacetic acid and citric acid medium ,respectively.

研究了二(2-乙基己基)膦酸(PIA-8)的庚烷溶液分别在高氯酸钠、氯乙酸、柠檬酸介质中对Pr3+的萃取。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。