查询词典 chlorination

In chlorination, conversion of Si-H groups reaches 90% and active groups, such as ethynyl, keep unchanged.

表征结果显示，硅氢基团的转化率达到90％，炔基活性基团未发生变化。

Teflubenzuron was synthesized from 2,4-difluoronitrobenzene and 2,6-dichlobenil as starting reagent through six-step reaction with the yield of 75.3%.3,5-Dichloro-2,4-difluoroaniline was synthesized by chlorination,reduction reaction from 2,4-difluoronitrobenzene,the yield was 84.5%;2,6-difluorobenzamide with the yield of 87.7% was synthesized by fluoridation and hydrolysis from 2,6-dichlobenil.

以2，4-二氟硝基苯和2，6-二氯苯腈为起始原料，经过6步反应合成伏虫隆，总收率为75.3%。以2，4-二氟硝基苯为原料，经过氯化、还原反应合成3，5-二氯-2，4-二氟苯胺，产率为84.5%；以2，6-二氯苯腈为原料，经过氟化和水解，制得2，6-二氟苯甲酰胺，产率为87.7%；将Ⅱ与二碳酸酯酰化，合成2，6-二氟苯甲酰异氰酸酯，产率为91.3%；Ⅲ与Ⅰ加成，得到杀虫剂伏虫隆，产率为95%。

In this work, a series of antimicrobial agents containing the hydantoin structure such as AM, BM and AM-AN, were synthesized by changing the reaction conditions such as temperature, time, concentration of initiator and so on, and the N-halamine structure which possessed the ability of durable antimicrobial, was transformed through a chlorination process.

本文设计合成了一系列含乙内酰脲结构的再生抗菌剂。通过改变合成反应的条件，如反应温度、反应时间、引发剂浓度、加料方式等，制备了再生型抗菌剂前体AM、BM和AM-AN共聚物。

The production and basic characteristics of hydrogen chloride gas in the production process of chlorination paraffin wax are introduced.

介绍了氯化石蜡生产过程中副产品氯化氢气体的产生及基本特征，根据氯化氢气体的特性，用吸水法对废气进行处理，将其制成30%盐酸，所得盐酸可用于工业生产，具有良好的经济效益和环保效益。

Because the pH of the electrophilic chlorination mixture is much lower than the pK a, the major species is hypochlorous acid.

因为加氯混合电的pH比pK a要低很多，主要化学物质是次氯酸。

It was resulted that the chlorination process of simple oxide is under chemical reaction control,while that of ilmenite is dependent on the ash layer diffusion.

试验结果表明，纯氧化物的氯化过程受化学反应控制，钛铁矿氯化受灰层扩散控制。

Through calculating the critical parameter and relative data of methyl chloride high pressure thermal chlorination, the phase of this reaction has been analyzed with some conclusion being obtained.

通过对一氯甲烷高压热氯化的临界参数及相关数据的计算，对反应的相态进行了分析并得出结论。

Flushes is cool when should take down the jewelry, meets 碱 a kind of product by against jewelry, after specially contains the chlorine bleaching agent and the silver contact, can have the chlorination to respond, causes the silver personal ornament rapid nigrescence.

冲凉时应取下首饰，以防首饰遇到碱类产品，特别是含氯的漂白剂和银接触后，会起氯化反应，使银饰迅速变黑。

Goal compound synthesis namely: Take the vanillic acid as outset raw material, obtains 4- hydroxyl - 3- anisole methyl formate with the methyl alcohol reflux conditions, then after the etherification, the nitration, the return to original state, the ring closure response obtains 6- methoxy - 7- animal pen oxygen radical kui zuo lin - 4- alkone, then passes through the chlorination, the substitution aniline, to escape responses again and so on animal pen oxygen radical, etherification to obtain the goal compound; The goal compound and the diethylamine had the amine substitution reaction to obtain TM1, namely 4- benzene amino - 6- methoxy - 7- [2- hydroxyl - 3-(N, N- two ethyl aminos) third oxygen radical] kui zuo lin; Through zuo has the etherification with the Austria niter to respond obtains TM2, namely 4- benzene amino - 6- methoxy - 7- [2- hydroxyl - 3-(2- methyl - 5- nitryl imidazole) third oxygen radical] kui zuo lin.

目标化合物的合成即：以香草酸为起始原料，与甲醇回流条件下得到4-羟基-3-甲氧基苯甲酸甲酯，然后经过醚化、硝化、还原、环合反应得到6-甲氧基-7-苄氧基喹唑啉-4-酮，然后再经氯化、取代苯胺、脱苄氧基、醚化等反应得到目标化合物；目标化合物与二乙胺发生胺取代反应得到了TM1，即4-苯氨基-6-甲氧基-7-[2-羟基-3-丙氧基]喹唑啉；通过与奥硝唑发生醚化反应得到TM2，即4-苯氨基-6-甲氧基-7-[2-羟基-3-(2-甲基-5-硝基咪唑)丙氧基]喹唑啉。

Modifications of alkylation, chlorination and Vilsmeier reaction were employed for the synthesis of aromatic aldehydes bearing nitrogen mustard derivatives and halogenoalkylpiperazinyl.

通过对Vilsmeier反应、烷基化反应和氯化反应的改进提出了以简单易得的苯胺和苯基哌嗪为原料制备氮芥和哌嗪芳香醛的方法。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。