查询词典 chloric ether

It was observed that the optimum temperature for the fluorous biphasic regioselective nitrations of toluene, ethylbenzene, flurobenzene, chlorobenzene, bromobenzene, odobenzene and diphenyl ether were 80℃, 60℃, 60℃, 60℃, 80℃, 80℃ and 70℃ respectively. The catalyst had almost no activity when the reaction system contained 25% of water. Simultaneously, increasing the volume ratio of fluorous phase and organic phase in the system in which the fluorous phase can miscible with organic phase could decrease ortho-para ratio.

发现甲苯、乙苯、氟苯、氯苯、溴苯、碘苯加二苯醚的最佳氟两相选择性硝化温度分别为80℃、60℃、60℃、60℃、80℃、80℃和70℃，当加入25%的水时，催化剂已基本失去活性，在氟相和有机相能完全互溶的体系中升高氟相和有机相的体积比有利于降低邻对位比值。

The main products are: phosphorous trichloride 300,000 tons / year, phosphorus oxychloride 100,000 tons / year, phosphorus pentachloride 50,000 tons / year, 10,000 tons trichloroisocyanuric parathion / year chloromethyl ether 5000 tons / year, triethyl phosphite 10,000 tons / year, triphenyl phosphite 5000 tons / year, three phosphoric acid ethyl butoxy 2000 tons / year.

主要产品有：三氯化磷30万吨/年、三氯氧磷10万吨/年、五氯化磷5万吨/年、三氯硫磷1万吨/年、氯甲基甲醚5000吨/年、磷酸三乙酯10000吨/年、磷酸三苯酯5000吨/年、磷酸三丁氧基乙酯2000吨/年。

Methods:The target compound was synthesized using 4-hydrazino-N-methyl-benzyl-sulphonamide hydrochloride and 4,4-dimethoxy-N,N-dimethyl butylamine as the starting materials,PPA and sodium dihydrogen phosphate instead as catalysts and isopropyl ether and acetone as solvents for recrylstallization,via 4-step reactions:condensation,rearrangement,cyclization and salt formtion.

以4-肼基-N-甲基-苄基磺酰胺盐酸盐与4，4-二甲氧基-N，N-二甲基-丁胺为起始原料，改用多聚磷酸和磷酸二氢钠作为催化剂，后处理采用异丙醚和丙酮作为重结晶溶剂，经缩合、重排、环合、成盐的4步反应合成琥珀酸舒马曲坦。

The models of auricular edema in mice by dimethyl benzene and increased permeability of celiac blood capillary by acetic acid were studied,the results showed that the petroleum ether and acetic ester fraction of fermentation product of Calvatia gigantea could inhibit ear edema;acetic ester and n-Butanol fraction of fermentation product could reduce the permeability of celiac blood capillary by acetic acid.

大秃马勃Calvatia gigantea发酵液的石油醚、乙酸乙酯和正丁醇提取物进行二甲苯诱导小鼠耳廓急性炎症和醋酸所致小鼠腹腔毛细血管通透性实验，结果表明大秃马勃Calvatia gigantea发酵液石油醚提取物处理组、乙酸乙酯提取物处理组对二甲苯诱导小鼠耳肿胀具有明显的抑制作用；大秃马勃Calvatia gigantea发酵液乙酸乙酯提取物处理组、正丁醇提取物处理组对醋酸所致小鼠腹腔毛细血管通透性具有明显的抑制作用。

Methods Using petroleum ether to extract crude fat from the Capparis spinosa fruit and identify separately with GC-MS method after methanolysis.

方法］用石油醚提取刺山柑果实中的粗脂肪，甲酯化后，用GC-MS法进行分离鉴定。

Accelerated solvent extraction and Soxhlet extraction were used to extract capparis spinosa seed oil with he-xane and ethyl ether.

采用加速溶剂萃取及索氏提取法，用正己烷和乙醚为提取剂从野西瓜种子中提取油脂，经浓H2SO4催化，甲醇甲酯化处理后，以气相色谱-质谱联用技术鉴定出野西瓜种子中的脂肪酸主要组成为：油酸、亚油酸、硬脂酸等，其中不饱和脂肪酸总量占91.4%，主要成分油酸占73.3%。

The ether extracting technology of carya kernel oil was experimentally studied in this work.

对乙醚浸提法提取山核桃油的工艺条件进行了试验。

The ether extracting technology of carya kernel Oi1 was experimentally studied in this work.

对乙醚浸提法提取山核桃油的工艺条件进行了试验。

Octachlorodipropyl ether was extracted from tea samples using n-hexane-acetone(22∶3,V/V),purified with celite 545-sulfuric acid(1g-0.4mL) using hexane as an eluent.

茶叶样品用正己烷-丙酮(22∶3，V/V)提取，经硅藻土545-浓硫酸(1g+0.4mL)净化，以正己烷洗脱，GC-ECD检测，外标法定量。

Wax ester was synthesized from soybean oil and cetyl alcohol in a packed-bed reactor with petroleum ether as solvent and immobilized lipase Candida sp.99-125 as catalyst.

以大豆油、十六醇为原料，在石油醚体系中，使用实验室自制的固定化Candida sp.99-125为催化剂。

You can snipe the second and third union leaders from this position.

您可以鹬第二和第三工会领袖从这一立场出发。

Aiming at the currently shortage of XML streams quality detecting, this paper proposes a new forecasting method of XML streams quality by least squares support vector machines, which is used the method of XML keys' vector matrix as windows, and vector product wavelet transform to multilevel decompose and refactor the XML streams series, that can fulfill real-time checking demand of XML quality, and ensure constraint, consist- ency and integrality. For even more adapting net load, it proposes a control strategy by weight and adaptive adjustment to ensure XML streams quality.

针对当前XML数据流质量检测存在的不足，提出构建XML键的矢量矩阵作为窗口，利用矢量积小波变换多级分解与重构XML数据流，再结合最小二乘支持向量机对XML数据流质量进行预测的一种方法，满足XML数据流质量重构时实时检测的要求，保证XML数据的约束性、一致性与完整性；为了更好的适应网络负载，采取加权与自适应窗口调整等调度策略充分保证XML数据流的质量检测。