查询词典 chemical compound

The preparation method comprises removing benzyl of the compound IV0 in alkali condition to obtain the compound (V, reacting the compound with benzyl chloroformate to obtain the compound, wherein the compounds can be used to prepare 5-substituted-hydride indolizine natural alkaloids.

本发明所提供的制备方法是将化合物在碱性条件下去苄基得到的化合物，将化合物与氯甲酸苄酯反应，生成的化合物。和化合物可以用于制备5-取代-氢化中氮茚天然生物碱。

Notably, compounds 12–14 can be described as a 3D open–framework with nano–channels, compound 15 can be described as a 3D open–framework with double helical channels, while compound 16 can be described as a 3D heterochiral coordination polymer with double helical channels, which can be obtained by spontaneous resolution from the racemic phosphonic acid.X–ray powder diffraction analysis shows that compound 16 is a pure phase. Surface photovoltage spectroscopy of compound 16 indicates that it possesses positive SPV response in the range of 300–600 nm and shows p–type semiconductor characteristic.

值得注意的是，化合物12-14为具有一维纳米孔道结构的三维开放骨架结构，化合物15是具有双螺旋孔道的三维开放骨架结构，而化合物16是外消旋的有机膦酸配体通过自发拆分而形成的具有双螺旋孔道的多手性三维开放骨架结构。X-射线粉末衍射分析表明化合物16为纯相；化合物16的表面光电压光谱分析中，在300-600nm范围内有3个正的光(来源：ABC论文12网www.abclunwen.com)伏响应带，表明它具有p型半导体的特征；化合物16的诱导表面光电压谱进一步确定它的p型半导体的特征；磁性研究表明，化合物16中两Mn原子之间存在弱的反铁磁相互作用。

The iliac bone defect moulds were prepared and the compound scaffolds were implanted. The compound scaffolds were taken out after four and eight weeks separately, bone healing status and appearance of scaffolds were observed by eyes, the osteoplast growth status in compound scaffolds were viewed by HE and chinalizarin dyeing separately, the degradation of the compound scaffolds in vivo were observed by SEM.

制作髂骨骨缺损模型，在骨缺损处植入骨支架复合体，植入后4周、8周取材大体观察材料与周围骨愈合情况，HE染色及茜素红染色观察支架复合体内成骨细胞生长及扫描电镜观察支架体内降解情况。

Deoxybenzoin(3) was prepareded by using the resorcinol and substituted phenylacetic as starting meterials in microwave-mediated.Then the compound(3) was reacted with acetic anhydride to produce(4).The compound(4) was hydrolyzed to convert compound(5) in the acid-mediated. The compound(5) was reacted with the 1,2-dibromo-ethane and 1,3-dibromo-propane in refluxed condition with acetone as solvent to give(6) or(7),respectively.Lastly,the title compounds were synthesized by refluxing(6) or(7) with 2-methyl-benzimidazole and potassium carbonate in acetone solution.

以取代苯乙酸和间苯二酚为起始原料，用微波辐射法合成脱氧安息香(3)，(3)与乙酸酐缩合生成2-甲基-7-乙酰氧基异黄酮(4)，(4)在酸性条件下水解生成相应的异黄酮(5)，化合物(5)分别与1，2-二溴乙烷和1，3-二溴丙烷反应生成(6)和(7)，化合物(6)和(7)再分别与2-甲基苯并咪唑偶合生成目标化合物。

The invention provides a phomopsis compound of sea weed fungus with strong antibacterial activity and application in antibacterial drugs, a relative preparation method and an application, wherein the sea weed fungus is hzla01-1(Phomopsis sp.hzla01-1) as phomopsis compound A and B, compound A is colorless oily substance, and the compound B is colorless acicular crystal.

提供一类来源于海藻真菌的具有强抗菌活性，可应用于抗菌药物的拟茎点菌素化合物及其制备方法和应用。海藻真菌为拟茎点属hzla01-1(Phomopsis sp.hzla01-1)。化合物分别为拟茎点菌素化合物A和B，化合物A为无色油状物，化合物B为无色针状晶体。

The results of the ability of anti-oxidation scavenging DPPH free radical shows that polyhydroxy substituted N-benzoylserotonin derivatives (compound 1-10) have the generally better ability of anti-oxidation than control group, in which the IC50 of compound 1-10 ranges 8.75 to 18.02 μg/ml and the IC50 of trolox is 13.04 μg/ml. The abilities of anti-oxidation of compound 1, 4, 5, 7, and 10 are all better than the control group, trolox. Among all, compound 10 has the best ability of anti-oxidation (IC50 is 8.75 μg/ml). This study also discovers that the ability of scavenging DPPH free radical is strongly related to the number and the position of hydroxyl.

在清除DPPH自由基的抗氧化能力结果显示，相较於对照组水溶性维生素E之IC50值13.04 μg/ml，多羟基取代之N-色洛冬宁苯甲醯胺衍生物（化合物 1 ~ 10），皆具有相当不错的抗氧化能力，十种醯胺化合物的 IC50值介於8.75 ~ 18.02 μg/ml之间，化合物1、4、5、7、10的抗氧化能力效果皆优於对照组水溶性维生素E的IC50值，其中又以化合物10的效果最佳(IC50值8.75 μg/ml)，而清除DPPH自由基的能力发现与羟基的数量及其位置有关。

In Chapter 4, we not only give a new definition of fuzzy finite automata, of which the state transition accords with a compound fuzzy transition, but also present an important conclusion that the coarsest respecting compound fuzzy transition partition of states is same with the coarsest equivalent partition. In the discussion of coarsest partition, we give an algorithm respecting compound fuzzy transition which would be applied to get the coarsest respecting compound fuzzy transition partition.

第四章根据分明自动机的等价分类，通过重新定义模糊自动机识别过程，使得模糊自动机的识别过程与一个合成模糊变换一致，而且得到了尊重合成模糊变换的最粗分类即为状态集的最粗等价分类这一重要结论。

Nanometer compound oxides,eg. Li-Mn-O compound oxides for Li-ion battery,gas sensitive Zn-Fe-O compound oxides, Zn-Co-O compound oxides, etc.,are one of important functional materials.

纳米功能复合氧化物如锂离子电池正极材料锂锰氧复合氧化物、气敏锌铁氧、锌钴氧复合氧化物等是一类重要的功能材料。

Nanometer compound oxides,eg. Li-Mn-O compound oxides for Li-ion battery,gas sensitive Zn-Fe-O compound oxides, Zn-Co-O compound oxides, etc.,are one of important functional materials.

中文摘要：纳米功能复合氧化物如锂离子电池正极材料锂锰氧复合氧化物、气敏锌铁氧、锌钴氧复合氧化物等是一类重要的功能材料。

The mainly conclusions in our research are as flowing: tungsten trioxide powders with 100 nm primary particle are obtained by spray drying,calcination and wet milling process, and an average size of quadric particle composed of agglomerated particles is 0.64 μm; tungtsen powders with 39 nm grain size and 60 -100 nm primary particle are produced directly from previous tungsten trioxide using one step reduction in hydrogen at 700℃, and an average size of quadric particle of tungsten powder is 2.91 μm; tungsten trioxide and copper tungstate compound powders with 100 nm - 200 nm primary particle are produced using ammonia metatungsten and copper nitrate as raw materials by spray drying,calcination and wet milling process;the compound powders are transformed completely into tungsten and copper compound powders by reduction in hydrogen at 700℃,in which tungsten grain size is 59 nm and copper grain size is 51 nm; primary particle size of compound powders is 80 - 120 nm,and an average size of agglomerated quadric particle is 1.86 μm; tungsten nitride powders with 35 nm grain size are prepared from tungsten trioxide powders by nitrogen treatment thoroughly in pure ammonia at 650℃, and an average size of agglomerated quadric particle is 0.64 μm in normal temperature.

研究结果表明：采用喷雾干燥—焙烧—球磨工艺可以制备出粒度约为100nm的WO_3粉体，它们在团聚后形成的二次颗粒平均粒度为0.64μm；采用一步直接氢还原方法可在700℃下从上述WO_3粉体制备出晶粒尺寸为39nm的、一次颗粒粒度为60-100nm的W粉体，其二次颗粒的平均粒度为2.91μm；以偏钨酸铵、硝酸铜为原料，采用喷雾干燥—焙烧—球磨工艺可制备出一次粒度为100-200nm的WO_3和CuWO_4混合粉体；采用氢还原工艺可在700℃下将这种粉体完全转变为W、Cu复合粉体，其中W的平均晶粒粒尺寸为59nm，Cu的平均晶粒尺寸为51nm；复合粉体的一次颗粒尺寸为80-120nm，在常温下团聚后形成的二次平均粒度为1.86μm；采用纯氨氮化工艺可以在650℃下由WO_3粉体制得WN，其晶粒尺度为35nm，在常温下团聚后的二次平均粒度为6.4μm。

The shaping method of noncircular part and the tool holder's radial motion characters in noncircular turning process are discussed in detail in the thesis.

论文详细研究了非圆零件的成型方法和加工过程中刀架的径向运动规律。

I have not really liked him,I do not like his this kind of disposition.

我没有真的喜欢他，我不喜欢他的这种性格。