查询词典 calorimetry

The structure of resultant IPN hydrogels was successfully characterized by Fourier transform infrared spectroscopy and scanning electron microscopy; the water retention at 50℃ was measured gravimetrically; dependence of storage modulus on temperature and phase transition behavior were investigated by dynamic mechanical analysis and differential scanning calorimetry, respectively.

利用FTIR和SEM分别表征了凝胶的化学结构和内部形态；测定了凝胶在高温(50℃)时的退溶胀性能；利用DMA和DSC分别研究了凝胶的储能模量随温度的变化及热相转变行为。

The synthesized PCU was then characterized by infrared spectroscopy, differential scanning calorimetry, thermogravimetric analysis, small-angle X-ray scattering, and tensile strength measurement. The IR showed that the polymer synthesized by the above two methods both have the polycarbonate-urethane structure and the tensile measurement showed good mechanical performance of the polymer. The DSC and TGA data showed that there is an obvious soft-hard glass transition area, which indicated the existence of the micro-phase separation structure. The extent of the phase separation was affected by the ratio of starting materials, the molecular weight of PCD, and the polymerization method. The decomposition upon heating was observed in two steps. SAXS result showed that the radius (r_2), the distance between domains (d_2), and gyral radius (R_2) of hard segment micro-domain were fairly affected by the starting materials ratio and soft segment content.

IR结果表明两种方法合成的聚合产物均具有聚碳酸酯聚氨酯的结构；拉伸实验表明聚合产物具有良好的力学性能；DSC、TG结果表明，聚合物呈现出较为明显的软硬段玻璃化转变区，表明存在微相分离的结构，相分离的程度受原料配比、软段分子量、聚合方法的影响，其热分解分为明显的两个阶段； SAXS结果表明，聚合物原料配比、软段含量的变化对硬段微区回旋半径R_2，微区间距d_2，微区半径r_2影响不大其值分别为9.5(A|°、29、7.4，但对软段的微区半径及间距影响较大，随着软段含量的增大，软段微区的半径r1和间距d1都增大。

Key words: polymer material;acrylonitrile;itaconic acid;copolymerization;molecular weight;differential scanning calorimetry; thermogravimetry

关键 词：高分子材料；丙烯腈；衣康酸；共聚合；分子量；差示扫描量热法；热重

The granular morphology and size, molecular weight distribution, crystal structure, thermodynamic properties, structural character, digestibility and glycaemic-index of starch from Kabuli and Desi chickpeas cultivars were investigated using scanning electron microscope, high performance liquid chromotagraphy, X-ray diffraction, differential scanning calorimetry,infrared spectrum and other modern analytical methods.

采用扫描电镜、高效液相色谱、X射线衍射、差示扫描量热仪、红外光谱等现代分析手段探讨了Kabuli与Desi品种鹰嘴豆淀粉的颗粒形貌与大小、分子量分布、结晶结构、热焓性质、结构特征、消化性能及血糖生成指数。

The granular morphology and size, molecular weight distribution, crystal structure, thermodynamic properties, structural character, digestibility and glycaemicindex of starch from Kabuli and Desi chickpeas cultivars were investigated using scanning electron microscope, high performance liquid chromotagraphy, Xray diffraction, differential scanning calorimetry, infrared spectrum and other modern analytical methods.

采用扫描电镜、高效液相色谱、X射线衍射、差示扫描量热仪、红外光谱等现代分析手段探讨了Kabuli与Desi品种鹰嘴豆淀粉的颗粒形貌与大小、分子量分布、结晶结构、热焓性质、结构特征、消化性能及血糖生成指数。

No entire nitrendipine crystals were observed visually in SEM photos. The results of X-ray diffraction and differential scanning calorimetry analysis indicated that the crystalline form of nitrendipine was highly dispersed in microspheres, so as amorphous state. The drug release rate of microspheres could be controlled with adjusting the ratio of solid dispersion carriers and retarding agents formulated. The agitation speed and temperature of the preparation process have distinct effect on micromeritic properties of microspheres. The release profiles of the microspheres were mainly affected by the stirring rate of paddle, the concentration of SDS and pH of dissolution medium. Cooling speed and time, however, have no evident influence on the drug release rate of the microspheres. The dissolution data showed that the mechanism of drug release from microsphers was mainly diffusion-controlled. The incorporation efficiencies of 3 batches sample were exceed 96. 8％, which implied that the current method was suitable for design sustained-release dosage form for poorly water-soluble drug.

在扫描电子显微镜下观察，在微球内外未发现尼群地平的完整结晶，X-射线粉末衍射和差示扫描量热试验结果也显示，尼群地平已经被高度分散在微球中；微球的释药速度可通过调整处方中固体分散体载体和阻滞剂的比例控制；制备温度和搅拌速度对微球的质量影响较大；溶出仪的搅拌速度，释放介质的浓度和pH对微球的释放有较大的影响；制备过程中的冷却速度和冷却时间对微球的释放行为影响不很明显；方程拟合的结果表明缓释微球的释药行为符合扩散机制；测定三批微球样品的包封率均在96.8％以上，表明该法适合于制备难溶性药物的缓释微球。

The structure and properties of TKGM were characterized by FT-IR, polarizing optical microphotography, low temperature differential scanning calorimetry and TG-DSC. The results indicated: a graft copolymerization reaction was taken place between KGM and VAc, MA.

采用傅立叶红外光谱、偏光显微镜照片、低温差示扫描量热仪和综合热分析等付改性材料的结构和性能进行了分析表征。

Differential scanning calorimetry and polarizing microscope were used to study their liquid properties. Among them, nine are found to exhibit liquid crystal properties, and most of them displayed as heating monotropic liquid crystals. There are one or two mesophases and certain phase transition temperature,Δ H and temperature range of liquid crystal.

用差示扫描量热仪和偏光显微镜研究了其液晶性，发现其中九个配合物具有液晶性，多为升温单变液晶，有一至两个中介相，有确定的相转变温度、热焓和相变区间。

And we have demonstrated through differential scanning calorimetry, thermogravimetry,XPS and SEM analysis that the formation of highly reflective and conductive silver layers on polyimide film is a result of the silver-catalyzed and oxygen-assisted decomposition of the polymer overlayer and the self-accelerated aggregation of silver clusters on the film surface.

并通过差示扫描量热、热失重、XPS和SEM分析证明了聚酰亚胺表面高反射高导电银层的形成是在银催化下、氧气辅助的表层聚合物降解和表层银颗粒自加速聚集共同作用的结果。

The non-isothermal crystallization kinetics of polyoxymethyleneand poly- oxymethylene/co-polyamideat different cooling rates were investigated uisng differential scanning calorimetry.

采用差示扫描量热法研究了聚甲醛和聚甲醛/盐聚酰胺二元共混体系在不同降温速率下的非等温结晶行为，并用 Jeziorny 法、Ozawa 法和莫志深法计算了聚甲醛及其共混物的非等温结晶动力学参数。

However, as the name（read－only memory）implies, CD disks cannot be written onorchanged in any way.

然而，正如其名字所指出的那样，CD盘不能写，也不能用任何方式改变其内容。

Galvanizes steel pallet is mainly export which suits standard packing of European Union, the North America. galvanizes steel pallet is suitable to heavy rack. Pallet surface can design plate type, corrugated and the gap form, satisfies the different requirements.

镀锌钢托盘多用于出口，替代木托盘，免薰蒸，符合欧盟、北美各国对出口货物包装材料的法令要求；喷涂钢托盘适用于重载上货架之用，托盘表面根据需要制作成平板状、波纹状及间隔形式，满足不同的使用要求。