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By means of molecular designing, a series of sodium branched-alkyl benzene sulfonates weresynthesized through seven process, involving Frieded-Crafts reaction, Grignard reaction, sulfonationand neutralization. Those isomers have similar structure, carbons of same quantity, but the position ofalkylaryl dissimilarity. Liner fat acid, metaxylene and halogenated hydrocarbon of different carbonnumber were used as the starting materials. Optimum processing condition was confirmed consideringinfluence of a series of reaction factors such as feed proportioning, quantity of catalysts, quantitysolvent, reaction time, temperature and pressure. Eight kinds of isomers of sodium hexadecylxylolsulfonates were finally synthesized, and characterized by FT-IR.
本文通过分子设计,以不同碳数直链脂肪酸、间二甲苯以及不同碳数的卤代烷为原料,经酰基化、格氏反应、加氢还原、磺化及中和等反应,合成了结构相似、烷烃链碳数一定、芳基在烷烃链不同位置的烷基芳基磺酸盐同分异构体;并考察了原料配比、催化剂用量、反应时间、反应温度、溶剂用量、反应压力等一系列因素对各反应的影响,进而确定最佳工艺条件,最终合成出十六烷基二甲苯磺酸钠的八种同分异构体,利用 FT-IR 对产物结构进行了分析。
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The features and mechanism of pollutant removal by microelectrolysis as well as the characteristics of UASB start-up were also studied by means of GC-MS and analyzing granular sludge.
通过GS-MS和颗粒污泥分析,分别研究了微电解对污染物去除特性和去除机理与UASB的启动特性。
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The electricity price curve in electricity market possesses the features of multicycle and strong fluctuation, whereas there is evident error in the prediction by grey GM(1,1) model with exponential growth, for this reason the authors propose a period residual modification based grey price forecasting model, which not only inherits the advantages of grey model but also makes the forecasting curve fluctuated by means of smooth processing of original data, improvement of initial condition and period residual modification.
电力市场中的电价曲线具有多周期、跳跃等特性,而呈指数增长的灰色GM(1,1)模型预测误差较大,为此,文章提出了基于残差周期修正的灰色电价预测模型。
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We have investigated on the chemical constituents of Nepeta partite collected from Gansu Zhuanglang, and twenty eight compounds were isolated from the methanol extraction of this species by chromatography techniques. Twenty five compounds were identified by means of chemical and spectra methods IR, FABMS, EI-MS,〓, DEPT, and 2D NMR), among which four compounds were new as isopimar-15-en-3β, 8β, 20-triol; phenylethanal-3-O-(2'-glycerin)-5-O-β-D-glucopyranoside; 3-O-linolenoylglyceryl-6'-O-(α-D-galactopyranosyl)-β-D-galactopyranoside; ethyl rosemarinate.
我们对采自甘肃庄浪的康藏荆芥进行了化学成分的研究,利用层析手段从该植物的甲醇浸膏中分离出二十八个化合物,经化学方法和波谱技术(红外,质谱,一维和二维核磁共振谱)鉴定了二十五个化合物的结构,其中四个为新的化合物,它们分别是:异海松-15-烯-3β,8β,20-三醇;苯乙醇-3-O-(2'-甘油基)-5-O-β-D-吡喃葡萄糖甙;3-O-亚麻酰基甘油-6'-0--β-D-吡喃半乳糖甙;迷迭香酸乙酯。
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The permanent magnets of single-phase exchange coupling Nd 〓N〓 and Nd 〓N〓 with ThMn〓 structure have been prepared by MM and MA process and the following treatments of crystallization、nitrogenation. By means of XRD、SEM、TEM、DTA/DSC and magnetic measurements, the variations of microstructure in each corresponding stage and the related magnetic properties have been studied systematically.
本文采用机械合金化和机械研磨法及随后的晶化、氮化处理分别制备了具有ThMn〓结构的Nd〓N〓单相耦合及Nd〓N〓纳米永磁材料,借助于X射线衍射、扫描电镜、电子探针、透射电镜、差热分析以及磁测量等分析技术系统地研究了上述工艺各阶段对应的组织结构的变化以及它们与磁性能的相互关系。
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Educational legal system,which is congealed by means of the nomothetic principles and ways and is organized by five parts,is a kind of law order of managing,stipulating and developing educational facilites that are combined with eduoational democratization.
教育法制是与教育民主化的发展相联系,按照依法治理的原则、方式来管理、规范和发展教育事业所形成的教育法律秩序。教育法制是由五个环节构成的实践体系。
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By means of establishing mathematical model of noncircular gears driving mechanism and simulating mechanism motion state by using computer animated drawings technique, transmission feasibility has been examined.
通过建立非圆齿轮机构传动的数学模型,运用计算机动画技术模拟了机构的运动状况,检验了传动的可行性。
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By means of the novelly decoded manner and the well constructed fitting function, the global searching performance for the GA is developed so that optimized RBPNN approaches to the parsimonious structure;(4) A ROLS micro-genetic algorithm was built by integrating the micro-genetic algorithm with good convergence performance based on tiny class of group with the ROLS-SOA.
提出一种新的基于径向基概率神经网络的模式识别融合系统,即多分类器系统,避免了单一径向基概率神经网络分类器的分类局限性,减少了寻求单一分类单元结构最优化时的计算复杂度,通过使用D-S融合算法,大大提高了对复杂模式识别问题的分类精度。
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The osmium-catalyzed asymmetric dihydroxylation of olefins provides one of the most effective methods for the preparation of vicinal diols. Almost all kinds of olefinic substrates can be transformed to the corresponding diols by means of AD reaction. The chiral osmium catalyst is generated in situ by the chiral ligand complexing with OsO〓 in the reaction.
手性锇催化剂催化的烯烃不对称二羟基化反应是合成手性邻二醇最有效的途径之一,可以将几乎所有类型的烯烃转变成相应的手性邻二醇,因此广泛地应用于药物、天然产物以及精细化工产品的合成。
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Thirdly, by means of distinguishing its features, in accordance with thesetup rule, with the aboved feature of society, economy, environment, logistics industry andsystem and network, and so on, in order to achieve sustainable development as target, throughfour angles as society, economy, environment, logistics industry, select 8 index to establish it,moreover, use the AHP law obtain their weight, besides, by analyzing incompatible problembetween index and method, existed in traditional methods, in accordance with principle andfeature of extension synthesis assessment method, evaluate and optimate logistics centerplanning schemes and get an accurate result in the practical example.
再次,通过分析研究物流中心规划方案的特点,根据建立评价指标体系的原则和要求,结合前述的社会、经济、环境、行业、系统、网络等特征,以促进可持续发展为总目标,从社会、经济、环境、物流行业四个角度考虑,有选择性的选取了8个评价指标,建立了物流中心规划方案的评价体系,并应用层次分析法得出了各指标权重。另外,在分析比较传统方法存在指标体系与评价方法存在不相容等问题的基础上,根据可拓综合评价法的原理及特点,将其引入到物流中心规划方案评价的研究中,并通过廊坊物流中心规划方案评价进行了实证研究,取得了合理的评价结果。
- 推荐网络例句
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I am accused of being overreligious," she said in her quiet, frank manner,"but that does not prevent me thinking the children very cruel who obstinately commit such suicide.""
客人们在卡罗利娜·埃凯家里,举止就文雅一些,因为卡罗利娜的母亲治家很严厉。
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Designed by French fashion house Herm è s, this elegant uniform was manufactured in our home, Hong Kong, and was the first without a hat.
由著名品牌 Herm è s 设计,这件高贵的制服是香港本土制造,是我们第一套不配帽子的制服。
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Do not 'inflate' your achievements and/or qualifications or skills .
不要 '夸大' 你的业绩或成果,条件或者技能。