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Linear solvation energy relation was firstly introduced in the paper, and the method and step of gaining the special parameters of solvent and solute were introduced in detail, and these special parameters were used to selection and optimization of extractive agent in extractive distillation. The model of predicting activity coefficient at infinite dilution was established by linear solvation energy relation. By the above theory, several candidate solvents were selected to separate C5 fraction, and by experiment of vapor-liquid phase equilibrium at atmosphere pressure, the mixture of N-methyl-pyrrolidone including 4% water was used extractive agent of separating C5 fraction. Then binary vapor-liquid phase equilibrium of the some compound in C5 fraction and N-methyl-pyrolidone were determined at atmosphere pressure and correlated by NRTL equation. Isoprene being objective compound, experiments were operated in the laboratory-scale column; the processes were simulated by RadFrac model in ASPEN PLUS. And by the combination of experiment and simulation, the new process of separation of C5 was established.

本文首先对线性溶剂化能关系进行了分析介绍,也介绍了采用溶剂化能关系得到溶质溶剂特性参数的方法步骤,并将这些参数用于萃取精馏萃取剂的选择与优化;也通过线性溶剂化能关系式建立无限稀释活度系数预测模型,取得了一定的预测精度;将通过上述方法初选的溶剂进行了常压汽液平衡的测定研究,通过实验研究选定含水4%的N-甲基吡咯烷酮溶液做为C5分离的萃取剂,测定了大量N-甲基吡咯烷酮与C5组分的二元平衡数据,并进行关联计算;以异戊二烯为目标产物在实验室规模的精馏塔内进行了C5分离的实验研究,取得大量塔内数据;通过选用合适的热力学模型,采用ASPEN中RadFrac模块对分离过程进行模拟研究,通过实验与模拟相结合,建立了C5分离的新工艺,为将来的工业化打下了坚实的基础。

By rational designs of mechanical structure and plan, the system uses PLC as the core of control on site, and accomplishes control of the installment and debug of the system step by step by software configuring design of the touch panel. Industrial computer, the centre of monitor, control and management of the system, composes epigyny and hypogyny machines' real-time monitoring and controlling system with PLC by designing the communicative model and program, and accomplishes man-machine dialogue in form of suppositional panel by designing supervisory software. Meanwhile, we also adopt client/server model and realize long-distance supervision of impact sensitivity experiment by program designing.

系统通过合理的机械结构和方案设计,采用PLC作为现场控制核心,通过对触摸屏软件组态设计,完成了系统现场安装、调试时的单步控制功能;作为系统的监控、调度中心的工控微机通过通讯模式和程序设计,与PLC组成上、下位机实时监控系统,间接地实现了对撞击感度试验的监控,并通过上位机实时监控管理软件的设计,以虚拟面板的形式较好地实现了人机对话;采用客户机/服务器模式,通过软件编程实现了撞击感度试验的远程监控功能。

But as most of the researchers haven't, by penetrating critiques of and reflections upon the traditional intellectualist methodology in the Western,come up to their high level of consciousness of the methodology used by themselves,this essay emphasizes that,only by the radical transforming this intellectualist methodology,which is constituted by the basic inclinations embodied by the theory of preformation,thinking modes,and research patterns in the Western intellectualism,and by sublating this kind of methodology by the methodology of the Social Individual Growing-up Theory,can the researches of philosophy of action go more smoothly and get numerous significant achievements.

不过,由于绝大多数研究者都没有通过对惟理智主义研究方法论的深刻批判反思而达到方法论的自觉,所以,只有真正实现了对由基本倾向、思维方式和研究模式构成的研究方法论的彻底变革,这样的突破才是可能的;本文认为,以社会个体生成论彻底扬弃和取代基于抽象个体的预成论,是实现这种变革的富有建设性意义的学术理路。客观决定性,意志自由,预成论,第一人称哲学,社会个体生成论

The conversion boundary of self-incompatibility was researched by sowing by stage. Sunshine of day and temperature was studied critically by investigating leafage and researching traits indoors. The results showed that the daily minimum temperature was the principal factor of affinity conversion and the affinity conversion boundary was 16.5~18.1℃.HE97 was primarily regard as self-incompatible line in this research. The method was by inbreeding and sib HE97, Half the silk of HE97 and Zheng58. Inbreeding and cross have been done simultaneously. The extending condition of pollen tube was observed by dying the silk after pollinating 4 hours. The individuals with pollen tube were observed having seeds, while the individuals without pollen tube were observed having few seeds or no seeds. So this study regard HE97 as sporophytic self-incompatibility .The planting ration of female parent HE97 and male parent 87-1 was 4:1.The nature cross-pollination was studied by the theory of endosperm xenity, the study show that the setting percentage of HE97 was 625%, in which the seed in self was 70% and the seed in hybrid was 30%. This was consistent with the study of silk anatomy structure, then come to the same conclusion: compatible pollen germination and fertilization can stimulate the self-incompatible pollen germination and fertilization in the same corn cob.

通过分期播种,进行了光温敏自交不亲和材料HE97亲和性转换区间的研究,依据田间跟踪调查叶龄及室内考种研究了HE97亲和性转换区间的光温临界值,结果表明:1日最低温度是影响HE97自交不亲和性的主要原因,亲和性转换区间在16.5℃~18.1℃之间。2通过HE97自交和姊妹交以及将HE97与郑58作为双亲,各自的花丝一分为二,分别正反交,授粉后4个小时分别取其花丝进行固定、染色,观察花粉管的伸长情况,根据结实率与花粉管伸长的对应关系,结果发现观察到花粉管的对应植株收获到了种子,而没有观察到花粉管的对应植株结实率极低或没有结实,本研究把HE97初步划为孢子体自交不亲和类型。3以HE97为母本,87-1为父本,按4母:1父行比,通过花粉直感效应研究天然异交率,结果母本HE97结实良好(62%),其中自交粒占70%,异交粒占30%,结合花丝切片观察表明,亲和花粉的萌发及受精会导致落在同一果穗柱头上不亲和花粉的萌发不再受抑制。

"That the doctrine of the Reformed churches concerning predestination, and the points annexed to it, by its own genius and necessary tendency, leads off the minds of men from all piety and religion; that it is an opiate administered by the flesh and by the devil, and the stronghold of Satan, where he lies in wait for all; and from which he wounds multitudes, and mortally strikes through many with the darts both of despair and security; that it makes God the author of sin, unjust, tyrannical, hypocritical; that it is nothing more than interpolated Stoicism, Manicheism, Libertinism, Turcism; that it renders men carnally secure, since they are persuaded by it that nothing can hinder the salvation of the elect, let them live as they please; and therefore, that they may safely perpetrate every species of the most atrocious crimes; and that, if the reprobate should even perform truly all the works of the saints, their obedience would not in the least contribute to their salvation; that the same doctrine teaches, that God, by a mere arbitrary act of his will, without the least respect or view to sin, has predestinated the greatest part of the world to eternal damnation; and, has created them for this very purpose; that in the same manner in which the election is the fountain and cause of faith and good works, reprobation is the cause of unbelief and impiety; that many children of the faithful are torn, guiltless, from their mothers' breasts, and tyrannically plunged into hell; so that, neither baptism, nor the prayers of the Church at their baptism, can at all profit by them;" and many other things of the same kind, which the Reformed Churches not only do not acknowledge, but even detest with their whole soul.

"该学说的革新教会联谊会关于宿命,并分附在它,由它自己的天才和必要的倾向,导致起飞的头脑男子从所有虔诚与宗教;这是一个鸦片类由血肉所魔鬼和据点撒旦,在那里他是在等待所有;从他的伤口众多,而致命打击,通过许多与飞镖都绝望与安全;因为它使上帝的作者单,不公正,专横,虚伪的,即它只不过是多插生活俭朴,摩尼教,放纵, turcism ;这使得男性的肉体关系稳固,因为它们是说服它说,没有任何东西可以阻碍救赎的选举,让他们住,因为他们请;因此,他们可以安全地胡作非为,每一个物种的最残暴的罪行,并认为,如果reprobate甚至应该真正履行全部工程的圣人,他们的服从,将不会在至少贡献出他们的救恩,即同一教义教导说,上帝,由一个单纯的任意行为,他的意志,如果没有起码的尊重,或以单,有predestinated最大的是世界的一部分,以永恒damnation ,并且创造了,他们为了这个目的,即在同一何种方式选举是喷泉和事业的信念和良好的工程, reprobation ,是导致不信者和不虔诚;说,许多儿童的教友们被拆除,无罪,从他们的母亲的乳房,并tyrannically陷入地狱,因此,既不洗礼,也没有祷告的教会,在他们的洗礼,能在所有利润由他们来主宰;"和许多其他东西的同类,而改革教会不仅不承认,但即使是讨厌自己的整个灵魂。

The UV and IR spectroscopic studies of the monomer films showed that the photoreaction ratio of monomer (about 50%) was higher than the corresponding photosensitive polymer (about 10%, PVCi). The polarized IR spectra proved that obvious anisotropic absorption was displayed in the irradiated photosensitive film. With polarizing microscopy method, we found that these kinds of photoalignment films exhibited good alignment ability, and the stability of the photoalignment film could reach about 100℃. 2 A photosensitive self-assembled monolayer was fabricated that contained photo-cycloadditable groups, such as, coumarin and cinnamate. The reaction process were detected by contact angle method because the IR absorption of monolayer was very weak. The photosensitive self-assembled monolayer promote uniform alignment of nematic liquid crystals by LPUV, and it thermal stability could reach about 130℃. 3 A cationic bolaform amphiphiles was synthesized that had two photosensitive double bonds, and can be polymerized by ultraviolet. A layer-by-layer self-assembled deposition film was prepared in aqueous solution by using this material and poly (sodium 4-styrenesulfonate). The UV-Vis. spectra proved that the multilayers film was uniform and layer-by-layer. When LPUV irradiated the film, the photopolymerizable double bond underwent [2+2] cycloaddition, and the production of the reaction distributed along the polarized direction of incident LPUV. Polarized UV-Vis. spectra indicated that the irradiated self-assembled multiplayer film was anisotropic, and the dichromic ration is about 0.09, it is higher than the spin-coating method of photosensitive polymer or monomer. We used this anisotropic film as alignment layer of nematic liquid crystals, and obtained a uniform and stability alignment result, the static contrast ratio is about 100, which is very close to application of liquid crystal device. This thesis is an instance that the photochemical material was used in the physics region of liquid crystals, the route that was from photosensitive monomer, self-assembled monolayer film to self-assembled multiplayer film was undergone, by this logical research method photoailgnment of liquid crystal was extended and consummated.

围绕上述思路开展了如下工作:1合成了三种可进行光二聚反应的光敏小分子单体,LPUV 辐照制作了光控取向膜;用紫外-可见光谱法和红外光谱法分析了薄膜中的光化学反应,发现小分子的光反应程度可达到50%以上,至少比光敏高分子高出5倍;薄膜的偏振红外光谱证实,经过LPUV 辐照后薄膜出现了明显的各向异性;将小分子光控取向膜制成液晶器件,在偏光显微镜下观察看到均匀一致的液晶取向;并且热稳定性达到100℃左右,接近实用化要求。2制备了含肉桂酸、香豆素基团的自组装单层膜;采用接触角的方法监测自组装反应的动力学过程;紫外-可见光谱证实了自组装单层膜在石英基板表面形成;自组装单层膜经LPUV 辐照后能诱导液晶均匀取向,而且热稳定性可达130℃,热稳定性进一步提高。3合成了含有光敏双键的双季铵盐,在水溶液状态下将它和聚乙烯基苯磺酸钠沉积生成layer-by-layer 自组装多层膜,紫外-可见光谱证实这是一个逐层均匀的沉积;在LPUV 照射下,自组装膜中的光敏双键按照偏振方向发生[2+2]环加成反应,形成取向膜,用二向色性值评价的分子取向度高于高分子及小分子光控取向膜的水平;实验证明用自组装多层膜制成的液晶器件亮暗态均匀,静态对比度约为100,达到实用化器件的水平。

All those whom God has predestinated to life, and those only, he is pleased, in his appointed and accepted time, effectually to call, Ro 8:30 11:7 Eph 1:10,11 by his word and Spirit, 2Th 2:13,14 2Co 3:3,6 out of that state of sin and death in which they are by nature, to grace and salvation by Jesus Christ; Ro 8:2 Eph 2:1-5 2Ti 1:9,10 enlightening their minds spiritually and savingly to understand the things of God; Ac 26:18 1Co 2:10,12 Eph 1:17,18 taking away their heart of stone, and giving to them an heart of flesh; Eze 36:26 renewing their wills, and by his almighty power determining them to that which is good; Eze 11:19 Php 2:13 De 30:6 Eze 36:27 and effectually drawing them to Jesus Christ; Eph 1:19 Joh 6:44,45 yet so as they come most freely, being made willing by his grace. So 1:4 Ps 110:3 Joh 6:37 Ro 6:16-18 2 This effectual call is of God's free and special grace alone, not from any thing at all foreseen in man; 2Ti 1:9 Tit 3:4,5 Eph 2:4,5,8,9 Ro 9:11 who is altogether passive in it, until, being made alive and renewed by the Holy Spirit, 1Co 2:14 Ro 8:7 Eph 2:5 he is enabled by it to answer this call, and to embrace the grace offered and conveyed in it.

2Jo 1:9-11 1Co 16:22 Ga 1:6-8 1 )所有的人对上帝有predestinated人生观,以及那些只,他很高兴,在他的任命,并接受了时间,有效地打电话,滚装8:30 11时07分弗1:10,11由他的文字和精神, 2th 2:13,14 2co 3:3,6出该国的罪恶和死亡的来信,他们都是本质上说,以恩典和救赎,由耶稣基督;滚装8:2弗2:1-5 2ti 1:9,10启发他们的头脑,在精神上和savingly了解事情的上帝;交流电26:18 1co 2:10,12弗1:17,18拿走他们铁石心肠,并给他们一个心脏的果肉;新教徒协会36:26自强不息他们的遗嘱,以自己的全能的能力决定他们说,这是个好;新教徒协会11时19分的PHP 2时13德30:6新教徒协会36:27 ,并有效地借鉴他们耶稣基督;弗1:19 joh 6:44,45然而,让他们来最自由,正在取得愿意由他的恩典,所以1:4的PS 110:3 joh 6时37滚装6:16-18 2 )本显效呼吁是上帝的自由和特别恩典单,而不是由任何事情在所有能预见在男子; 2ti 1时09山雀3:4,5厄2:4,5,8,9滚装9时11分,他们是完全处于被动,直到,正活着,并再次由圣灵1co 2时14滚装8时07弗2时05分,他是启用的,它要回答这个号召,并接受恩典提供,并转达了此事。

VII. And whereas also by authority of parliament, in the five-and-twentieth year of the reign of King Edward III, it is declared and enacted, that no man shall be forejudged of life or limb against the form of the Great Charter and the law of the land; and by the said Great Charter and other the laws and statutes of this your realm, no man ought to be adjudged to death but by the laws established in this your realm, either by the customs of the same realm, or by acts of parliament;and whereas no offender of what kind soever is exempted from the proceedings to be used, and punishments to be inflicted by the laws and statutes of this your realm; nevertheless of late time divers commissions under your Majesty's great seal have issued forth, by which certain persons have been assigned and appointed commissioners with power and authority to proceed within the land, according to the justice of martial law, against such soldiers or mariners, or other dissolute persons joining with them, as should commit any murder, robbery, felony, mutiny, or other outrage or misdemeanor whatsoever, and by such summary course and order as is agreeable to martial law, and is used in armies in time of war, to proceed to the trial and condemnation of such offenders, and them to cause to be executed and put to death according to the law martial.

鉴于在爱德华国王三世统治的第二十五年,通过国会的权力宣称和颁布:不得违背大宪章和世上法律的形式,未经审判而处置任何人的生命和肢体;又据大宪章和其它王国内的法律和条令,除依本王国已确定之法律或习俗或国会法案,任何人不得被判处死刑;无论何种罪人,都不得被剥夺接受诉讼程序的权利,也不得免除王国内的法律和条令施加的惩罚;然而近来,若干国王委托函签发,据此指定某些人担当代理人在王国内行使权力,根据军事法律的审判,对这样的海陆军士兵或其他加入他们的放肆人等,连同谋杀,抢劫,重罪,叛变,或其它暴行或轻罪,一律通过如在战争时期军队中使用的军事法律一样的简略的程序和规则,来审理和判决这些罪人,并依据军事法律处以死刑。

Humbly show unto our Sovereign Lord the King, the Lords Spiritual and Temporal, and Commons in Parliament assembles, that whereas it is declared and enacted by a statute made in the time of the reign of King Edward I, commonly called Stratutum de Tellagio non Concedendo, that no tallage or aid shall be laid or levied by the king or his heirs in this realm, without the good will and assent of the archbishops, bishops, earls, barons, knights, burgesses, and other the freemen of the commonalty of this realm; and by authority of parliament holden in the five-and-twentieth year of the reign of King Edward III, it is declared and enacted, that from thenceforth no person should be compelled to make any loans to the king against his will, because such loans were against reason and the franchise of the land; and by other laws of this realm it is provided, that none should be charged by any charge or imposition called a benevolence, nor by such like charge; by which statute:(efore mentioned, and other the good laws and statutes of this realm, your :(cts have inherited this freedom, that they should not be compelled to contribute to any tax, tallage, aid, or other like charge not set by common consent, in parliament.

,谦卑的呈给本次国会集会的我们世间的王,贵族院,以及众院,鉴于爱德华一世(1239 – 1307)国王统治期间制定的一部条令——通常称为&Stratutum de Tellagio non Concedendo&——所宣称和颁布的:若没有善意和王国内大主教,主教,厄尔,巴仁,骑士,自由民,以及平民中其他的自由民的同意,我们王国内的国王或者国王的继承人不得摊派或征收租税和援助;又爱德华三世(1312 – 1377)统治的第二十五年通过国会所拥有的权力所宣称和颁布的:自此,不得强迫任何人违背他的意愿借贷与国王,因为这样的借贷违背了理性和世上的权利;以及依据我们王国内提供的其它法律,不得以一种被称作捐税的索取征收任何东西,亦不得通过诸如此类的索取;依据以上提到的法律,以及其它王国内的善法和条令,你的臣民已经继承了这种自由,即他们不应当被强迫提供任何税款,租税,援助,或者其它没有国会共同同意的类似索取。

Every one of us should be exercising what is still our democratic right to exert the maximum pressure on our MPs - by (to paraphrase the words of Henry Porter) bombarding them with letters and e-mails, by confronting them repeatedly at their surgeries, by contributing to blogs and phone-ins, by talking to friends and colleagues, by expressing in no uncertain terms our dismay at, and disapproval of, what is being done by Labour's centralisers and controllers who manipulate our elected parliament, and by their data men who would invade every aspect of our lives.

我们每个人都应该行使什麼仍然是我们的民主权利,尽最大的压力,对我们的国会议员-由轰击他们的信件和电子邮件,由对抗他们多次在他们的手术,由作出贡献的博客和手机程式,交谈的朋友和同事,表示毫不含糊地,我们感到失望,并表示反对,正在做些什麼劳工的centralisers和控制器谁操纵我们的选举产生的议会,以及他们的个人资料男子谁,将入侵的各个方面,我们的生活。

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With Death guitarist Schuldiner adopting vocal duties, the band made a major impact on the scene.

随着死亡的吉他手Schuldiner接受主唱的职务,乐队在现实中树立了重要的影响。

But he could still end up breakfasting on Swiss-government issue muesli because all six are accused of nicking around 45 million pounds they should have paid to FIFA.

不过他最后仍有可能沦为瑞士政府&议事餐桌&上的一道早餐,因为这所有六个人都被指控把本应支付给国际足联的大约4500万英镑骗了个精光。

Closes the eye, the deep breathing, all no longer are the dreams as if......

关闭眼睛,深呼吸,一切不再是梦想,犹如。。。。。。