查询词典 brominating

This paper studied two new processes for catalytic synthesis of decabromodiphenyl ether which were carried out distinguishingly by brominating diphenyl oxide with bromine and bromine chloride in the presence of a novel metal catalyst.

本文研究了采用新型金属型催化剂催化合成十溴二苯醚的溴素法和氯化溴法两种新工艺；利用均匀实验设计和单纯形优化试验技术对两种新工艺的工艺条件进行了优化研究，分别确定了两种工艺路线的最佳工艺条件；通过筛选，确定了一种十溴二苯醚的精制新工艺。

A process for preparingp-fluo-2-(2-methyl-3-propionyl)-4-oxy-N,3-diphenyl-phenylbutylamide includes such steps as Friedle-Craft acylating of newly prepared phenylacetyl chloride and fluorobenzene under catalysis of AlCl3 to obtain 4-fluoro-phenylbenzyl ketone, brominating at carbonyl alpha position under catalysis of less AlCl3 to obtain alpha-bromo-4-fluo-phenylbenzyl ketone, and condensing with isobutyryl acetanilide under action of sodium ethoxide.

本发明涉及一种制备对氟－2－(2－甲基－3－氧丙基)－4－氧－N，3－二苯基－苯丁酰胺(1)的方法，其包括以下步骤：新制的苯乙酰氯与氟苯在AlCl3催化下进行Friedle－Craft酰化反应，得到对4－氟－苯基苄基酮(4)；化合物(4)在少量AlCl3催化下进行羰基α位溴化，得到α－溴－4－氟－苯基苄基酮(5)；然后(3)异丁酰乙酰苯胺在乙醇钠作用下与化合物(5)进行缩合。

Initial experiment showed that the aromatic compounds were brominated to corresponding bromides with hydrobromic acid or bromine as brominating agent in the presence of sodium nitrite under the mild conditions.

研究发现在NaNO_2存在时，氧气能够以HBr(或Br_2)为溴化试剂，在温和条件下将芳香化合物氧化溴化生成相应的溴代芳香化合物。

A new process for the preparation of 5-bromo-vanillin with vanillic aldehyde as raw material,AlBr3 as activator,HBr and H2O2 as brominating agent and anhydrous alcohol as solvent was developed in this paper.

摘 要：以甲基香兰素为原料，氢溴酸与过氧化氢为溴化剂，溴化铝为催化剂，无水乙醇为溶剂制备5-溴香兰素。

One subject of the present work relates to a green chemistry synthesis of tetrabromobisphenol A wherein the combination of sodium bromide and sodium bromated as brominating agent which completely replaces conventional liquid bromine.

据文献报道，该产品在某些阻燃材料中将是十溴二苯醚的理想替代品之一，目前，仅有国外公司在销售该种产品，我国还没有实现真正的工业化生产，所以研制开发溴化环氧树脂阻燃剂具有重要意义，本文研究工作主要包括三方面的内容。

In the process of bromotion of ester, it adopted high selective brominating agent , the yield exceeded 90% and the purity was above 95%.

在芳醚的溴化反应中，首次采用了高选择性的溴化剂，使溴化一步的收率超过90％，含量均在95％以上，具有很好的经济效益和应用前景。

Solid content≥30%,cationic, residual monomer≤9%（Brominating methods

固含量≥30%，阳离子性，残单≤9%溴化法

To the product yield is mainly studied in the brominating process, and the best synthesizing process conditions is obtained; the effect of the selection, quantity of the solvent, the reaction temperature, reaction time, and the catalyzer to the product yield is researched in the process of ketalization and the relative preferable process conditions has been got.

在脱溴反应中，主要研究了溶剂的用量、溶剂配比、物料配比、反应时间和反应温度等对目标产物得率的影响；在选择性溴化反应中，主要研究了溶剂和溴化剂的选择、物料配比、溶剂的用量等参数对产物质量和得率的影响，最终得到了合成的最佳工艺条件；在缩酮化反应中，主要研究了溶剂的选择、溶剂的用量、反应温度、反应时间和催化剂的选择等参数对产物得率的影响，并得到合成的较佳工艺条件。

In the reaction, industrial chlorinating agent and brominating agent with low cost and easy acquisition are used as oxidants to oxidize the ethyl lactate into the ethyl pyruvate.

反应中使用了廉价易得的工业用氯化剂、溴化剂作为氧化剂，将乳酸乙酯氧化为丙酮酸乙酯。

A new oscillographic potentiometric kinetic method for determining super trace aromatic amine was developed, based on the brominating reaction of aromatic amine and bromine.

将动力学分析法与示波电位法相结合，利用KBrO3与KBr的反歧化反应和溴代反应体系，提出了测定痕量芳胺的新方法。

For a big chunk of credit-card losses; the number of filings (and thus charge-off rates) would be rising again, whether

年美国个人破产法的一个改动使得破产登记急速下降，而后引起了信用卡大规模的亏损。

Eph. 4:23 And that you be renewed in the spirit of your mind

弗四23 而在你们心思的灵里得以更新