查询词典 benzene

By using lead ion as the template molecule, sodium vinylbenzoic- acid as the functional monomer and divinyl benzene as the cross-linking monomer, lead molecularly imprinted polymers were synthesized by preassembling and surface-imprinting technology.

以对乙烯基苯甲酸钠为功能单体，铅离子为模板分子，对乙烯基苯为交联剂，采用预组装方法结合表面印迹技术合成得到铅的分子印迹聚合物。

In the first step, star-shaped polystyrene,_n, was synthesized by the arm-first method via ATRP using a preformed PS macroinitiator obtained by ATRP of styrene, in the presence of divinyl benzene.

合成过程具体是：首先，先由ATRP合成线形聚苯乙烯，并以此作大分子引发剂，二乙烯基苯作偶联剂，采用先臂后核的方法，制备星形聚苯乙烯_n。

The results showed that when 0.3 g of divinyl benzene was used as crosslinking agent, the crosslinking degree increased significantly from 28.26% to 90.95% with the increase of MAA amount from 4.0 mol% to 10.0 mol%, and this increase became slowly as MAA amount was more than 10.0 mol%; the particle volume expansion was increased gradually as MAA amount increased, and reached a maximum of 42.1% when 12.0 mol% of MAA was used, and perfect porous morphology inside particles was observed even when the crosslinking degree reached 95.4% at 14.0 mol% of MAA.

结果表明：在交联剂二乙烯基苯用量一定(0.3 g)的条件下，随着MAA用量从4.0 mol%增加到 10.0 mol%，聚合物交联程度从28.26%迅速增大至90.95%，当其用量超过10.0 mol%后 P x增大趋势变缓；随着MAA用量的增加，处理后胶粒体积膨胀百分率逐渐增大，在MAA用量为12.0 mol%时Δ V 达到42.1%的最大值，当MAA用量增大到14.0 mol%时，尽管 P x高达95.44%，胶粒仍具有完好的孔状结构。

The amphiphilic block copolymers are synthesized using TEMPO controlled polymerization method with tertrabutylammonium styrenesulfonate and divinyl benzene as monomers for each block.

此双亲性共聚高分子乃利用TEMPO之方式进行活性聚合，将磺酸钠盐聚苯乙烯单体转换成疏水性单体，第二链段选择DVB作为具备交联之单体。

Bis vinyl phenyl terminated polydimethylsiloxane was synthesized by the hydrosilylation of bis dimethylhydrogen siloxyl terminated PDMS with m divinyl benzene. The structure of the VTPDMS was characterized by 1H NMR.

通过双二甲基氢硅氧封端的聚二甲基硅氧烷与间二乙烯基苯的硅氢加成反应制备了双乙烯基苯封端的聚二甲基硅氧烷，用1H NMR对其结构进行了表征。

The results show that the introducing of multivinyl monomer and CaCO3 can slow down polymerization rate to different extent.Using 1％～5％ trimethylolpropane trimetbacrylateor divinyl benzene,tight encapsulation of CaCO3 can be realized and beyond 94％PS cannot be extracted. The amount of crosslinker or emulsifier should be accommodated when the load amount of CaCO3 is increased.CaCO3 content in the product increases consequently with the increase of the loaded amount of CaCO3,which can be known from FT-IR and TGA.TEM observations reveal that when the load amount of CaCO3 is 14.8％,most CaCO3 particles are encapsulated and each latex particle contains one CaCO3 particle.Composite particles have well-defined core—shell structure and the thickness of polymer shells is around 10 nm.However,the thickness of polymer shell decreases and many free CaCO3 particles appear when the load amount of CaCO3 reaches 29.3％and 58.7％,respectively.

结果表明，多乙烯基单体以及碳酸钙的引入会使聚合反应速率有不同程度的降低；使用1%～5%的TMPTMA或DVB，可实现PS对碳酸钙颗粒的牢固包覆，不可抽提的PS达94%以上；当碳酸钙用量改变时，需要适当调整乳化剂和多乙烯基单体的用量；IR和TGA的结果表明，随着碳酸钙用量增加，产物中的碳酸钙含量也相应增加；TEM照片和计算结果显示，当碳酸钙用量为14.8%时，绝大部分碳酸钙颗粒被包覆，且基本上每个乳胶粒中包覆一个碳酸钙颗粒，复合粒子具有清晰的核壳结构，壳层厚度约为10 nm，而当碳酸钙用量增加到29.3%和58.7%时，壳层厚度减小，并且出现较多裸露的碳酸钙颗粒。

To establish a MPLC method for the content determination of resveratrol in Polygonum cuspidatum Sieb. Et. Zucc, Analytical column SOURCE 5RPC ST 4.6/150 was used with a mixture of acetonitrile+water (30+70,volume ratio ) as mobile phase ,with a flow rate of 1ml/min and the UV detection wavelength was 306nm, The linear range was 0.6-1.6mg/ml (r=0.9919). The average recovery of prodatin was 103.0%-90.4%(RSD=7.21%). The method is convenient and accurate. Result indicated a reverse phase chromatography media based o n polystyrene/divinyl benzene has excellent resolution for resveratrol in cuspidatum. P rovide theoretical support for process development.

色谱条件采用SOURCE 5RPC ST 4.6/150预装柱，以乙腈/水(体积比30/70)溶液为流动相，流速1ml/min、检测波长为308nm，结果表明，白藜芦醇在0.6～1.6mg/ml的浓度范围内峰面积积分值与浓度的相关系数r=0.9919；所测定的虎杖饮片中白藜芦醇平均含量为0.304％，平均回收率为103.0％～90.4％；实验表明，以聚苯乙烯为基架的反相介质对于虎杖中自藜芦醇具有良好的分辨率，适合其有效成分的检测、分离，对虎杖中白藜芦醇制备的科学研究过渡到工艺开拓有很好的借鉴。

Firstly, partial sulfonated polystyrene were prepared by solution polymerization with the raw materials of styrene, sodium styrene sulfonate and divinyl benzene; Secondly, the SPS/OMMT nanocomposites were prepared by intercalation polymerization with the monmers and organically modified montmorillonite.

首先，利用NMP为溶剂，BPO引发苯乙烯、苯乙烯磺酸钠、二乙烯基苯溶液共聚；同时，采用高分子的单体与有机蒙脱土插层聚合制备了磺化聚苯乙烯阳离子树脂／蒙脱土复合材料。

The title nano-sized polymeric microgels were synthesized by emulsion polymerization method,using divinyl benzene as crosslinking agent and methyl methacrylate,hydroxyl ethyl methacrylate,butyl acrylate as monomers.

通过乳液聚合的方法，以二乙烯基苯为交联剂，用甲基丙烯酸甲酯、甲基丙烯酸-β-羟乙酯、丙烯酸丁酯等丙烯酸酯类单体合成纳米尺寸的聚合物微凝胶粒子。

Results showed that the monomer conversion increased slightly in the presence of the crosslinking agents The size of particles decreased slowh as the amount of cmsslinking agent increased.and the size distribution of the particles broadened at a higher amount of cmsslinking agent Divinyl benzene was more effective than ethyl glycol dimethyl methacrylate to make polymer crosslinked.During alkali treatment process,void latex particles can be obtained when no DVB or less than 0.5 wt％ of EGDMA was used,while muhihollow structure was generated when DVB or more than 1.0 wt％ of EGDMA was introduced.The volume expansion of the particles decreased with increasing the amount of emsslinkirlg agents.

结果表明，体系中加入交联剂后，单体转化率都有不同程度的提高；随交联剂用量的增加，乳胶粒粒径略有减小，交联剂用量较高时，乳胶粒粒径分布加宽；二乙烯基苯的交联效率稍高于双甲基丙烯酸乙二醇酯；不加入交联剂及EGDMA用量低于0.5%时，处理后乳胶粒呈空腔结构，加入DVB及EGDMA用量高于1.0%时，处理后乳胶粒呈多孔结构，并且乳胶粒体积增量随交联剂用量的增加而减小。

By the time of its fall, most of the prisoners were writers who had written against the corruptions of the government.

到它被攻陷的时候，里面多数的犯人是写了反对政府贪污文章的作家。

The most obvious variation to ovum morphological character was that the color was changed from light green to sepiaceous in embryonic development, and all the ovums were almost hatched after 96h.

在胚胎发育过程中卵的形态特征最明显的变化是颜色从淡绿到深褐色，卵在发育96h后卵基本全部孵化。