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The main object of this research is to investigate synthesis of Cu23Cl Cu and CuO nanoparticles through electrospinning and heat-treated method The research is mainly focused on preparative parameter and the change of heat-treated temperature to form the nanoparticles inlaid in silicon fibers the shape and color change are dicussed First of all to prepare the Polyvinyl butyral and silica dioxide complex nanofiber by electrospinning and then to investigate different heat-treated temperature and reactive time to being an influence on the products The results detected by SEM XRD TEM EDS FTIR combined sol-gel process and electrospinning can prepare Polyvinyl butyral and silica complex nanofiber The experimental result is found when heat-treated temperature is 100~4750C it can produce Cu23Cl nanoparticles; Above 4750C~ 4900C it can produce Cu nanoparticles; Above 450~7000C it can produce CuO nanoparticles And the viscosity is lain between 20~40cp and the sol-gel process time is 3hr it can produce the thinner fibers The average diameter of the fibers are 107 88±21 01nm;Due to the nanoparticles inlaid in the silica fibers the thinner fibers can be inlaid the smaller nanoparticles so this is the result that the experiment is expected To calcine the complex fibers is to produce surface silica fibers contain Cu23Cl Cu and CuO nanoparticles due to surface plasma resonance it make the color of the fibers become yellowish green from light white green turn into the red nuclear finally As the experimental result to utilize sol-gel process combine electrospinning can produce porous silica fibers contain Cu23Cl Cu and CuO nanoparticles
本研究旨在探讨「利用放电纺丝和热处理法来合成Cu23Cl、Cu和CuO奈米粒」之研究,实验著重在制备参数与热处理温度变化对所形成的奈米粒镶嵌在二氧化矽纤维中的形态与颜色变化探讨。首先,利用放电纺丝法制备出聚乙烯醇缩丁醛及二氧化矽之奈米纤维,比较不同的热处理温度与反应时间的改变对产物生成产生影响,进而研究不同热处理温度和时间对生成奈米粒的影响。产物经由SEM、XRD、TEM、EDS和FTIR等仪器分析结果显示,结合溶胶-凝胶法(sol-gel process)和放电纺丝法可产生聚乙烯醇缩丁醛及二氧化矽复合奈米纤维。实验结果发现,若热处理温度在100~4750C下可得到Cu23Cl奈米粒,475~4900C 可得Cu奈米粒,450~7000C以上可得 CuO奈米粒。而黏度介於20~40cp间和溶胶-凝胶时间为3hr时,可产生直径比较细的纤维,纤维直径为107 88±21 01nm;且由於奈米金属颗粒镶嵌在二氧化矽纤维中,直径比较细的纤维,可以得到比较小的奈米金属颗粒,这与实验预期相符。而锻烧此复合物产生多孔的二氧化矽纤维并包含Cu23Cl、Cu和CuO奈米微粒时,由於表面电浆子共震关系,而使纤维颜色由淡白黄绿色变成黄绿色,再变红褐色。由实验结果得知,利用溶胶-凝胶法(sol-gel process)结合放电纺丝法和不同热处理温度,可产生Cu23Cl、Cu和CuO奈米粒镶嵌在二氧化矽纤维。
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4 Of our country s Company Law makes provision of limited company s stock right transfer become the arbitrary clause,but this does not mean there is no border in the corporation by-law autonomy of stock right transfer .
我国《公司法》第七十二条第四款使有限责任公司股权转让规范成为任意性条款,但这不意味着股权转让的公司章程自治没有边界。
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Canton has been gifted with the leaders of the world's leading companies as Microsoft, Cisco, Hewlett-Packard, CA, trends, Oracle set up a close working relationship, at the same time actively with China Mobile-based mobile value-added business in-depth cooperation, currently the company's self-Product "excellent its mobile commerce platform,"and" profit off fat - the development of customer management system "has become mobile and Hainan, Guangdong Mobile's core information products and gradually move with the provinces to carry out the depth of cooperation, Guangzhou No. gifted the parties head into the hands of Chinese enterprises information Construction of the ranks!
广州优号已经与全球著名的领袖企业微软、思科、惠普、CA、趋势、甲骨文等建立紧密的合作关系,同时积极与中国移动开展基于移动增值业务的深度合作,目前公司的自主产品"优号移动商务平台"及"利客发-客户开发管理系统"已经成为广东移动及海南移动的核心信息化产品,并逐步与全国各省移动开展深度合作,广州优号携手各方昂首挺进中国企业信息化建设的行列!
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He studied the esoteric doctrine of the Cabbala, but lost himself in the maze of its abstruse problems, and, after having become, in academic retirement, the pride and glory of his nation, was suddenly forced by a peculiar incident into European notoriety.
他认真研究了深奥的理论Cabbala ,但失去了自己的迷宫其深奥的问题,之后,成为在学术退休,感到自豪和光荣,他的国家,突然被强迫特殊事件融入欧洲声名狼藉。
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From its application, rotation times of streamlined weight become lower, failures of current meters also decrease, thus greatly improving life time of hydrometric cableway.
从使用情况看,铅鱼的旋转频率降低了,流速仪的损坏减少了,从而有效提高缆道的使用寿命。
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In addition, we can also read some jokes of Englishs or the humor essay more at ordinary times, grasping English in hold the belly cachinnation of vivid,humor with full of wit and humour, invisibly and then will like this kind of language gradually, as time passes, more like to more love to learn, more love to learn to more like, very quick can become the virtuous cycle.
除此之外,我们还可以平时多读一些英语的笑话或幽默小品,在捧腹大笑中领略英语的生动、幽默和妙趣横生,无形中便会逐渐喜欢这种语言,久而久之,越喜欢越爱学,越爱学越喜欢,很快就可以形成良性循环。
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Every "Little India" offers a feeling of deja vu a transferred memory of the bustling bazaars of Old Delhi or Ranganethan Street in Madras the peddlers with their cacophonous calls the posters of Bollywood the stray of cow dog pig or monkey pottering around the Hindi music the tandoori hordes of people on the street…that become closer.
每个"小印度"都给人一种似曾相识的感觉,一个被转移的记忆逐渐拉近:喧闹的旧德里市场或是马德拉斯的 Ranganethan 街道,摊贩们刺耳的叫卖声,宝莱坞的海报,牛、狗、猪或猴子在四周晃来荡去,印度的音乐,泥炉炭火,熙来攘往的人群
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Every "Little India" offers a feeling of deja vu, a transferred memory of the bustling bazaars of Old Delhi or Ranganethan Street in Madras, the peddlers with their cacophonous calls, the posters of Bollywood, the stray of cow, dog, pig or monkey pottering around, the Hindi music, the tandoori, hordes of people on the street…that become closer.
每个"小印度"都给人一种似曾相识的感觉,一个被转移的记忆逐渐拉近:喧闹的旧德里市场或是马德拉斯的 Ranganethan 街道,摊贩们刺耳的叫卖声,宝莱坞的海报,牛、狗、猪或猴子在周围晃来荡去,印度的音乐,泥炉炭火,熙来攘往的人群
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Therefore the preparation of light calcium carbonate, which has a big market demand, will become a good approach of the comprehensive treatments of calcium carbide residue.
因此利用电石渣生产市场需求量大的轻质碳酸钙,无疑是电石渣综合治理很好的途径。
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After the death of Muhammad in 632, Aisha, a childless widow of 18, helped her father become first caliph, or ruler, of the Muslims.
去世后,穆罕默德在632的Aisha ,无子女的遗孀18岁的帮助,她的父亲成为第一哈里发,或统治者,对穆斯林。
- 推荐网络例句
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They weren't aggressive, but I yelled and threw a rock in their direction to get them off the trail and away from me, just in case.
他们没有侵略性,但我大喊,并在他们的方向扔石头让他们过的线索,远离我,以防万一。
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In slot 2 in your bag put wrapping paper, quantity does not matter in this case.
在你的书包里槽2把包装纸、数量无关紧要。
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Store this product in a sealed, lightproof, dry and cool place.
密封,遮光,置阴凉干燥处。