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Furthermore, the one-dimensional complexes 26 and 28 with strongπ-πpacking interactions are prepared from DMF solvent, which indicates that the traditional solvent volatilizing method could bring low-dimensional complex.4. By measuring the enthalpy changes of the liquid phase formation reaction for complexes a~e, and calculating the electronic densities of five 5-substituted derivation of isophthalic acid, we can make a conclusion that 5-substituted group changing of the ligand has a little influence on oxygen atoms of carboxyl groups.5. Fluorescence experiments of these complexes indicated that they could be used for luminescence materials in future.6. Using packing saturation rule we calculated and analyzed these series of complexes, and the results showed that the changes of complexes with changes of ligands could be explained from the rule.

在DMF溶剂中得到了具有强π-π堆积作用力的一维配位聚合物[Ln(5-NO_2-bdc)(NO_3)]Ln=Pr(26和Ho(28),表明传统的溶剂挥发合成条件可以得到低维的配合物。4、通过配合物a~e的液相生成反应焓的测定,以及配体阳离子的电子密度计算,进一步佐证了间苯二甲酸的5位取代基变化对配体的羧基氧原子配位能力影响不大的结论。5、荧光特性表明此类配合物可以用于发光材料。6、利用堆积饱和规律对所得系列的配合物的进行计算和分析,发现随着配体的变化,配合物的变化可以从堆积饱和规律出发进行解释。

A polar sensitive probe with selective marks prepared by the invention can be used for compounds comprising mercapto. Owning to the introduction of the maleimide group, the probe can be used for the measurement and research of marks of biomacromolecules that comprise the mercapto and adjacent regional polarity change situations of the mercapto, in particular to the research of the selective marks of the mercapto and the adjacent regional polarity change situations of the mercapto in protein.

本发明制备出一种能够用于含有巯基的化合物的选择性标记的极性敏感探针,该探针由于马来酰亚胺基团的引入,可以用于含有巯基的生物大分子的标记及巯基附近区域极性变化情况的测定和研究,特别是蛋白质中巯基的选择性标记和巯基附近极性变化情况的研究。

In accordance with the invention, the hG-CSF protein can be prepared with high purity through rather simple process facilitating secretion of large amount of hG-CSF fusion protein into the periplasm, which does not require complicated processes such as solubilization and subsequent refolding required for isolation of the hG-CSF protein produced in cytoplasm as insoluble inclusion bodies by conventional techniques, thus, the hG-CSF protein can be widely used as an active ingredient in the development of supplementary agents for anticancer therapy.

根据本发明,通过促进大量hG-CSF融合蛋白分泌到周质中的相当简单的方法可以高纯度制备hG-CSF蛋白,所述方法不需要复杂的加工过程例如对于通过常规技术分离胞质中产生的作为不溶性包函体的hG-CSF所需的溶解和随后再折叠,因此,在开发用于抗癌治疗的补充药物的过程中可用hG-CSF蛋白广泛地作为活性成分。

Second,the sterically demanding substituted magnesium alcoholates can be prepared from dialkylmagnesiums R_2Mg and alcohol.The main disadvantage of this synthesis route lies in the fact that relative expensive dialkyl magnesium compounds,such as Et_2Mg for example,have to be used as starting materials.For this problem,a convenient preparation route of pure dialkylmagnesium from a Grignard reagent.

二、烷基镁法:具有空间位阻效应的仲醇镁和叔醇镁可以直接用烷基镁R_2Mg和醇进行反应来制备,这条路线的主要缺点是烷基镁比较昂贵,为了解决这个问题,本文采用格式试剂来制备烷基镁,将制得的烷基镁与叔丁醇反应制得叔丁醇镁。

First removed the external electrical wiring, and do a good job in marking, for example, asynchronous motor, three-phase power should be prepared with the corresponding tag line for the DC motor, and Patrick do a good job should be winding, armature winding, etc. corresponding with the external wiring tags.

先拆下电机的外部接线,并做好标记,例如对于异步电动机,应做好与三相电源线对应的标记,对于直流电机,应分别做好并励绕组、电枢绕组等与外部接线对应的标记。

When numerous wild animals are bought, slaughtered and processed to be sold for profits, when they are "well" prepared for the nonchalant "epicures", some of whom just eat to flaunt their wealth and some of whom are officials "greasing the mouths" of their superiors for promotion, then, do we have any consideration for the animals — the "other members", just like us, in the ecological chain?

餐馆大肆收购、杀戮、烹煮野生动物为牟取暴利;食客面不改色食用野生动物以饱&口福&或炫耀财富;官吏不惜以野生珍稀动物作为最高规格的宴席;&贿赂&上级领导为自己铺设升官晋级的阶梯——在这个破坏自然生态的&人链&中,可有&他人&的位置么?

Construction bids should be prepared to do the work, the goal of four tender model, analyzed in the bidding process works according to different environmental conditions of the tender should be taken by the strategy are: a high level of operation and management by winning strategy, by improving the original design, to win on the proposal to rationalize the strategies for the future development strategy for low-cost strategy claims.

阐述了建筑工程施工投标应做的准备工作,提出了四种投标目标模式,分析了在投标过程中根据不同的工程环境情况所应采取的投标策略,分别有:靠高水平的经营管理取胜策略,靠改进原设计方案、提合理化建议取胜策略,未来发展策略,低价索赔策。

Construction bids should be prepared to do the work, the goal of four tender model, analyzed in the bidding process works according to different environmental conditions of the tender should be taken by the strategy are: a high level of operation and management by winning strategy, by improving the original design, to win on the proposal to rationalize the strategies for the future development strategy for low-cost strategy claims.

中国建设银行股份有限公司温州分行浙江温州325000;2。温州市伟业造价师事务所浙江温州325000)阐述了建筑工程施工投标应做的准备工作,提出了四种投标目标模式,分析了在投标过程中根据不同的工程环境情况所应采取的投标策略,分别有:靠高水平的经营管理取胜策略,靠改进原设计方案、提合理化建议取胜策略,未来发展策略,低价索赔策。

The primary cause of acquired platelet defect is thought to be activation and release of alpha granules during CPB. Before CPB, platelet-rich plasma was prepared by obtaining the required amount of patient's whole blood by autologous plateletpheresis. PRP could be reinfused after operation in order to protect the function and quantities of the platelets. On the other hand, PRP could be made into autologous platelet gel. APG contains supraphysiologic amounts of growth factors, and has adequate tensile strength and adhesive ability. Therefore, it can be used for hemostasis in operation, sealing wound and enhancing incision or dehiscent sternal wounds healing.

CPB前,利用自体血小板分离技术可将部分血小板从患者全血中分离出来制成富血小板血浆(platelet-richplasma,PRP),PRP可在术后回输,以达到血小板数量和功能的双重保护,另一方面可将PRP制备成自体血小板浆(autologousplateletgel,APG), APG中含有丰富的生长因子,并且具有足够的抗张强度和粘性,因此可起到术中止血、封闭伤口、促进胸骨及伤口愈合的作用。

Mark had the full confidence to be competence for the position with his ablity.but ,when the school officer talked with him and asked him the last question that whether he had the confidence to be the president of student union,he said,'''oh,I am prepared for the failure,it;s really a challenge to me'.

马克信心十足,他觉得,以自己的能力,一定可以胜任。但是,校方找他谈话时,在回答最后一个关于有没有信心做好学生会主席的问题时,他说:&哦,我做好了失败的准备,因为它对我来说,的确是挑战。&

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The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应,而且减少跟风的可能性。

The new PS20 solar power tower collected sunlight through mirrors known as "heliostats" to produce steam that is converted into electricity by a turbine in Sanlucar la Mayor, Spain, Wednesday.

聚光:照片上是建在西班牙桑路卡拉马尤城的一座新型PS20塔式太阳能电站。被称为&日光反射装置&的镜子将太阳光反射到主塔,然后用聚集的热量产生蒸汽进而通过涡轮机转化为电力