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Preparation of the cathode includes:shaping under the press of 40Mpa, sintering at 550℃for 1 hour and at 900℃for 8 hours and threading with molybdenum bar; Considering the literatures we choose CaCl2 as salt for preparation titanium. Pretreatment of salt is for 1 hour at 100℃and for 2 hours at 300℃. Partial pressure of oxygen which need lower than 5.11×10-7Pa to reduct titanium oxides and hygroscopic property of salt need a sealed equipment to electrolyse. And finally successfully designed a satisfied one and the results show that the equipment can be satisfied the requirment of the experiment. Flow of the inert gas is 1.5L/min, the voltage is 2.8 V, temperature is 850℃and time is 2 hours during pre-electrolysis. Flow of the inert gas is 0.2L/min, the voltage is 3.1 V, temperature is 900℃and time changes with the mass of TiO2 during electrolysis, namely the greater need the longer time; To eliminate influence of salt and other impurities, the products need to wash with distilled water and dilute chlorhydric acid , then wash with dilute hydrochloric acid under supersonic wave assistant. Finally, electrometical properties of the electrolysis of TiO2 is researched by cyclic voltammetry and chronoamperometry, and results show that there are two main reodox steps, namely from TiO2 to TiO and from TiO to Ti.
阴极制备主要包括40MPa压力下模压成型、两段式烧结(1小时内升至550℃保温1小时,再1小时升温至900℃保温8小时)及烧结后TiO2块打孔用钼棒串接三个主要环节;实验中选用CaCl2作为电解熔盐,并对其进行预处理(100℃,保温1小时; 300℃,保温2小时);经热力学计算,还原钛氧化物的氧分压至少要低于5.11×10-7Pa,结合电解过程中所用熔盐CaCl2有极强的吸水性的特点,电解装置应有较高的密封性,自行设计了一套密封性可靠的电解装置,便于实验过程中熔盐预处理和氧分压的控制;通过干燥处理预电解过程中Ar流量大约为1.5L/min、电压为2.8 V、温度为850℃、时间为2小时,电解过程中Ar流量大约为0.2L/min、电压为3.1V、温度为900℃,实验结果表明电解时间与TiO2质量密切相关,质量越大需要电解的时间越长;通过自来水冲洗—稀盐酸浸泡、洗涤—在超声波辅助作用下稀盐酸洗涤,可减少熔盐及其它杂质对电解产物检测结果的影响;最后,通过循环伏安法、计时电流法对电解机理的研究,确定电解还原TiO2制备金属钛主要经历了TiO2-TiO-Ti的过程。
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Study the bioactivity of the n-HA/PA66 composite and the effects it would be to body's metabolism of calcium and phosphorus ion in vivo.(3) Study the osteo-conductivity and the ability to repair bone defect of the porous n-HA/PA66 composite and the feasibility use it as the scaffold of bone tissue engineering. Objects and Methods as follows: 1.To evaluate the biocompatability of nano-hydroxyapatite crystals and polyamide composite (n-HA/PA66) with the L929 cells.To proceed the morphological observation and take pictures of L929 cells after 1d,2d,4d,and 7d of co-cultured with extract of n-HA/PA66 ,and direct contact with n-HA/PA66.To determine light absorbtion value of every hole under 500 nm with enzyme linked immunity instrument after 1 d,2 d,4 d,and 7 d of contact of n-HA/PA66 extract with L929 cells,and direct contact with n-HA/PA66.In the meanwhile calculate the relative multiplication rate of cells,and evaluate them by six degree tests for cytotoxicity. To investigate the acute and chronic toxic reaction on the whole body induced by the new nano-hydroapatite crystals and polyamide composite(n-HA/PA66)after implanting in vivo and its effects on partial constitution of animal organs after implanting in vivo,and evaluate the potential and degree of subcuticular stimulation reaction.
本实验主要由以下三部分组成:一、n-HA/PA66 复合材料在动物体内、体外的生物相容性及生物安全性评价二、n-HA/PA66 复合材料植入动物体内的生物活性及近期对机体钙、磷代谢影响的实验研究三、网孔 n-HA/PA66 复合材料作为支架修复兔桡骨节段缺损的动物实验研究主要研究目标及方法如下:参照 GB/T16886.5-1997-ISO 10993-5:1992《医疗器械生物学评价细胞毒性试验体外法》之评价标准和要求,采用规定的 L929 细胞(小鼠结缔组织成纤维细胞),分别经直接接触和材料浸提液与细胞共培养等方式对 n-HA/PA66 复合材料进行细胞毒性测试,采用细胞形态观察法观察两种细胞各组在 24h、48h、72h、5 天后各时相点的细胞形态学变化,并在显微镜下照相,从而对细胞与材料的生物相容性进行定性评价;同时采用细胞生长抑制法,以酶标仪定量测定评价各组 1,2,4,7 天 L929 细胞的相对增殖率,以定量测定并判别材料对细胞的毒性程度。
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While logocentrism, with sense as tool and induction and deduction as guidance, obtains comparatively deeper cognition than sense centralism (the cognition is not limited in partial images and is extended to such aspects as family and genus of the elephant.) Logocentrism is superior to sense centralism, but it is still a kind of very limited method of cognition other than a kind of real whole logical thinking. It carries out cognition within sensation or a slight larger scope, while the materials obtained and used are very limited. To make up the shortage, it needs to isolate the limited materials obtained, and idealizes that the matters temporarily unavailable or hard to be involved in are non-existent.
而逻各斯中心主义以感官为工具以归纳演绎为主导得到了相比感官中心主义较完整深刻的认识(如大象的属和科及习性等而不再限于局部形象),逻各斯中心主义高于感官中心主义,但它仍然是非常有限的认识方法而并非是一种真正的整体逻辑思维,仍只在感官或稍大范围内进行着认知活动,所得到并运用的质料仍是有限的,为弥补不足,它还需要将所得到的有限质料孤立起来而将暂且不能得到或难以涉及的周围的东西理想化为不存在。
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Days of Baidu apologize at this point on its website, say to partial website uses contest price to rank a service to spread false medicine information, it is this company cause to selling operation system to manage not to be pooh-poohed.
17日百度在其网站上就此道歉,称有部分网站利用竞价排名服务推广虚假医药信息,是该公司对销售运营体系管理不善造成的。
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Baidu says:"Partial website uses contest price rank to spread false medicine information, it is Baidu cause to selling operation system to manage not to be pooh-poohed, baidu expresses genuine regret to this ".
百度称:&部分网站利用竞价排名推广虚假医药信息,是百度对销售运营体系管理不善造成的,百度对此表示真诚的歉意&。
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Baidu makes known his position to say to partial website uses contest price to rank a service to spread the false medicine information on its website, it is this company cause to selling the administrative not to be pooh-poohed of operation system, express regret to user and client at this point.
百度表态称有部分网站利用竞价排名服务推广其网站上的虚假医药信息,是该公司对销售运营体系的管理不善造成的,就此向用户与客户表示歉意。
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Changes suddenly in the net joining reason place steel bar section, has the stress concentration, creates the pan partial crack compared to bend the region the crack to widen generally about 25%, this may through cause the lap joint to be located the stress to compare the narrow view the stipulation to solve, may cause the joining reason place crack opening not to surpass the standing operating procedure.
在网片搭接端头处钢筋截面突然变化,产生应力集中,造成板面局部裂缝比一般受弯区域的裂缝加宽25%左右,这可通过使搭接接头位于受力较小处的规定来解决,可使搭接端头处的裂缝宽度不超过标准规定。
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Is located in Chicago's Graphix Products business card printing and membership card production company responsible for a workplace Jason Tews said that as early as 5 years ago they began with two jianeng CLC5000 color digital business card printing and membership card-making machine to engage in commercial business card printing and membership card making to "" transformation of the enterprise is in dire need of hard to get rid of their own partial parts had to be turned over to other digital business card printing and membership card of the status quo.
位于芝加哥的Graphix Products 制卡和会员卡制息公司的负责人Jason Tews说,早在5年后,他们不离不休用两台佳能CLC5000不黑白数字制卡和会员卡制息机来从事贸易制卡和会员卡制息,催促他们&转型&合座是因为企业亟需开脱自己艰苦篡夺的局部板件却务必转交给其他数字制卡和会员卡制息公司的近况。
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It's 15 hours, universal time,here is the news from the voice of american ,i'm david deforest from the VOA news center in washington.governments around the world are moving to boost the banks was more tie billion dollar beyer today.they are trying to get banks to rezoom london.and restore the stock and credit market that thread the push the world into a recession.but consider the government action we should many ,but not at all , that dasters.key stock markets in hongkong ,britain,germany and united stated gained between 4 and 10percents , a huge reversal from major loses suffers over the last week, but the key market in moxico dropped so sharply the trading was suspended.the british government has a anouncement it is partial renationalization three british banks with up to six billion dollars of taxpayer's money.president minister golden brown promises the unpresident bayer loud is it important step in foring out the frozen money market.from VOA time ravers has reported from london.you gonna both move the money again the british government wanna thirsty four billion dallors was the capital and into the royal bank scotland just less than thirty billion into loyal's tsben ach box.dunst tution is curtely really go shading emerge terms .prime minister golden brown says the stand by is do nothing with never anoption.the extrodinary retimes was financial martket seems to work .the government canos just made people ont the owe to be bufit about.
现在是格林尼治时间下午三点整,这是美国之音新闻节目。我是华盛顿新闻中心的大卫。世界各地政府今天正在积极给予银行几十亿美圆的紧急援助。他们试图让银行重新带领和开始已经停止的信贷时常,担心世界经济进入衰退。政府的协调动作鼓舞了许多企业,但并不是所有的投资者。在香港,英国,法国,德国和美国的重要股票都上升了4到10个百分点,自过去一个星期的损失中一次巨大的倒转。但是莫斯科的一个重要指数在停盘时积聚下滑。英国政府已经声明,三家部分国有化银行拥有纳税人630亿美圆。首相GB保证这次的前所未有的紧急援助对于金融市场的解冻十分重要。TOM在伦敦发回报道。又一次大胆行动以恢复金融市场,英国政府将注340亿美圆的资金在苏格兰皇家银行和只不到300亿美圆在Lloyds-TBS和HBOS,这两所机构现在正在重新谈判合作项目。首相GB说站在一边什么事不做永远不是一个选择。在现在特殊的时刻,金融时常停止工作,政府不能让人民将自己的利益推来推去。
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Because waits for in stays at the hotel entrance the singer fan population to be numerous, but also has the partial singer fan to meet does not give a thought to the safety to pursue the vehicle crazily, always for safety, the flywheel sea four people by the staff "the pass" in the hotel, are not permitted they to go out.
由於守候在下榻饭店门口的歌迷人数众多,还有部份歌迷会不顾安危疯狂追车的,总是为了安全起见,飞轮海四个人被工作人员「关」在饭店里,不准他们外出。
- 推荐网络例句
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With Death guitarist Schuldiner adopting vocal duties, the band made a major impact on the scene.
随着死亡的吉他手Schuldiner接受主唱的职务,乐队在现实中树立了重要的影响。
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But he could still end up breakfasting on Swiss-government issue muesli because all six are accused of nicking around 45 million pounds they should have paid to FIFA.
不过他最后仍有可能沦为瑞士政府&议事餐桌&上的一道早餐,因为这所有六个人都被指控把本应支付给国际足联的大约4500万英镑骗了个精光。
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Closes the eye, the deep breathing, all no longer are the dreams as if......
关闭眼睛,深呼吸,一切不再是梦想,犹如。。。。。。