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METHODS The structures of compound I, extracted from Clausena lansium Skeels, and synthesized compound III were determined by single crystal X-ray diffraction analysis. The stereo-structures of compound II and IV were also built up through Tripos force field based on crystal structures of compound I and III. RESULTS The molecular formula and molecular weight were found to be C18H17O2N and 279.34 respectively.
方法用单晶X-射线衍射分析法测定了从植物黄皮提取物中分离得到的化合物I和采用合成方法得到的化合物III的晶体结构,并用分子力学计算方法分别模建化合物II和IV的立体结构。
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Once you have determined what you would like to be doing, visualize it.
一旦你确定了你喜欢做什么,设想一下。
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By the experiment studying, the relationship of ξ1, and v1 is determined. In a word, the water-power calculation of pipe can be done by taking corresponding ξ1, according to the design velocity v1 and .
通过实验研究,确定了ξ1与流速v1及A1/A2之间的关系,在设计中,只要根据设计流速v1与A1/A2就可以采用相应的ξ1进行管道的水力计算。
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Reading "cask" theories feeling recently, i read a "log links theory," emotionally,"akebia theory" tells us : can be equipped with a number of buckets of water is determined by the shortest piece of dried; the other hand, not only can carry buckets of water from a number of the shortest piece of dried decision, but also by the gap between the board to decide.
读&木桶理论&有感近日,我读了&木通理论&后深有感触,&木通理论&告诉我们:一个水桶能装多少水,是由最短的一块木片决定的;另一方面,一个水桶能装多少水不仅由最短的一片木片决定,还要由木板间的缝隙来决定。
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The diagenetic stage and pore-evolution properties of clastic rock can be effectively determined according to the assemblage of authigenic clay mineral.
根据自生粘土矿物的组合特征,可以有效地确定碎屑岩的成岩阶段及其孔隙发育特征。
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In the aqueous solution of sodium hydroxide,benzoylformic acid can coordinate with 2,4-dinitrophenylhydrazine to form a complex which has maximum absorption at 458 nm.Thus the content of benzoylformic acid can be quantitatively determined.
在氢氧化钠溶液中,苯乙酮酸和2,4-二硝基苯肼形成一种红棕色的溶液,该溶液在458 nm处有最大吸收,据此可以快速分析混合物中苯乙酮酸的含量。
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The synthesis of l-(4-acetylaminophenyl)-2-bromo-1-propanone was discussed, and the mechanism and possible factors were analyzed. Hence the routine was determined, in which l-(4-acetylaminophenyl)- 1-propanone was reacted with Bromine dissolved in ethanol, so that the a -bromination can be carried on, resulted in the yield of up to 70.4%.
探讨了1-(4-乙酰胺基苯基)-2-溴代-1-丙酮的合成方法,分析了反应机理和影响因素,确定将1-(4-乙酰氨基苯基)-1-丙酮溶解在乙醇中以溴的乙醇溶液进行α-溴化的合成路线,产率可达70.4%。
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MethodsThe resin suitable for separation of chromone glycoside was determined by static absorption experiment on seven different kinds of resins, and further more, the absorption and elution of chromone glycoside on the selected resin were studied by fixed bed absorption experiment. ResultsThe AB-8 resin was founded to be suitable for separation and purification of chromone glycoside.
方法采用静态吸附实验考察D101,AB8,S8,X5等7种大孔吸附树脂对升麻苷和5O甲基维斯阿米醇苷两种色原酮苷的吸附效果,筛选出吸附性能较好的树脂;对所筛选出的树脂,进一步采用固定床吸附法分离玉屏风提取物中色原酮苷,探讨主要参数对色原酮苷固定床穿透曲线及洗脱曲线的影响。
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Studies on stability indicated that PHGF proliposomes should be stored at low temperature and against light, which ensured unchange of their redispersity, content of drug, encapsulation efficiency, acid value and peroxide value. Liposomes were multilamellar vesicle structure under transmission electron microscopy. Average particle size was 0.65 micrometer, ranging from 0.09 micrometer to 1.21 micrometer. Cryoscopic value was 0.64 C determined by cryoscopic method, which was a little higher than that of isotonic solution.
以透射电镜观测PHGF前体脂质体再分散后的形态为囊泡状;激光散射法测得平均粒径为0.65μm,且粒度分布在0.09μm~1.21μm之间;该脂质体荷负电,ζ电位为-44.23mV;冰点降低法测得冰点降低度数为0.64℃,略高于等渗溶液冰点降低度数;测得粘度为1.83mPa·s,达到生理要求;此外,对PHGF脂质体的刺激性、溶血性、热原、异常毒性和过敏沈阳药科大学硕士学位论文拘要性检查表明均符合静脉注射给药的标准。
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Based on the problem of various types of catalyst and according to the features of carbonylation catalysts reactions, our team has been designed a series of new metal complexes of benimidazoles, which can be used for carbonylation catalyst of industry. Seven new benzimidazole derivatives were prepared by the o-phenylenediamine、oxalic acid、glycolic acid、monomethyl monopotassium malonate、ethyl cyanoacetate、succinic anhydride. The structures of them were confirmed by IR、Elemental analsis. The crystal structures of d and e were determined by X-ray single crystal diffraction of Germanic Bruker Smart APEX II CCD. The catalysis of them was tested by carbonylation reactions.
本文设计以邻苯二胺和草酸、羟基乙酸、丙二酸单甲酯、氰基乙酸乙酯、丁二酸单甲酯为原料采用PPA催化和无机酸催化法,合成了4种苯并咪唑-2-羧酸衍生物并进行了表征;培养了2个化合物d、e的晶体并测定和讨论了晶体结构;制备了3种未见报道的苯并咪唑金属配合物,对配合物在羰基化法制醋酐-醋酸反应的催化作用进行了初步试验。
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On the other hand, the more important thing is because the urban housing is a kind of heterogeneity products.
另一方面,更重要的是由于城市住房是一种异质性产品。
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Climate histogram is the fall that collects place measure calm value, cent serves as cross axle for a few equal interval, the area that the frequency that the value appears according to place is accumulated and becomes will be determined inside each interval, discharge the graph that rise with post, also be called histogram.
气候直方图是将所收集的降水量测定值,分为几个相等的区间作为横轴,并将各区间内所测定值依所出现的次数累积而成的面积,用柱子排起来的图形,也叫做柱状图。
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You rap, you know we are not so good at rapping, huh?
你唱吧,你也知道我们并不那么擅长说唱,对吧?