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New contributions of this work are as follows:(1). Preparation of Spherical MgCl_2-Supported Late-Transition Metal Catalysts for Ethylene PolymerizationFacile and effective immobilization of late-transition metal catalysts. 2,3-bis-(2,6-diisopropylphenyl) butane diimine nickel dibromide (1) and 2,6-bis-[1-(2,4,6-trimethylphenylimino)ethyl]pyridine iron dichloride (2), for ethylene polymerization has been achieved, using spherical MgCl_2 supports obtained by thermal dealcoholization of MgCl_2·2.56C_2H_5OH, and the effects of dealcoholization temperature on supported late-transition metal catalysts and the properties of resultant polymers were studied, the results indicated that:1.Supports with appropriate mechanical strength, high surface area and high porosity could be prepared by thermal dealcoholization of spherical MgCl_2·2.56C_2H_5OH supports; 2.BET, XRD, IR, SEM, GPC and DSC analyses indicate that the activities of the supported late-transition metal catalysts and the properties of resultant polymers are strongly dependent on the dealcoholization temperature.
本工作的新贡献如下:(1)、球形氯化镁负载后过渡金属催化荆催化乙烯聚合本文将配合物2,3-双(2,6-二异丙基苯亚胺)丁烷二溴化镍(1)和配合物2,6-二[1-(2,4,6-三甲基苯亚胺)乙基]吡啶二氯化铁(2)分别直接负载于经不同热脱醇温度处理的球形氯化镁载体上,研究了氯化镁载体的脱醇温度对负载化后过渡金属催化剂及其聚合物的影响,研究表明:1、通过对球形MgCl_2·2.56C_2H_5OH载体进行热脱醇处理,可以获得合适机械强度、较高比表面积和较高孔隙度的球形氯化镁载体;2、BET,XRD,IR,SEM,GPC和DSC研究表明,脱醇温度极大地影响负载后过渡金属催化剂的活性和聚合物的性能。
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New contributions of this work are as follows:(1). Preparation of Spherical MgCl_2-Supported Late-Transition Metal Catalysts for Ethylene Polymerization Facile and effective immobilization of late-transition metal catalysts. 2,3-bis-(2,6-diisopropylphenyl) butane diimine nickel dibromide (1) and 2,6-bis-[1-(2,4,6-trimethylphenylimino)ethyl]pyridine iron dichloride (2), for ethylene polymerization has been achieved, using spherical MgCl_2 supports obtained by thermal dealcoholization of MgCl_2·2.56C_2H_5OH, and the effects of dealcoholization temperature on supported late-transition metal catalysts and the properties of resultant polymers were studied, the results indicated that: 1.Supports with appropriate mechanical strength, high surface area and high porosity could be prepared by thermal dealcoholization of spherical MgCl_2·2.56C_2H_5OH supports; 2.BET, XRD, IR, SEM, GPC and DSC analyses indicate that the activities of the supported late-transition metal catalysts and the properties of resultant polymers are strongly dependent on the dealcoholization temperature.
本工作的新贡献如下:(1)、球形氯化镁负载后过渡金属催化荆催化乙烯聚合本文将配合物2,3-双(2,6-二异丙基苯亚胺)丁烷二溴化镍(1)和配合物2,6-二[1-(2,4,6-三甲基苯亚胺)乙基]吡啶二氯化铁(2)分别直接负载于经不同热脱醇温度处理的球形氯化镁载体上,研究了氯化镁载体的脱醇温度对负载化后过渡金属催化剂及其聚合物的影响,研究表明: 1、通过对球形MgCl_2·2.56C_2H_5OH载体进行热脱醇处理,可以获得合适机械强度、较高比表面积和较高孔隙度的球形氯化镁载体; 2、BET,XRD,IR,SEM,GPC和DSC研究表明,脱醇温度极大地影响负载后过渡金属催化剂的活性和聚合物的性能。
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The feedback resistance, R1, is dependent on cell sensitivity and should be chosen for either maximum dynamic range or for a desired scale factor. R2 is elective: in the case of photovoltaic cells or of photodiodes, it is not required in the case of photoconductive cells, it should be chosen to minimize bias current error over the operating range.
反馈电阻R1的取值由电池的灵敏度和要求的最大动态范围,或者需要的电流——电压转换比例决定。R2分情况选取:在光电池和光电二极管时不需要这个电阻,在光电导的时候,电阻的阻值应该能使在工作范围内,由OP输入偏置电流所带来的误差最小。
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Today the software is becoming more and more dependent on the hardware platform, especially the I/O subsystem. There are usually a mass of data that from the video or audio source to be processed, sometime they even need to be real time processed.
今天的软件应用越来越依赖于硬件平台,特别是输入输出子系统,日常应用中常常会出现从视频源和音频源传来的大量的流数据要处理,甚至有许多的数据是要求实时处理的。
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In contrast to their fears that the election would deliver an unstable coalition dependent on India's reform-allergic leftwing parties, investors are looking at what promises to be a stable government based on one of the large national parties.
投资者一度担心,大选将产生一个不稳定的联合政府,依赖于对改革"过敏"的左翼政党,但如今他们看到的,将是一个由印度最大全国性政党之一组建的稳定政府。
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If desired, you can manifest a power at a lower manifester level than normal, but the manifester level must be high enough for you to manifest the power in question, and all level-dependent features must be based on the same manifester level.
如果你愿意的话,可以用比你目前的显能者等级更低的等级状态来展现一道异能,但是被调低之後的等级状态必须要达到展现该道异能的最低等级要求,而且所有和等级相关的异能特性都必须以降低之後的显能者等级来进行计算。
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A plugin is a more decoupled run-time library, supposedly not dependent on the main application being a certain version, and preferably the requirements on the plugin should be a bit more loose (they shouldn't need to know about every header file and #define in the application, and they need not mutually resolve massive amounts of global symbols).
插件是一个较为分离运行时库,据说不是主要的是某一个版本的应用程序依赖性,最好是插件的要求应更宽松一点(他们不应该需要了解每一个头文件和#在应用程序中定义,他们需要互不解决全球大量符号)。
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It is revealed that both the roasting and cooling air flow run radially at inlets and then run slantingly upwards or downwards into roasting-preheating zone inside IVAC. And the gas flow in the whole soaking zone is weakened. There are possibly three gas flow patterns in PSF, which are mainly dependent on the ratio of inflow, i.e., the greater the ratio is, the higher the downward roasting air flowrate and the lower the upward air flowrate will be. The critical ratio of inflow mainly depends on the constructional parameters and packed bed conditions of PSF.
结果表明:焙烧风和冷却风在进口处呈放射状,之后斜向上或斜向下分别流入焙烧-预热带和导风墙内;整个均热带内气流较为薄弱;炉内存在三种气流分流的可能,流入风量比是决定气流分流的最主要因素,其中,流入风量比增加,焙烧风下行趋势增大,而冷却风上行趋势减小;临界流入风量比主要取决于结构参数和料层情况。
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The analyses of electronic structures shows that the catalytic reactivities for H2 adsorption of the different surfaces are dependent on the numbers of s orbital bonding electrons around Fermi level for the uppermost layer metal atoms which interact directly with H2. It is easy to form vacancy for hydrogen atoms next to iron atom, which indicates that hydrogen atom cannot be escaped, but it is difficult to from vacancy for hydrogen atoms next to magnesium atom, which indicates that hydrogen atom can be escaped. Hence it is thought that the change of dehydrogenating properties of MgH2 with or without a little iron addition attributes to the weakened bonding between magnesium and hydrogen.
分析电子结构发现:空位缺陷有助H2吸附于Mg表面,与Mg(0001)表面最上层与H2直接产生吸附作用的金属原子在费米能级附近s轨道的成键电子数密切相关;在Fe合金化MgH2体系中,与合金化元素Fe近邻的H原子形成空位的难度增加,H原子较难释放;与Mg近邻的H原子形成空位的难度减少,H原子容易释放;Fe合金化导致Mg-H之间存在较弱的成键作用,因此,MgH2体系的解氢性能得到提高。
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Simultaneously, the exports of ionization rate and nonionzed concentration are set up as a powerful tool for studying thoroughly the freeze-out effect. dN〓/dp and dN〓/dn are neglected in the linearized equation system of the iteration methods of Newton and Gummel, due to having lower 15 orders or more than dN〓/dn and dN〓/dp, thus the computing effort is cut down with no effect on precision. A new cut-off technique is adopted to accelerate the convergence speed, about twice reduced for Newton iteration method and six times or so for Gummel iteration method. The approximate formulae of Fermi-Dirac statistics are also put forward with simpler form and higher precision. 3. A term dependent on time is added to the electron and hole current succession equations respectively. It is only this model that conservation of charge in transient analysis and alternating small-signal analysis at low temperature can be kept by. 4. The performance of SE-PISCES is explained by the simulation example of PISCES-2B, diode.
研究了低温半导体器件模拟的数值方法:对载流子浓度进行了新的归一化;编制了不考虑掺杂所引进的内建电场时的电离率计算程序;由于低温杂质电离率随偏压状态而变化,为此编制了每次求解迭代时的电离浓度计算程序,并将其插入到求解迭代程序中;同时,设置了杂质电离率和未电离杂质浓度的出口点,为更深入地研究冻析效应提供了有力工具;在Newton迭代法和Gummel迭代法的线性化方程组中忽略了dN〓/dp、dN〓/dn,是因为它们比dN〓/dn、dN〓/dp低15个数量级以上,这样减小了计算量又不影响模拟精度;对Newton迭代法和Gummel迭代法采取了新的截断技术,提高了收敛速度,Newton法迭代法和两次左右,Gummel法减少六次左右;给出了表达式更简单而精度更高的Fermi-Dirac积分近似计算公式。
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Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).
呼气,收缩臀部肌肉;拱起身体,尽量抬起头来,右腿伸直朝向天花板(膝微屈,以避免肌肉紧张)。
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The cost of moving grain food products was unchanged from May, but year over year are up 8%.
粮食产品的运输费用与5月份相比没有变化,但却比去年同期高8%。
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However, to get a true quote, you will need to provide detailed personal and financial information.
然而,要让一个真正的引用,你需要提供详细的个人和财务信息。