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Based on the previous literatures, the following major innovation works were carried out in this dissertation:(1) The derivatization reaction conditions of ephedrine and pseudoephedrine with sensitive derivation reagent in aqueous system were studied and two new methods were developed for the assay of them by microemulsion electrokinetic chromatography and micellar electrokinetic chromatography with LIF detection. The sensitivity and analysis times were greatly improved compared with the previous reports;(2) A new method of CZE with indirect LIF detection was developed for the simultaneous determination of six coumarin compounds (esculin, esculetin, isofraxidin, genistein, naringin and sophoricoside) with fluorescein as the probe. The proposed method enlarges the application range of LIF detector, and provides new approach for the analysis of certain compounds difficult to derivatize;(3) Based on the above research, an MEKC with indirect LIF detection method for the simultaneous determination of adenine and guanine in DNA extracts from fungus, maize and soybean was established;(4) A new method for the investigation of the complexes formed between human serum albumin and ampicillin sodium under the simulated physiology conditions using laser light scattering technique was developed.
该论文在综述前人工作的基础上,开展了如下未见文献报道的创新性的研究工作:(1)使用灵敏的衍生试剂对麻黄碱和伪麻黄碱在水体系中的衍生反应条件进行了系统研究,建立了微乳电动色谱-激光诱导荧光检测法和胶束电动色谱—激光诱导荧光检测法测定麻黄碱和伪麻黄碱的灵敏分析新方法,与以前的报道相比,灵敏度和分析时间均有很大改善;(2)使用荧光素钠作为背景荧光试剂,建立了同时分析测定六种黄酮类化合物(秦皮甲素、秦皮乙素、异秦皮定、染料木素、柚皮苷和槐角苷)的毛细管区带电泳—间接激光诱导荧光检测新方法,扩大了激光诱导荧光检测的应用范围,对难衍生化合物的分离分析提供了一种新思路和新途径;(3)以荧光素钠作为背景荧光试剂,建立了一种用于同时测定食品提取DNA中的腺嘌呤和鸟嘌呤含量的胶束电动色谱—间接激光诱导荧光检测新方法;(4)用动态和静态激光散射法研究了模拟生理条件下人血清白蛋白与氨比西林钠盐相互作用所形成的复合物,为药物分子与蛋白质的相互作用、药代动力学等的研究提供了一种新思路。
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A region superresolution spectrum estimation method based on coventional DFT computation is presented for obtaining one dimensional range profile, which has the advantages of real-time in computation and robustness under clutter and noise background over general superresolution methods. A iterative extropolation method based on both priori knowledge provided by conventional DFT spectrum and matching filtering process of target return data is also presented for range profile processing, which has the advantages of robustness in improving range resolution, suppressing clutter and noise.
在目标一维距离成像谱估计中,提出了以常规DFT为基础的邻域超分辨谱估计方法,它与普通超分辨算法相比,具有实时性强、在杂波与噪声背景中稳健性好的优点;在外推成像处理中,提出了以常规DFT目标结构图像为约束条件并结合目标信号准匹配滤波处理的迭代外推算法,其优点是稳健性好,能适度地提高距离分辨力但保留适度的抗杂波抗噪声能力。
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The software and hardware realizing scheme of high performance, AC servo system based on the digital-analog mixed type of 16 bits high performance, single piece micro computer 80C196 is presented in this paper It expounds the theory and method of system design for industrial applications, and it also gives out the situation of system industrial applications Based on the analysis of the influential characteristics of servo system the method of improving the system precision, estimative model of loading torque and instantaneous velocity, compensative predictive control under low speed motion are dicussed in this paper.
论述了面向工业对象的系统设计原理与方法。并给出了本文系统工业应用的情况。在分析影响交流伺服系统性能的基础上,提出了改善系统精度的方法,给出了负载力矩和瞬时转速的估计模型,研究了低速运行时的补偿预测控制,提高了伺服系统低速稳定运行的范围。
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A new soft decision metric for QAM is presented in this paper. Unlike traditional soft decision metric based on minimum Euclidean distance, the proposed metric is based on the bit confidences.
传统的软判决度量大多是基于最小欧氏距离准则生成,该文提出一种基于比特置信度快速生成QAM软判决度量的算法,通过将比特置信度引入到QAM软判决度量的计算中来减少计算的复杂性。
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Distance-based and density-based clustering algorithms in Euclidean space can be used in this framework.
欧几里德空间内基于距离、基于密度的聚类算法均适用于本框架。
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A variable-step modified Euler time integration method is proposed and analyzed. Four major factors that affect the efficiency of the variable-step modified Euler time integration method are discussed. These include stability and accuracy analysis for the damped fix-step modified Euler integration formula, adjustment method of the fix-step basic integration formula to accommodate step-size changes, suitable range of the step-size selection strategy based on truncation error concept and development of the step-size selection strategy based on apparent frequency concept to satisfied the specified error bound and stability condition.
提出了变步长修正Euler时间积分法,详细讨论了影响变步长修正Euler时间积分算法效率的四个主要因素,它们包括:有阻尼问题的修正Euler法的稳定性和精度分析,调整固定步长的基本积分公式使之容纳步长大小变化的研究,基于截断误差概念的步长大小选择策略适用范围的讨论,同时满足规定误差界和稳定性条件的、基于表观频率概念的步长大小选择策略的建立。
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Such as the beverage trademark Coca Cola, there is no meaning of its own, translated as "Coca-Cola", the method is based on a transliteration-based, but the transliteration of Chinese characters when they are not taken according to the rules of the selected sound and meaning, but to use the Chinese language in a special language phenomena - euphony, see at a glance the catering commodities for consumers need to purchase food is naturally meaningful.
就像如饮料商标Coca Cola,其本身并无含义,译为"可口可乐",所用方法以音译为主,但音译时所取地汉字并不是按音义地规则选取地,而是利用了汉语中地一种特殊语言现象——谐音,一看便知是饮食类商品,对于需要购买预购饮食地消费者来说自然是意味深长句号。
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The marks of evidentiary system are standard of proof based on weight of evidence and credibility rules based on competency of evidence.
证据制度的标志应为以证据证明力为支点的证明标准与以证据资格为支点的证据能力法则。
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A minimum TOEFL score of 530 for paper examination; 179 for computer based and 71 for Internet based.
最低托福成绩为530的文件审查; 179基于计算机和互联网为基础的71 。
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Based on the research on traveling salesman problem, a scheduling algorithm based on exchange is presented. As is demonstrated by experiments, the results from our algorithm, as far as we know, are the best.
5借鉴了研究旅行商问题的成果,从而提出了基于交换的调度算法,其实验结果超过了我们见到的调度结果。
- 相关中文对照歌词
- BasedGod Fucked My Bitches
- CNBFTBGB Based Freestyle
- Money Over Suckas
- Everything Based
- Be Brave Welcome Home
- Wonton Soup
- Cashout On Me Based Freestyle
- Pretty Boy
- Bitch Mob Gangsta
- So Based
- 推荐网络例句
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Salt is good, but if the salt becomes flat and tasteless, with what do you season it?
14:33 盐本是好的,盐若失了味,可用什么叫它再咸呢?
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He reiterated that the PLA is an army of the people under the leadership of the Communist Party of China.
他重申,人民解放军是在中国共产党领导下的人民军队。
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After five years at the Laue-Langevin Institute in Grenoble, France, Jolie turned his focus to experimental work when, in 1992, he accepted a position at the University of Fribourg in Switzerland.
他在法国格赫诺柏的劳厄–蓝吉分研究所工作了五年之后,1992年转往瑞士夫里堡大学从事实验研究。