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The mian works are as follows:(1)By coprecipitation technique and coprecipitation- gel technique the nano zirconia powder was produced, factors affecting the properties of nano zirconia powder such as pH and the content of stabilizator are analyzed;(2)By the new pressless sintering process, the nano zirconia ceramic was produced, factors which can affecting the properties of nano zirconia sinter body such as moulding press and the sinter temperature are analyzed;(3)By the microtherm pressless sintering process, the nano copper added functional zirconia ceramic composite was produced, microscopic dimensionality and electric properties of such sinter body and the factors affecting such sinter body are analyzed;(4)By the self-invented "external albumen coating" technique the zirconia powder was successfully coated by carbon in the corresponding sinter body, which can help solve the traditional aggregation problem to some degree;(5)Based on analyze the characteristics in the nano powder sinter process, the "three-ball sinter model" was proposed, for the relationship between the relative density and porosity of sinter body, by mathematical fitting, such model was successfully verified.

本研究比较系统地研究了纳米氧化锆陶瓷的合成与成型机理,特别是讨论了纳米氧化锆陶瓷的稳定性,为防止纳米颗粒在外场作用下的团聚和长大提供了理论基础和实验数据,具体工作有以下几方面:(1)采用共沉淀法和共沉淀-凝胶法制备了纳米氧化锆粉体,并分析了pH值和稳定剂含量对粉体性能的影响;(2)采用新型无压烧结工艺制备了纳米氧化锆陶瓷,并分析了成型压力和烧结温度对烧结体性能的影响;(3)采用低温无压烧结工艺制备出添加纳米铜的功能性纳米氧化锆复合陶瓷,并分析了烧结体的微观尺度和电学性能的变化以及影响因素;(4)通过自创的&鸡蛋清外敷法&在真空镀膜台上对纳米氧化锆粉体进行包敷碳颗粒的表面处理,并采用真空烧结工艺制得相应烧结体,初步开始解决陶瓷烧结过程中团聚长大这一传统难题;(5)通过分析纳米颗粒在制备烧结体过程中的实际特点,提出了&三球烧结数学模型&,通过引入坯体相对密度和孔隙率的相对关系分析并通过自行编写的数学拟合软件,验证了这一数学模型。

The barium-strontium titanyl oxalate precursor powder was prepared successfully by using the simple oxalate chemical coprecipitation method. The pyrolysis of BSTO at 905℃ in air produced barium-strontium titanate powder. BST powder was characterized with SEM, TEM, XRD and FT-IR, which revealed that the powder was spherical, highly pure, perovskite, and the average particle diameter was 36nm.

采用草酸盐化学共沉淀法制备了草酸氧钛锶钡前驱体,通过905℃高温煅烧,制得了高纯纳米钛酸锶钡,并利用SEM、TEM、FT-IR和XRD对其进行了表征;并将该粉体应用于水中重金属镉离子的吸附。

At the same time for all kinds of snake venom lyophilized powder, fresh gall bladder, do gall bladder,±, snake powder, snake oil, live snakes, frozen snake, snakes do, acutus wine, liquor±, viper wine, snake wine, snake powder capsule, powder Shedan, Snake Oil Soft Capsule, recreation Capsule, Capsule Oolong, snakes ointment, Dongchuang Unguentum, Shedan SOD Honey, Honey SOD snake oil, disinfectant spray, snake leather, snake handbags, snake package with products such as snake skin, forming from the aquaculture, processing and selling one-stop service system.

同时可供各种蛇毒冻干粉、鲜蛇胆、干蛇胆、蛇鞭、蛇粉、蛇油、活蛇、冻蛇、蛇干、五步蛇酒、蛇鞭酒、蝮蛇酒、蛇胆酒、蛇粉胶囊、蛇胆粉胶囊、蛇油软胶囊、康乐宝胶囊、乌龙宝胶囊、蛇油膏、冻疮膏、蛇胆SOD蜜、蛇油SOD蜜、消毒喷剂、蛇皮革、蛇皮包、蛇包带等蛇皮工艺制品,形成从养殖、加工到销售一条龙服务体系。

A preparation method of the visible-light photocatalyst Bi2WO6 nano-powder is characterized by comprising the steps as follows:(1) the selection of raw materials;(2) bismuth nitrate Bi(NO33 question mark 5H2O is added into a citric acid solution to obtain the citric acid solution containing white sediment;(3) EDTA is added into ammonia water which is then added dropwise with the citric acid solution containing the Bi(NO3)3 question mark 5H2O so to obtain a solution of bismuth;(4) the solution of bismuth is added with (NH4)6W7O24 question mark 6H2O solution to form a precursor solution which is then stirred, dried, coked, cooled and ground to obtain decarburized powder;(5) the decarburized powder is roasted for 2h to 4h under 450 DEG C to 550 DEG C to obtain the visible-light photocatalyst Bi2WO6 nano-powder.

可见光催化剂Bi 2 WO 6 纳米粉体的制备方法,其特征在于它包括如下步骤:1原料的选取;2将Bi(NO 3 ) 3 5H 2 O加到柠檬酸溶液中,得到含有白色沉淀的柠檬酸溶液;3将乙二胺四乙酸加到氨水中,并缓慢滴加入含有Bi(NO 3 ) 3 5H 2 O的柠檬酸溶液中,得铋的溶液;4将(NH 4 ) 6 W 7 O 24 6H 2 O溶液加入上述铋的溶液中,组成前驱液;搅拌,干燥,焦化,冷却后,研磨,得去碳的粉体;5将去碳的粉体在450~550℃下焙烧2~4h后,得到可见光催化剂Bi 2 WO 6 纳米粉体。

Meal: in the city of Qiongshan Ling Shanzhen famous, and its ratio of Hainan powder coarse powder, the production process of Hainan powder with a slightly different, the food is also a law "to eat salt," but characterized by powder Shuanghua quality, marinades focus on raw seafood, highlighted a "taste of seafood."

灵山粗粉:是在琼山市灵山镇一举成名的,其粉比海南粉粗,其生产工艺与海南粉略有不同,其食法也是&腌吃&,但特色是粉质爽滑,腌料注重海鲜原料,突出一个&海鲜味&。

At the same time production and management: fermented flour paste, bean paste, chili pepper oil, pepper oil and a variety of pickles and seafood powder, soy sauce powder, vinegar powder, raw powder, monosodium glutamate, sodium, etc. VC thirty different kinds of products; are Subei , Lunan region's largest manufacturer of condiments.

同时还生产和经营:甜面酱、豆瓣酱、椒油辣酱、油辣椒和各种酱菜及海鲜粉、酱油粉、香醋粉、生粉、味精、异VC钠等三十余种产品;是苏北,鲁南地区最大的调味品制造企业之一。

PLLA composites with cotton powder, wool powder and opal powder were fabricated with the powder contents of 10% and 20% respectively.

在相同的工艺条件下,制备了棉粉、羊毛粉和蛋白石粉体与PLLA的复合材料,以及PLLA膜材料。

Carbide in the process of grinding, the powder will produce some waste, recycling all kinds of high-priced steel scrap tungsten carbide tool steel and tungsten, tungsten alloy Trim, grinding material, PCB waste bit, tungsten steel tool, used powder tungsten, tungsten steel powder, tungsten steel scrap, carbide grinding materials, including waste tungsten alloy grinding expected, the film cutter, drill, milling cutter , NC knives, cutting-tungsten steel mold, drawing die, a round cutter, saw, anvil, PCB bit, V-CUT knives, gongs, knives, a high proportion of alloy, non-magnetic alloy, tungsten steel powder, tungsten wire cutter Tungsten steel waste, and other tools.

硬质合金在打磨的过程中,会产生一些粉末废料,高价回收各种硬质合金钨钢报废工具以及钨钢、钨合金边角料、磨削料、废PCB钻头、钨钢工具、废钨粉、钨钢粉末、钨钢废料、硬质合金磨削料、含钨废料、合金磨削料、铣刀片、钻头、立铣刀、数控刀具、线切割钨钢模具、拉丝模具、圆切刀、锯片、顶锤、PCB钻头、V-CUT刀、锣刀、高比重合金、无磁合金、钨钢粉末、钨绞丝等各种钨钢废工具。

This makes Ni-W-P powder more suitable for partial hydrogenation of dienes. The kinetic results suggest there are some different between the active sites of Ni-P and Ni-W-P powder. DSC, XRD and EXAFS results suggest that the tungsten codeposition makes Ni-W-P powder more amorphous than Ni-P powder.

动力学结果表明在两种合金微粒上,不仅环戊二烯与环戊烯的相对配位能力不同,而且它们各自的反应速率常数也不一样,表明非晶态Ni-P、Ni-W-P合金微粒的催化活性中心存在着一定的差异。

Extraction of pine nut oil, residual oil dregs food after extraction as well as its producing method, that is obtaining pine nut after exuviating and removing skin; obtaining pine nut oil by exceed critical CO2 hydro-extraction; to get out the residual oil dregs after extraction to dry, then to grind into powder, and adding Chinese chestnut powder and walnut powder to mix as well as dry again to produce complex pine nut nutrition powder.

松籽仁油的萃取、萃取剩余油渣食品及其制造方法,是松籽经脱壳、去衣得松籽仁;进行超临界CO 2 流体萃取得松籽油;萃取剩余油渣取出进行烘干,再经磨碎成粉、加入板栗粉和核桃粉、混合、再次干燥成复合松籽仁营养粉。

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